Frictional experiments of dolerite at intermediate slip rates with controlled temperature: Rate weakening or temperature weakening?

A rotary shear apparatus has been newly set up in Chiba University which can control the temperature near a sliding surface, T_meas, up to 1000°C independently from slip rate, V. Frictional experiments at 0.010 m/s, 1 MPa normal stress, and variable T_meas for dolerite have revealed a remarkable effect of temperature on the friction coefficient, f. With increasing T_meas, f starts from 0.7 to 0.8 at room temperature (RT), decreases down to 0.5–0.6 at 400°C, increases until 800°C, and then decreases again. We have also conducted XRD analyses of the wear materials (mainly submicron particles) and investigated microstructures of the sliding surfaces developed at different temperatures T_meas, and we found that there is a negative correlation between f and the amount of amorphous material except at RT and 1000°C. The generation of the amorphous phase probably causes the weakening. There is no amorphous phase recognized for a sample at 1000°C which is an aggregate of rounded crystals. EBSD analyses show that the material on the sliding surface at 1000°C contains randomly oriented hematite grains, which together with the observed microstructural features suggests that granular flow was taking place. We have also demonstrated that f depends not only on the instantaneous value of temperature, but also on its history. By comparing with conventional rotary shear friction experiment for the same dolerite without temperature control, we conclude that strong “rate weakening” as recently observed in high-velocity frictional experiments without an active control of the temperature has a significant amount of contribution from the temperature effect