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Investigation of the microstructure of the fine-grained YPO:Gd ceramics with xenotime structure after Xe irradiation
The paper reports on the preparation of xenotime-structured ceramics by the
Spark Plasma Sintering (SPS) method. Phosphates YGdPO
(YPO:Gd) were obtained by the sol-gel method. The synthesized nanopowders
are collected in large agglomerates 10-50 mkm in size. Ceramics has a
fine-grained microstructure and a high relative density (98.67%). The total
time of the SPS process was approximately 18 min. High-density sintered
ceramics YPO:Gd with a xenotime structure were irradiated with Xe
ions (E = 167 MeV) to fluences of - cm.
Complete amorphization at maximum fluence was not achieved. As the fluence
increases, an insignificant increase in the depth of the amorphous layer is
observed. According to the results of grazing incidence XRD (GIXRD), with an
increase in fluence from - cm, an
increase in the volume fraction of the amorphous structure from 20 to 70% is
observed. The intensity of XRD peak 200 YPO:Gd after recovery annealing
(700C, 18 h) reached a value of ~80% of the initial intensity I0.Comment: 16 pages, 10 figure