114 research outputs found

    Magnetic properties of GdT2T_2Zn20_{20} (T = Fe, Co) investigated by X-ray diffraction and spectroscopy

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    We investigate the magnetic and electronic properties of the GdT2T_2Zn20_{20} (TT = Fe and Co) compounds using X-ray resonant magnetic scattering (XRMS), X-ray absorption near-edge structure (XANES) and X-ray magnetic circular dichroism (XMCD) techniques. The XRMS measurements reveal that the GdCo2_2Zn20_{20} compound has a commensurate antiferromagnetic spin structure with a magnetic propagation vector τ\vec{\tau} = (12,12,12)(\frac{1}{2},\frac{1}{2},\frac{1}{2}) below the N\'eel temperature (TNT_N \sim 5.7 K). Only the Gd ions carry a magnetic moment forming an antiferromagnetic structure with magnetic representation Γ6\Gamma_6. For the ferromagnetic GdFe2_2Zn20_{20} compound, an extensive investigation was performed at low temperature and under magnetic field using XANES and XMCD techniques. A strong XMCD signal of about 12.5 %\% and 9.7 %\% is observed below the Curie temperature (TCT_C \sim 85 K) at the Gd-L2L_2 and L3L_3 edges, respectively. In addition, a small magnetic signal of about 0.06 %\% of the jump is recorded at the Zn KK-edge suggesting that the Zn 4pp states are spin polarized by the Gd 5dd extended orbitals

    Quantitative comparison of the magnetic proximity effect in Pt detected by XRMR and XMCD

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    X-ray resonant magnetic reflectivity (XRMR) allows for the simultaneous measurement of structural, optical and magnetooptic properties and depth profiles of a variety of thin film samples. However, a same-beamtime same-sample systematic quantitative comparison of the magnetic properties observed with XRMR and x-ray magnetic circular dichroism (XMCD) is still pending. Here, the XRMR results (Pt L3_{3} absorption edge) for the magnetic proximity effect in Pt deposited on the two different ferromagnetic materials Fe and Co33_{33}Fe67_{67} are compared with quantitatively analyzed XMCD results. The obtained results are in very good quantitative agreement between the absorption-based (XMCD) and reflectivity-based (XRMR) techniques taking into account an ab initio calculated magnetooptic conversion factor for the XRMR analysis. Thus, it is shown that XRMR provides quantitative reliable spin depth profiles important for spintronic and spin caloritronic transport phenomena at this type of magnetic interfaces.Comment: This article may be downloaded for personal use only. Any other use requires prior permission of the author and AIP Publishing. This article appeared in Appl. Phys. Lett. 118, 012407 (2021) and may be found at https://aip.scitation.org/doi/abs/10.1063/5.003258

    Pressure effects on the structural and superconducting transitions in La₃Co₄Sn₁₃

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    La3Co4Sn13 is a superconducting material with transition temperature at Tc = 2.70 K, which presents a superlattice structural transition at T ∗ ≃ 150 K, a common feature for this class of compounds. However, for this material, it is not clear that at T ∗ the lattice distortions arise from a charge density wave (CDW) or from a distinct microscopic origin. Interestingly, it has been suggested in isostructural non-magnetic intermetallic compounds that T ∗ can be suppressed to zero temperature, by combining chemical and external pressure, and a quantum critical point is argued to be observed near these critical doping/pressure. Our study shows that application of pressure on single-crystalline La3Co4Sn13 enhances Tc and decreases T ∗ . We observe thermal hysteresis loops for cooling/heating cycles around T ∗ for P & 0.6 GPa, in electrical resistivity measurements, which are not seen in x-ray diffraction data. The hysteresis in electrical measurements may be due to the pinning of the CDW phase to impurities/defects, while the superlattice structural transition maintains its ambient pressure second-order transition nature under pressure. From our experiments we estimate that T ∗ vanishes at around 5.5 GPa, though no quantum critical behavior is observed up to 2.53 GPa

    Chlamydia pneumoniae and Mycoplasma pneumoniae in children with cystic fibrosis: impact on bacterial respiratory microbiota diversity.

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    The contribution of intracellular and fastidious bacteria in Cystic fibrosis (CF) pulmonary exacerbations, and progressive lung function decline remains unknown. This project aimed to explore their impact on bacterial microbiota diversity over time in CF children. Sixty-one children enrolled in the MUCOVIB multicentre prospective cohort provided 746 samples, mostly nasopharyngeal swabs, throat swabs and sputa which were analysed using culture, specific real-time qPCRs and 16S rRNA amplicon metagenomics. Chlamydia pneumoniae (n = 3) and Mycoplasma pneumoniae (n = 1) were prospectively documented in 6.6% of CF children. Microbiota alpha-diversity in children with a documented C. pneumoniae was highly variable, similarly to children infected with Staphylococcus aureus or Pseudomonas aeruginosa. The transition from routine follow-up visits to pulmonary exacerbation (n = 17) yielded variable changes in diversity indexes with some extreme loss of diversity. The high rate of C. pneumoniae detection supports the need for regular screenings in CF patients. A minor impact of C. pneumoniae on the microbial community structure was documented. Although detected in a single patient, M. pneumoniae should also be considered as a possible aetiology of lung infection in CF subjects

    Mecanização da colheita do feijoeiro: uso de recolhedoras trilhadoras.

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    Neste documento são abordados os aspectos relacionados à umidade dos grãos para o arranquio e trilhamento; componente, funcionamento e operação de uma recolhedora trilhadora de feijão; tamanho das leiras; cuidados na instalação, condução e colheita da lavoura e monitoramento das perdas de grãos na operação da máquina.bitstream/CNPAF/17338/1/circ_37.pd
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