Role of hybrid tool pin profile on enhancing welding speed and mechanical properties of AA2219-T6 friction stir welds

The friction stir welds of thick precipitation-hardenable aluminum alloys suffer from reduced joint strength due to dissolution/coarsening of the strengthening precipitates. The article portray hybrid pin profiled tool that enables sound welds at speeds 7-times faster than a conventional tool (a conical threaded tool), without pin breakage. The conical threaded and triangular cross-section in the upper and lower pin half-lengths of the hybrid tool facilitate material flow in a downward direction and shear deformation at a faster rate, respectively. The paper brings out the process mechanism responsible for the enhanced welding speed and mechanical properties obtainable with the hybrid tool through a case of 13-mm thick aluminum alloy AA2219-T6. The hybrid tool facilitates a 28% improvement in weld strength by reducing TMAZ softening, as evidenced by the microhardness and mechanical properties and supported by microstructural investigation and fractography

Welding of nickel free high nitrogen stainless steel: Microstructure and mechanical properties

AbstractHigh nitrogen stainless steel (HNS) is a nickel free austenitic stainless steel that is used as a structural component in defence applications for manufacturing battle tanks as a replacement of the existing armour grade steel owing to its low cost, excellent mechanical properties and better corrosion resistance. Conventional fusion welding causes problems like nitrogen desorption, solidification cracking in weld zone, liquation cracking in heat affected zone, nitrogen induced porosity and poor mechanical properties. The above problems can be overcome by proper selection and procedure of joining process. In the present work, an attempt has been made to correlate the microstructural changes with mechanical properties of fusion and solid state welds of high nitrogen steel. Shielded metal arc welding (SMAW), gas tungsten arc welding (GTAW), electron beam welding (EBW) and friction stir welding (FSW) processes were used in the present work. Optical microscopy, scanning electron microscopy and electron backscatter diffraction were used to characterize microstructural changes. Hardness, tensile and bend tests were performed to evaluate the mechanical properties of welds. The results of the present investigation established that fully austenitic dendritic structure was found in welds of SMAW. Reverted austenite pools in the martensite matrix in weld zone and unmixed zones near the fusion boundary were observed in GTA welds. Discontinuous ferrite network in austenite matrix was observed in electron beam welds. Fine recrystallized austenite grain structure was observed in the nugget zone of friction stir welds. Improved mechanical properties are obtained in friction stir welds when compared to fusion welds. This is attributed to the refined microstructure consisting of equiaxed and homogenous austenite grains

Influence of process parameters on physical dimensions of AA6063 aluminium alloy coating on mild steel in friction surfacing

AbstractAn attempt is made in the present study to obtain the relationships among process parameters and physical dimensions of AA6063 aluminium alloy coating on IS2062 mild steel obtained through friction surfacing and their impact on strength and ductility of the coating. Factorial experimental design technique was used to investigate and select the parameter combination to achieve a coating with adequate strength and ductility. Spindle speed, axial force and table traverse speed were observed to be the most significant factors on physical dimensions. It was observed that the thickness of the coating decreased as the coating width increased. In addition, the width and thickness of the coatings are higher at low and high torques. At intermediate torque values, when the force is high, the width of the coating is high, and its thickness is thin; and when the force is low, the width and thickness are low. The interaction effect between axial force (F) – table traverse speed (Vx) and spindle speed (N) – table traverse speed (Vx) produced an increasing effect on coating width and thickness, but other interactions exhibited decreasing influence. It has also been observed that sound coatings could be obtained in a narrow set of parameter range as the substrate-coating materials are metallurgically incompatible and have a propensity to form brittle intermetallics

Ballistic behavior of boron carbide reinforced AA7075 aluminium alloy using friction stir processing – An experimental study and analytical approach

AbstractHigh strength-to-weight ratio of non-ferrous alloys, such as aluminium, magnesium and titanium alloys, are considered to be possible replacement of widely accepted steels in transportation and automobile sectors. Among these alloys, magnesium is self explosive and titanium is costlier, and aluminium is most likely to replace steels. Application of aluminium or its alloys is also thought of as an appropriate replacement in defence field, especially to enhance the easiness in mobility of combat vehicles while maintaining the same standard as that of conventional armour grade steels. Hence most of the investigations have been confined to aluminium or its alloys as base material and open an era of developing the newer composite materials to address the major limitation, i.e. tribological properties. The surface composites can be fabricated by incorporating the ceramic carbides like silicon carbide, carbides of transition metals and oxides of aluminium using surface modification techniques, such as high energy laser melt treatment, high energy electron beam irradiation and thermal spray process which are based on fusion route. These techniques yield the fusion related problems, such as interfacial reaction, pin holes, shrinkage cavities or voids and other casting related defects, and pave the way to need of an efficient technique which must be based on solid state. Recently developed friction stir processing technique was used in the present investigation for surface modification of AA7075 aluminum alloy, which is an alternative to steels. In the present investigation, 160 μm sized boron carbide powder was procured and was reduced to 60 μm and 30 μm using high energy ball mill. Subsequently these powders were used to fabricate the surface composites using friction stir processing.Ballistic performance testing as per the military standard (JIS.0108.01) was carried out. In the present work, an analytical method of predicting the ballistic behavior of surface composites was developed. This method was based on energy balance, i.e., the initial energy of impact is same as that of energy absorbed by multi layers. An attempt also has been made to validate the analytical results with the experimental findings. Variation between the analytical and experimental results may be accounted due to the assumptions considering such as isotropic behavior of target and shearing area of contact as cylindrical instead of conical interface As the analytical model yields the ballistic performance in the closer proximity of experimentally obtained, it can be considered to be an approximation to evaluate the ballistic performance of targets

Role of Threaded Tool Pin Profile and Rotational Speed on Generation of Defect Free Friction Stir AA 2014 Aluminium Alloy Welds

Influence of threads on tool pin and rotational speeds on defect occurrence in friction stir welding (FSW) of aluminum alloy AA 2014 T6 plates has been studied. The effect of FSW forces on the evolution of mechanistic defects, caused in turn through a variation in heat generation during the process has also been examined. In case of conical tool pin, relatively lower rotational speeds resulted in unbounded zones and micro defects while high speeds caused excessive flash, thereby resulting in surface defects and voids inside the weld. The FSW joints were defect-free at moderate speeds, hinting an optimum heat generation and flow. Reaction forces on the tool pin, in the welding direction, were correlated with the defect formation. Tools equipped with a threaded conical pin profile resulted in sound welds, irrespective of the tool rotational speeds in the entire range of 400 rpm - 2400 rpm. The threaded conical pin, with a relatively larger frictional area, may be contributing to higher levels of heat generation compared to a plain conical pin. Further, positive displacement of the hot plasticised material by the threads will carry away excess heat from the advancing-to-the-retracting side and simultaneously downwards, thus confining all heat within the weld zone.

Process parameters-weld bead geometry interactions and their influence on mechanical properties: A case of dissimilar aluminium alloy electron beam welds

Prediction of weld bead geometry is always an interesting and challenging research topic as it involves understanding of complex multi input and multi output system. The weld bead geometry has a profound impact on the load bearing capability of a weld joint, which in-turn decides the performance in real time service conditions. The present study introduces a novel approach of detecting a relationship between weld bead geometry and mechanical properties (e.g. tensile load) for the purpose of catering the best the process could offer. The significance of the proposed approach is demonstrated by a case of dissimilar aluminium alloy (AA2219 and AA5083) electron beam welds. A mathematical model of tensile braking load as a function of geometrical attributes of weld bead geometry is presented. The results of investigation suggests the effective thickness of weld - a geometric parameter of weld bead has the most significant influence on tensile breaking load of dissimilar weld joint. The observations on bead geometry and the mechanical properties (microhardness, ultimate tensile load and face bend angle) are correlated with detailed metallurgical analysis. The fusion zone of dissimilar electron beam weld has finer grain size with a moderate evaporation and segregation of alloying elements magnesium and copper respectively. The mechanical properties of weld joint are controlled by optimum bead geometry and HAZ softening in weaker AA5083 Al alloy

Design and Enantiopure Synthesis of( R

A new synthetic method for the preparation of high enantiopure (R)-2-((2-oxooxazolidin-5-yl)methyl)isoindoline-1,3-dione has been developed. The enantiopurity of the obtained (R)-2-((2-oxooxazolidin-5-yl)methyl) isoindoline-1,3-dione is established using chiral high performance liquid chromatography (HPLC) i.e. enantiomeric excess (ee) as 100%. One among the two proposed approaches, is succeeded in preparing enantiopure targeted chiral building block using (R)-2-(chloromethyl)oxirane ((R)-epichlorohydrin) as precursor. This heterocyclic 2-oxazolidinone moiety could be useful to prepare a series of antibacterial agents containing 2-oxazolidinone

Enantioselective Synthesis of Antiepileptic Drug: (-)-Levetiracetam-Synthetic Applications of the Versatile New Chiral N-Sul�nimine

We report an asymmetric synthesis of (-)-Levetiracetam (1) in six steps starting from versatile new chiral N-sul�nimine (3). e key step, stereoselective 1,2-addition of ethylmagnesium bromide (EtMgBr) to chiral N-sul�nimine derived from (R)-glyceraldehyde acetonide and (S)-t-BSA, gave the corresponding sulfonamide (2) in high diastereoselectivity. Simultaneous deprotection and deacetylation followed by NaIO 4 cleavage and reduction gave -amino alcohol (6). Subsequent reactions yielded the targeted compound levetiracetam (1)