Charring effects on stable carbon and nitrogen isotope values on C4 plants: Inferences for archaeological investigations

Experimental studies demonstrated that charring affects stable isotope values of plant remains. Therefore, it is necessary to consider the impact of charring to reliably interpret δ13C and δ15N values in archaeobotanical remains before using this approach to reconstruct past water management, paleoclimatic changes, and infer paleodietary patterns. Research so far has focused mostly on C3 plants while the charring effect on C4 plants is less understood. This study explored the effects of charring on δ13C, δ15N, %C, %N, and C:N in grains of two C4 species, Sorghum bicolor (L.) Moench (NADP-ME) and Cenchrus americanus (L.) Morrone (heterotypic synonym Pennisetum glaucum (L.) R.Br.) (NAD-ME), grown under the same controlled environmental conditions (watering, light, atmospheric humidity). Sorghum and pearl millet grains were charred from 1 to 3 h at 200–300 °C. Comparing first the uncharred grains, the results show that sorghum has lower δ15N and higher δ13C values than pearl millet. This evidence is also recorded in the charred grains. The charring experiments indicate that the temperature to which the grains are exposed has a higher impact than time on the preservation, mass loss, %C, %N, C:N, and δ13C and δ15N values. Every 50 °C of increase resulted in significant increases of δ15N (+0.37‰) and of δ13C (+0.06‰) values. Increasing the duration of charring to 3 h resulted in significant changes of δ15N (+0.17‰) and no significant changes for δ13C (−0.04‰) values. The average charring effects estimated in our experiment is 0.27‰ (95% CI between −0.02 and 0.56) for δ15N and −0.18‰ (95% CI between −0.30 and −0.06‰) for δ13C. Considering the average values, our data show that pearl millet is more affected by charring than sorghum; however, according to the standard deviations, sorghum shows a greater variability charring effect than pearl millet. This study provides new information to correctly assessing the isotopic values obtained from ancient C4 crops, providing a charring offset specific for C4 plants. Furthermore, it suggests that NAD-ME and NADP-ME species present isotopic differences under the same growing conditions and this must be taken into account in analytical works on ancient C4 crops.This work was funded by the ERC Staring Grant RAINDROPS (G.A. n 759800) under the Horizon 2020 program of the European Commission. CASEs is a Quality Research Group funded by the Government of Catalonia (SGR00950-2021)

How many grains are needed for quantifying catchment erosion from tracer thermochronology?

Detrital tracer thermochronology utilizes the relationship between bedrock thermochronometric age–elevation profiles and a distribution of detrital grain ages collected from riverine, glacial, or other sediment to study spatial variations in the distribution of catchment erosion. If bedrock ages increase linearly with elevation, spatially uniform erosion is expected to yield a detrital age distribution that mimics the shape of a catchment's hypsometric curve. Alternatively, a mismatch between detrital and hypsometric distributions may indicate spatial variability of sediment production within the source area. For studies seeking to identify the pattern of sediment production, detrital samples rarely exceed 100 grains due to the time and costs related to individual measurements. With sample sizes of this order, detecting the dissimilarity between two detrital age distributions produced by different catchment erosion scenarios can be difficult at a high statistical confidence level. However, there are no established software tools to quantify the uncertainty inherent to detrital tracer thermochronology as a function of sample size and spatial pattern of sediment production. As a result, practitioners are often left wondering “how many grains is enough to detect a certain signal?”. Here, we investigate how sample size affects the uncertainty of detrital age distributions and how such uncertainty affects the ability to infer a pattern of sediment production of the upstream area. We do this using the Kolmogorov–Smirnov statistic as a metric of dissimilarity among distributions. From this, we perform statistical hypothesis testing by means of Monte Carlo sampling. These techniques are implemented in a new tool (ESD_thermotrace) to (i) consistently report the confidence level allowed by the sample size as a function of application-specific variables and given a set of user-defined hypothetical erosion scenarios, (ii) analyze the statistical power to discern each scenario from the uniform erosion hypothesis, and (iii) identify the erosion scenario that is least dissimilar to the observed detrital sample (if available). ESD_thermotrace is made available as a new open-source Python-based script alongside the test data. Testing between different hypothesized erosion scenarios with this tool provides thermochronologists with the minimum sample size (i.e., number of bedrock and detrital grain ages) required to answer their specific scientific question at their desired level of statistical confidence

Inferências sobre Vegetação e Clima no Holoceno a partir de Fitólitos e Pólen da Lagoa do Macuco, Litoral Norte do Estado do Espírito Santo (Brasil)

[EN] An interproxy approach focused on phytoliths and pollen, including radiocarbon dating and sediment particle-size analyses, has been carried out at Lagoa do Macuco, Linhares municipality, Espírito Santo State, Brazil. Three pollen zones were identified: the first one (MAC-C I) indicates the presence of mangrove vegetation between 7700 cal yr BP and 4396 cal yr BP; the second one a displacement of the vegetation from the lower areas to the more elevated margins of the valley (MAC-C II, from between 4396 to 1287 cal. yr BP) and third one (MAC-C III), representing the period of the current lake evolution, between 1287 cal. yr BP and the present day. The displacement of the mangrove seems to be connected to the landward migration of the palaeo-estuary and the flooding of the lower parts of the valley, reflecting the relative sea-level highstand, which occurred after 7000 cal yr BP. The phytolith analysis indicated four main zone. The phytolith zone I (7700-7100 cal yr BP) did not show the presence of phytoliths. The phytoliths zone II (7100-3400 cal yr BP) indicates the presence of an open vegetation predominantly of grasses while phytolith zone III (3400-400 cal yr BP) shows a phase with more forested vegetation. Finally, the phytolith zone IV (400 cal yr BP to modern) has a decrease in tree cover and the setting of vegetation with a strong grasses component. Phytoliths indices indicate trends of humidity and temperature at a more local scale, allowing understanding the environmental conditions during the formation of the current lake.[PT] Uma abordagem interproxy focada na análise de fitólitos e de grãos de pólen, também incluindo datação 14C e análise granulométrica de sedimentos, foi aplicada ao estudo da Lagoa do Macuco, em Linhares no Estado do Espírito Santo. Foram identificadas três zonas polínicas definidas com base nas mudanças do registro polínico, a primeira (MAC-C I) indicando a presença de uma vegetação de mangue entre 7700 anos cal AP e 4396 anos cal AP, a segunda (MAC-C II) que representa o deslocamento da vegetação das áreas mais baixas para as partes marginais mais elevadas do vale (4396 anos cal AP - 1287 anos cal AP) e a terceira (MAC-C III) que representa o período da instalação do atual lago, entre 1287 anos cal AP e os dias atuais. O deslocamento do mangue parece estar conectado a migração em direção ao paleo-estuário e o alagamento das partes baixas do vale, refletindo a elevação do nível relativo do mar depois de 7000 cal anos AP. A análise fitolítica indicou quatro zonas principais. A zona fitolítica I (7700-7100 anos cal AP), não apresentou fitólitos. A zona fitolítica II (7100-3400 anos cal AP) indica a presença de uma vegetação predominantemente composta por gramíneas, enquanto a zona fitolítica III (3400-400 anos cal AP) mostrou uma fase com uma vegetação mais florestada. Finalmente, a zona fitolítica IV, (400 anos cal AP até os dias atuais) apresentou decréscimo da cobertura arbórea e uma estrutura de vegetação com forte presença de gramíneas em sua composição. Os índices fitolíticos indicaram tendência de umidade e temperatura em escala local permitindo a compreensão das condições ambientais durante a formação do lago atual.The authors express their gratitude to Vale and Sooretama Nature Reserves (Linhares, ES, Brasil) for the field support. This work received financial support by the São Paulo Foundation for Research (FAPESP), grant 2011/00995-7, and CNPq (Universal), grant 470210/2012-5.Peer Reviewe

Automated detection of archaeological mounds using machine-learning classification of multisensor and multitemporal satellite data.

This paper presents an innovative multisensor, multitemporal machine-learning approach using remote sensing big data for the detection of archaeological mounds in Cholistan (Pakistan). The Cholistan Desert presents one of the largest concentrations of Indus Civilization sites (from ca 3300 to 1500 BC). Cholistan has figured prominently in theories about changes in water availability, the rise and decline of the Indus Civilization, and the transformation of fertile monsoonal alluvial plains into an extremely arid margin. This paper implements a multisensor, multitemporal machine-learning approach for the remote detection of archaeological mounds. A classifier algorithm that employs a large-scale collection of synthetic-aperture radar and multispectral images has been implemented in Google Earth Engine, resulting in an accurate probability map for mound-like signatures across an area that covers ca 36,000 km2 The results show that the area presents many more archaeological mounds than previously recorded, extending south and east into the desert, which has major implications for understanding the archaeological significance of the region. The detection of small (30 ha) suggests that there were continuous shifts in settlement location. These shifts are likely to reflect responses to a dynamic and changing hydrological network and the influence of the progressive northward advance of the desert in a long-term process that culminated in the abandonment of much of the settled area during the Late Harappan period.ER

The unexpected land use: rain-fed agriculture in drylands

Although excluded from most maps of current and past land use, dryland rain-fed (non-irrigated) agriculture has been and is pivotal to enhance resilience of human communities, and understand land-atmosphere interactions and regional climate in many parts of the world

High and medium resolution satellite imagery to evaluate late holocene human-environment interactions in arid lands: A case study from the Central Sahara.

We present preliminary results of an Earth observation approach for the study of past human occupation and landscape reconstruction in the Central Sahara. This region includes a variety of geomorphological features such as palaeo-oases, dried river beds, alluvial fans and upland plateaux whose geomorphological characteristics, in combination with climate changes, have influenced patterns of human dispersal and sociocultural activities during the late Holocene. In this paper, we discuss the use of medium- and high-resolution remotely sensed data for the mapping of anthropogenic features and paleo- and contemporary hydrology and vegetation. In the absence of field inspection in this inaccessible region, we use different remote sensing methods to first identify and classify archaeological features, and then explore the geomorphological factors that might have influenced their spatial distribution.EM201

Glacial catchment erosion from detrital zircon (U‐Th)/he thermochronology: Patagonian Andes

Alpine glacial erosion exerts a first-order control on mountain topography and sediment production, but its mechanisms are poorly understood. Observational data capable of testing glacial erosion and transport laws in glacial models are mostly lacking. New insights, however, can be gained from detrital tracer thermochronology. Detrital tracer thermochronology works on the premise that thermochronometer bedrock ages vary systematically with elevation, and that detrital downstream samples can be used to infer the source elevation sectors of sediments. We analyze six new detrital samples of different grain sizes (sand and pebbles) from glacial deposits and the modern river channel integrated with data from 18 previously analyzed bedrock samples from an elevation transect in the Leones Valley, Northern Patagonian Icefield, Chile (46.7°S). We present 622 new detrital zircon (U-Th)/He (ZHe) single-grain analyses and 22 new bedrock ZHe analyses for two of the bedrock samples to determine age reproducibility. Results suggest that glacial erosion was focused at and below the Last Glacial Maximum and neoglacial equilibrium line altitudes, supporting previous modeling studies. Furthermore, grain age distributions from different grain sizes (sand, pebbles) might indicate differences in erosion mechanisms, including mass movements at steep glacial valley walls. Finally, our results highlight complications and opportunities in assessing glacigenic environments, such as dynamics of sediment production, transport, transient storage, and final deposition, that arise from settings with large glacio-fluvial catchments

Making city in the "Non-City": the integration of irregular settlements in Andalusia. A case study

The problems associated with numerous irregular buildings existing in Andalucia today, demands a new approach. In order to deepen the definition of strategies of urbano-territorial integration of these settlements, we present a case study in which, at the end of its implementation in agent-based simulation models, we summarize the ODD Protocol which will form the basis of the simulation, indicating the determining factors to consider for an effective and participatory planning, that minimize the progressive estrangement between the normative framework and the reality that is tried to order.

High and Medium Resolution Satellite Imagery to Evaluate Late Holocene Human–Environment Interactions in Arid Lands: A Case Study from the Central Sahara

We present preliminary results of an Earth observation approach for the study of past human occupation and landscape reconstruction in the Central Sahara. This region includes a variety of geomorphological features such as palaeo-oases, dried river beds, alluvial fans and upland plateaux whose geomorphological characteristics, in combination with climate changes, have influenced patterns of human dispersal and sociocultural activities during the late Holocene. In this paper, we discuss the use of medium- and high-resolution remotely sensed data for the mapping of anthropogenic features and paleo- and contemporary hydrology and vegetation. In the absence of field inspection in this inaccessible region, we use different remote sensing methods to first identify and classify archaeological features, and then explore the geomorphological factors that might have influenced their spatial distribution.Satellite imagery used in this study was generously provided by the DigitalGlobe Foundation, thanks to a grant entrusted to SB. This study was funded by the Marie S. Curie IEF the Europen Commission, grant No. 622344 PastoralMod, entrusted to SB, by the ‘PaisArque—Paisajes Arqueológicos Inaccesibles y en Peligro: Observación Terrestre y Tecnologías 3D para la Protección y Preservación del Patrimonio Cultural’ of the Fundación BBVA, and by the ‘SimulPast project’, CONSOLIDER-INGENIO 2010 from the MINECO (CSD2010-00034)

Development and testing scenarios for implementing land use and land cover changes during the Holocene in Earth system model experiments

Anthropogenic changes in land use and land cover (LULC) during the pre-industrial Holocene could have affected regional and global climate. Current LULC scenarios are based on relatively simple assumptions and highly uncertain estimates of population changes through time. Archaeological and palaeoenvironmental reconstructions have the potential to refine these assumptions and estimates. The Past Global Changes (PAGES) LandCover6k initiative is working towards improved reconstructions of LULC globally. In this paper, we document the types of archaeological data that are being collated and how they will be used to improve LULC reconstructions. Given the large methodological uncertainties involved, we propose methods to evaluate the revised scenarios by using independent pollen-based reconstructions of land cover and of climate. A further test involves carbon-cycle simulations to determine whether the LULC reconstructions are consistent with constraints provided by ice-core records of CO2 evolution and modern-day LULC. Finally, we outline a protocol for using the improved LULC reconstructions in palaeoclimate simulations within the framework of the Palaeoclimate Modelling Intercomparison Project in order to quantify the magnitude of anthropogenic impacts on climate through time and ultimately to improve the realism of Holocene climate simulations