Deuteron spin-lattice relaxation times in undercooled aqueous potassium- and cesium halide solutions

Abstract Aqueous emulsions of potassium-and cesium halides in cycloalkane mixtures can be undercooled at a pressure of 225 MPa to temperatures around 170K. In these emulsions deuterium spin-lattice relaxation times T1 have been determined as function of salt concentration, temperature and pressure at magnetic fields of 2.4 Tesla and 7.0 Tesla. The frequency and temperature dependence of the relaxation time curves is described quantitatively within a motional model which is consistent with known local structural features in these solutions. Model parameters deduced are compared with those obtained in related studies of the other alkali-halides, and conclusions are drawn regarding the influence of structure and composition on molecular motions. </jats:p

ROSAT monitoring of persistent giant and rapid variability in the narrow-line Seyfert 1 galaxy IRAS 13224-3809

We report evidence for persistent giant and rapid X-ray variability in the radio-quiet, ultrasoft, strong Fe II, narrow-line Seyfert 1 galaxy IRAS 13224-3809. Within a 30 day ROSAT High Resolution Imager (HRI) monitoring observation at least five giant amplitude count rate variations are visible, with the maximum observed amplitude of variability being about a factor of 60. We detect a rise by a factor of about 57 in just two days. IRAS 13224-3809 appears to be the most X-ray variable Seyfert known, and its variability is probably nonlinear. We carefully check the identification of the highly variable X-ray source with the distant galaxy, and it appears to be secure. We examine possible explanations for the giant variability. Unusually strong relativistic effects and partial covering by occulting structures on an accretion disc can provide plausible explanations of the X-ray data, and we explore these two scenarios. Relativistic boosting effects may be relevant to understanding the strong X-ray variability of some steep spectrum Seyferts more generally.Comment: 14 pages, submitted to MNRA

Emission Optics of the Steigerwald Type Electron Gun

The emission optics of a Steigerwald type electron gun is re-examined. The virtual and real points of divergence, divergence angles and beam-widths of the electron beams at different telefocusing strength are measured in detail for first time . Two different Wehnelt cylinders are used to establish a contrasting viewpoint. The original `focusing' curves measured by Braucks are reconstructed and will be explained only through a `new' interpretation which is different from the conventional views. While the image of the emitting surface in front of the filament is indeed telefocused beyond the anode, the envelope of the beam does not `focus' as expected. A new model for the emission mechanism is established based on our results.Comment: 14 pages, 10 figure

Non-destructive imaging of an individual protein

The mode of action of proteins is to a large extent given by their ability to adopt different conformations. This is why imaging single biomolecules at atomic resolution is one of the ultimate goals of biophysics and structural biology. The existing protein database has emerged from X-ray crystallography, NMR or cryo-TEM investigations. However, these tools all require averaging over a large number of proteins and thus over different conformations. This of course results in the loss of structural information. Likewise it has been shown that even the emergent X-FEL technique will not get away without averaging over a large quantity of molecules. Here we report the first recordings of a protein at sub-nanometer resolution obtained from one individual ferritin by means of low-energy electron holography. One single protein could be imaged for an extended period of time without any sign of radiation damage. Since ferritin exhibits an iron core, the holographic reconstructions could also be cross-validated against TEM images of the very same molecule by imaging the iron cluster inside the molecule while the protein shell is decomposed

The Morphology of Lava Flows in Planetary Environments: Predictions From Analog Experiments

The rates of surface cooling and lateral spreading are evaluated for lava flows on the surface of Earth, Venus, Mars, the Moon, and 10. Differences between the flow morphologies expected in these environments are then predicted under the assumption that the results of recent laboratory simulations oflavas using wax extruded beneath cold water (Fink and Griffiths, 1990) can be carried over. These experiments involved the spreading of viscous liquid under gravity in the presence of a solidifying surface crust and revealed a set of four distinct surface morphologies. Transitions from one morphology to the next occurred in a well-defined sequence when the relative rates of surface solidification and lateral spreading were varied. In comparison with subaerial flows on Earth, the surface of lavas solidifies faster on Venus, where the dense atmosphere provides additional convective heat transfer. Lateral flow oflava is much slower under the smaller gravity of the Moon. Hence, for a given extrusion rate and viscosity, solid crust is predicted to form closer to the vent on both the Moon and Venus than on Earth. Equivalently, faster extrusion rates than those on Earth are required on the Moon, 10, and Venus in order to produce a given surface morphology. A comparison of observed structure, flow rates, and estimated viscosities for some well-documented terrestrial lava flows shows reasonable agreement with the predictions of the model. Extrapolation to extraterrestrial lavas is then illustrated by constraining the effusion rate for a Martian lava flow whose composition is assumed. Spectral information on the chemical composition of Martian flows to be sought by the thermal emission spectrometer on the Mars Observer mission, in conjunction with detailed morphologic observations from the Mars Observer camera, could allow much more accurate estimates of effusion rates for Martian lavas

Diffuse LEED intensities of disordered crystal surfaces : III. LEED investigation of the disordered (110) surface of gold

The LEED pattern of clean (101) surfaces of Au show a characteristic (1 × 2) superstructure. The diffuseness of reflections in the reciprocal [010] direction is caused by one-dimensional disorder of chains, strictly ordered into spatial [10 ] direction. There is a transition from this disordered superstructure to the normal (1 × 1) structure at 420 + 15°C. The angular profiles of the and (01) beam are measured at various temperatures and with constant energy and angles of incidence of the primary beam. The beam profiles are deconvoluted approximately with the instrument response function