126 research outputs found
X-ray standing wave and reflectometric characterization of multilayer structures
Microstructural characterization of synthetic periodic multilayers by x-ray
standing waves have been presented. It has been shown that the analysis of
multilayers by combined x-ray reflectometry (XRR) and x-ray standing wave (XSW)
techniques can overcome the deficiencies of the individual techniques in
microstructural analysis. While interface roughnesses are more accurately
determined by the XRR technique, layer composition is more accurately
determined by the XSW technique where an element is directly identified by its
characteristic emission. These aspects have been explained with an example of a
20 period Pt/C multilayer. The composition of the C-layers due to Pt
dissolution in the C-layers, PtC, has been determined by the XSW
technique. In the XSW analysis when the whole amount of Pt present in the
C-layers is assumed to be within the broadened interface, it l eads to larger
interface roughness values, inconsistent with those determined by the XRR
technique. Constraining the interface roughness values to those determined by
the XRR technique, requires an additional amount of dissolved Pt in the
C-layers to expl ain the Pt fluorescence yield excited by the standing wave
field. This analysis provides the average composition PtC of the
C-layers .Comment: 12 pages RevTex, 10 eps figures embedde
Shape Transition in the Epitaxial Growth of Gold Silicide in Au Thin Films on Si(111)
Growth of epitaxial gold silicide islands on bromine-passivated Si(111)
substrates has been studied by optical and electron microscopy, electron probe
micro analysis and helium ion backscattering. The islands grow in the shape of
equilateral triangles up to a critical size beyond which the symmetry of the
structure is broken, resulting in a shape transition from triangle to
trapezoid. The island edges are aligned along directions. We have
observed elongated islands with aspect ratios as large as 8:1. These islands,
instead of growing along three equivalent [110] directions on the Si(111)
substrate, grow only along one preferential direction. This has been attributed
to the vicinality of the substrate surface.Comment: revtex version 3.0, 11 pages 4 figures available on request from
[email protected] - IP/BBSR/93-6
Theory and Applications of X-ray Standing Waves in Real Crystals
Theoretical aspects of x-ray standing wave method for investigation of the
real structure of crystals are considered in this review paper. Starting from
the general approach of the secondary radiation yield from deformed crystals
this theory is applied to different concreat cases. Various models of deformed
crystals like: bicrystal model, multilayer model, crystals with extended
deformation field are considered in detailes. Peculiarities of x-ray standing
wave behavior in different scattering geometries (Bragg, Laue) are analysed in
detailes. New possibilities to solve the phase problem with x-ray standing wave
method are discussed in the review. General theoretical approaches are
illustrated with a big number of experimental results.Comment: 101 pages, 43 figures, 3 table
Production and characterisation of a recombinant scFv reactive with human gastrointestinal carcinomas
SC142-reactive antigen are highly glycosylated glycoproteins expressed on tissues of gastric and colon cancers but not on normal tissues. Murine SC142 antibody specific for the SC142-reactive antigen has been produced by immunisation with SNU16 stomach cancer cells. However, SC142 antibody has several potential problems such as high immunogenicity and poor tumour penetration owing to their large size. To improve tumour penetration potential in vivo, recombinant single-chain fragments have been produced using the original hybridoma cells as a source of variable heavy- and variable light-chain-encoding antibody genes. The use of the polymerase chain reaction, expression cloning technology and gene expression systems in E. coli has led to the production of SC142 single-chain fragments, which was similar in activity to the SC142 parent antibody confirmed by immunohistochemistry. Analysis by DNA sequencing, SDS–PAGE and Western blotting has demonstrated the integrity of the single-chain fragments. Competitive ELISA showed that SC142 single-chain fragments originated from parent SC142 antibody. BIAcore biosensor binding experiments showed that the SC142 single-chain fragments had an ideal dissociation rate constant as a tumour imaging reagent. These results illustrate the potential application of these novel products as an immunodiagnostic and further immunotherapeutic reagent
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Liquid gallium cooling of silicon crystals in high intensity photon beam
The high-brilliance, insertion-device-based, photon beams of the next generation of synchrotron sources will deliver large thermal loads (1 kW to 10 kW) to the first optical elements. Considering the problems that present synchrotron users are experiencing with beams from recently installed insertion devices, new and improved methods of cooling these first optical elements, particularly when they are diffraction crystals, are clearly needed. A series of finite element calculations were performed to test the efficiency of new cooling geometries and new cooling fluids. The best results were obtained with liquid Ga metal flowing in channels just below the surface of the crystal. Ga was selected because of its good thermal conductivity and thermal capacity, low melting point, high boiling point, low kinetic viscosity, and very low vapor pressure. Its very low vapor pressure, even at elevated temperatures, makes it especially attractive in uhv conditions. A series of experiments were conducted at CHESS in February of 1988 that compared liquid gallium cooled silicon diffraction crystals with water cooled crystals. 2 refs., 16 figs., 1 tab
Spin-Charge-Lattice Coupling through Resonant Multi-Magnon Excitations in Multiferroic BiFeO3
Spin-charge-lattice coupling mediated by multi-magnon processes is
demonstrated in multiferroic BiFeO3. Experimental evidence of two and three
magnons excitations as well as multimagnon coupling at electronic energy scales
and high temperatures are reported. Temperature dependent Raman experiments
show up to five resonant enhancements of the 2-magnon excitation below the Neel
temperature. These are shown to be collective interactions between on-site Fe
d-d electronic resonance, phonons and multimagnonsComment: 11 pages including figure
Systematic Improvements in Transmon Qubit Coherence Enabled by Niobium Surface Encapsulation
We present a novel transmon qubit fabrication technique that yields
systematic improvements in T coherence times. We fabricate devices using an
encapsulation strategy that involves passivating the surface of niobium and
thereby preventing the formation of its lossy surface oxide. By maintaining the
same superconducting metal and only varying the surface structure, this
comparative investigation examining different capping materials and film
substrates across different qubit foundries definitively demonstrates the
detrimental impact that niobium oxides have on the coherence times of
superconducting qubits, compared to native oxides of tantalum, aluminum or
titanium nitride. Our surface-encapsulated niobium qubit devices exhibit T
coherence times 2 to 5 times longer than baseline niobium qubit devices with
native niobium oxides. When capping niobium with tantalum, we obtain median
qubit lifetimes above 200 microseconds. Our comparative structural and chemical
analysis suggests that amorphous niobium suboxides may induce higher losses.
These results are in line with high-accuracy measurements of the niobium oxide
loss tangent obtained with ultra-high Q superconducting radiofrequency (SRF)
cavities. This new surface encapsulation strategy enables further reduction of
dielectric losses via passivation with ambient-stable materials, while
preserving fabrication and scalable manufacturability thanks to the
compatibility with silicon processes
Lawson criterion for ignition exceeded in an inertial fusion experiment
For more than half a century, researchers around the world have been engaged in attempts to achieve fusion ignition as a proof of principle of various fusion concepts. Following the Lawson criterion, an ignited plasma is one where the fusion heating power is high enough to overcome all the physical processes that cool the fusion plasma, creating a positive thermodynamic feedback loop with rapidly increasing temperature. In inertially confined fusion, ignition is a state where the fusion plasma can begin "burn propagation" into surrounding cold fuel, enabling the possibility of high energy gain. While "scientific breakeven" (i.e., unity target gain) has not yet been achieved (here target gain is 0.72, 1.37 MJ of fusion for 1.92 MJ of laser energy), this Letter reports the first controlled fusion experiment, using laser indirect drive, on the National Ignition Facility to produce capsule gain (here 5.8) and reach ignition by nine different formulations of the Lawson criterion
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