Investigating the effect of ultrasonic consolidation on shape memory alloy fibres

This research was driven by the capability of the Ultrasonic Consolidation (UC) manufacturing process to create smart metal matrix composites for use within high value engineering sectors, such as aerospace. The UC process is a hybrid additive/subtractive manufacturing process that embeds fibres into metal matrices via the exploitation of a high plastic flow, low temperature phenomenon encountered at ultrasonic frequency mechanical vibrations. The research concerned an investigation of the use of the UC process for embedding Nickel-Titanium alloy (NiTi) shape memory alloy (SMA) fibres into Aluminium (Al) matrices which could potentially be used as vibration damping structures, stress state variable structures, as well as other future smart material applications. It was hypothesised that the fibre volume fraction within a UC matrix was limited due to a reduction in foil/foil bonding, caused by increased fibre numbers, as opposed to the total level of plastic flow of the matrix material being insufficient to accommodate the increased fibre numbers. This hypothesis was tested by increasing the NiTi SMA fibre volume fraction, within an Al 3003 (T0) metal matrix, beyond that of previous UC work. The metal matrix and the fibre matrix interface of these samples was then microscopically analysed and the overall UC sample integrity was tested via mechanical peel testing. It was found that a fibre volume fraction of ~9.8% volume (30 X Ø100 µm SMA fibres) was the maximum achievable using an Al 3003 (T0) 100 µm thick foil material and conventional UC fibre embedding. A revised hypothesis was postulated that the interlaminar structure created during UC was affected by the process parameters used. This interlaminar structure contained areas of un-bonded foil and the increase of UC process parameters would reduce this area of un-bonded foil. Areas of this interlaminar structure were also thought to have undergone grain refinement which would have created harder material areas within the structure. It was suggested that maximum plastic flow of the matrix had not been reached and thus the use of larger diameter NiTi SMA fibres were embedded to increase the effective SMA fibre volume fraction within Al 3003 (T0) UC samples. It was suggested that the embedding of SMA fibres via UC had an abrasive effect on the SMA fibres and the SMA fibres had an effect on the Al 3003 (T0) microstructure. It was further suggested that the activation of UC embedded SMA fibres would reduce the strength of the fibre/matrix interface and the matrix would impede the ability of the SMA fibres to contract causing a forceful interaction at the fibre to matrix interface, weakening the UC structure. The investigation to test the revised hypothesis was broken down into three sections of study. Study 1 was a methodology to determine the characteristics of the interlaminar surface created via UC and how this surface affected the nature of the consolidated sample. UC samples of Al 3003 (T0) were manufactured using a range of process parameters. The analysis involved optical microscopy to determine the UC weld density and the interlaminar surface; mechanical peel testing to quantify the interlaminar bond strength; white light interferometry to measure the interlaminar surface profile and microhardness measurements to determine the hardness of the interlaminar material. Study 2 was a methodology to allow the analysis of the microstructural and mechanical interactions at the fibre/matrix interface, post-UC. Al 3003 (T0) samples were manufactured via UC using a range of process parameters with various NiTi SMA fibre diameters embedded. The analysis involved using mechanical peel testing to determine the interlaminar bond strength; optical microscopy to determine the level of fibre encapsulation; scanning electron microscopy and focussed ion beam analysis to analyse the fibre and matrix grain structures and microscopic interactions. Study 3 was a methodology to investigate the fibre usage as would be expected from envisaged applications of an SMA containing metal matrix composite. Samples were manufactured using a range of UC process parameters with various SMA fibre diameters embedded and the embedded SMA fibres were subjected to different extension/contraction cycle numbers. The analysis involved using mechanical peel testing to determine the interlaminar bond strength; optical microscopy to determine the level of fibre encapsulation and the interlaminar effect of fibre activation; fibre pullout testing to measurement the strength of the fibre/matrix interaction and load rate testing of the activated SMA fibres to monitor performance. The interlaminar surface was found to affect the strength and density of interlaminar bonding during the UC process and the use of higher UC process parameters affected this interlaminar structure. Levels of un-bonded material were found within the interlaminar structure and these levels were found to decrease with increasing sonotrode amplitude and pressure with reducing speed. It was suggested that a specifically texture sonotrode could be developed to modify the interlaminar structure to the requirements of the intended sample application. The measurement of the interlaminar material hardness was unsuccessful and future work would likely require a different methodology to measuring this. The work identified a grain refining effect of the embedded SMA fibres on the Al 3003 (T0) matrix material, (grain sizes were reduced from ~15 µm to <1 µm within 20 µm of the SMA fibres), as well as localised damage caused by the UC process to the SMA fibres. The performance of the activated SMA fibres established that this damage did not prohibit the ability of the SMAs to function however the compressive nature of the Al 3003 (T0) matrix was identified as reducing the ability of the SMA fibres to contract. Additionally it was found that the activation of SMA fibres within an Al 3003 (T0) matrix resulted in a reduction of the fibre/matrix interface strength which allowed fibres to be pulled from the composite with greater ease (a loss of ~80% was encountered after a single activation and extension cycle). The use of larger SMA fibre diameters allowed for the fibre volume fraction to be increased however the activation of these SMA fibres had a delaminating effect on the Al 3003 (T0) structure due to the size of the radial expansion of the SMA fibre. The work furthered the understanding of the effect of UC on SMA fibres and highlighted the importance of the interlaminar surface in UC and that to increase the SMA fibre volume fraction to a useable level (25-50%) then an alternative fibre embedding method within UC is required. The fibre/matrix interface interactions during SMA activation have implications in the ability of UC SMA embedded smart metal matrix composites to function successfully due to weakening effects on fibre matrix interface strength and the ability to achieve SMA fibre activation within the metal matrix

A nanometre-scale fibre-to-matrix interface characterization of an ultrasonically consolidated metal matrix composite

Future ‘smart’ structures have the potential to revolutionize many engineering applications. One of the possible methods for creating smart structures is through the use of shape memory alloy (SMA) fibres embedded into metal matrices. Ultrasonic consolidation (UC) allows the embedding of SMAs into metal matrices while retaining the SMA's intrinsic recoverable deformation property. In this work, NiTi SMA fibres were successfully embedded into an Al 3003 (0) matrix via the UC layer manufacturing process. Initially the plastic flow of the Al matrix and the degree of fibre encapsulation were observed using optical microscopy. Then microstructural grain and sub-grain size variation of the Al 3003 (0) matrix at the fibre–matrix interface, and the nature of the fibre–matrix bonding mechanism, were studied via the use of focused ion beam (FIB) cross-sectioning, FIB imaging, scanning electron microscopy, and mechanical peel testing. The results show that the inclusion of the NiTi SMA fibres had a significant effect on the surrounding Al matrix microstructure during the UC process. Additionally, the fibre–matrix bonding mechanism appeared to be mechanical entrapment with the SMA surface showing signs of fatigue from the UC embedding process

3D printing with moondust

Purpose – The purpose of this paper is to investigate the effect of the main process parameters of Laser Melting (LM) type Additive Manufacturing (AM) on multi layered structures manufactured from JSC-1A Lunar regolith (Moondust) simulant powder. Design/methodology/approach – Laser diffraction technology was used to analyse and confirm the simulant powder material particle sizes and distribution. Geometrical shapes were then manufactured on a Realizer SLM™ 100 using the simulant powder. The laser-processed samples were analysed via Scanning Electron Microscopy (SEM) to evaluate surface and internal morphologies, Energy-dispersive X-ray Spectroscopy (EDS) to analyse the chemical composition after processing and the samples were mechanically investigated via Vickers micro-hardness testing. Findings – A combination of process parameters resulting in an energy density value of 1.011 J/mm2 allowed the successful production of components directly from Lunar regolith simulant. An internal relative porosity of 40.8 %, material hardness of 670 ± 11 HV and a dimensional accuracy of 99.8 % were observed in the fabricated samples. Originality/value – This research paper is investigating the novel application of a Powder Bed Fusion AM process category as a potential on-site manufacturing approach for manufacturing structures/components out of Lunar regolith (Moondust). It was shown that this AM process category has the capability to directly manufacture multi-layered parts out of Lunar regolith, which has potential applicability to future moon colonization

Ultrasonic additive manufacturing - a hybrid production process for novel functional products

Ultrasonic Additive Manufacturing (UAM), or Ultrasonic Consolidation as it is also referred, is a hybrid form of manufacture, primarily for metal components. The unique nature of the process permits extremely novel functionality to be realised such as multi-material structures with embedded componentry. UAM has been subject to research and investigation at Loughborough University since 2001. This paper introduces UAM then details a number of key findings in a number of areas that have been of particular focus at Loughborough in recent years. These include; the influence of pre-process material texture on interlaminar bonding, secure fibre positioning through laser machined channels, and freeform electrical circuitry integration

Ultrasonic additive manufacturing research at Loughborough University

Ultrasonic Additive Manufacturing (UAM) has been subject to research and investigation at Loughborough University since 2001. In recent years, three particular areas of significant focus have been: • The influence of pre-process material texture on interlaminar bonding. • Secure fibre positioning through laser machined channels. • Freeform electrical circuitry integration. This paper details the key findings and a number of conclusions from these work areas. The results of this work have led to the further research and developmental applications for the UAM technology

The effect of ultrasonic excitation on the electrical properties and microstructure of printed electronic conductive inks

Ultrasonic Additive Manufacturing (UAM) is an advanced manufacturing technique, which enables the embedding of electronic components and interconnections within solid aluminium structures, due to the low temperature encountered during material bonding. In this study, the effects of ultrasonic excitation, caused by the UAM process, on the electrical properties and the microstructure of thermally cured screen printed silver conductive inks were investigated. The electrical resistance and the dimensions of the samples were measured and compared before and after the ultrasonic excitation. The microstructure of excited and unexcited samples was examined using combined Focused Ion Beam and Scanning Electron Microscopy (FIB/SEM) and optical microscopy. The results showed an increase in the resistivity of the silver tracks after the ultrasonic excitation, which was correlated with a change in the microstructure: the size of the silver particles increased after the excitation, suggesting that inter-particle bonding has occurred. The study also highlighted issues with short circuiting between the conductive tracks and the aluminium substrate, which were attributed to the properties of the insulating layer and the inherent roughness of the UAM substrate. However, the reduction in conductivity and observed short circuiting were sufficiently small and rare, which leads to the conclusion that printed conductive tracks can function as interconnects in conjunction with UAM, for the fabrication of novel smart metal components

The effect of ultrasonic excitation on the electrical properties and microstructure of printed electronic conductive inks

Ultrasonic Additive Manufacturing (UAM) is an advanced manufacturing technique, which enables the embedding of electronic components and interconnections within solid aluminium structures, due to the low temperature encountered during material bonding. In this study, the effects of ultrasonic excitation, caused by the UAM process, on the electrical properties and the microstructure of thermally cured screen printed silver conductive inks were investigated. The electrical resistance and the dimensions of the samples were measured and compared before and after the ultrasonic excitation. The microstructure of excited and unexcited samples was examined using combined Focused Ion Beam and Scanning Electron Microscopy (FIB/SEM) and optical microscopy. The results showed an increase in the resistivity of the silver tracks after the ultrasonic excitation, which was correlated with a change in the microstructure: the size of the silver particles increased after the excitation, suggesting that inter-particle bonding has occurred. The study also highlighted issues with short circuiting between the conductive tracks and the aluminium substrate, which were attributed to the properties of the insulating layer and the inherent roughness of the UAM substrate. However, the reduction in conductivity and observed short circuiting were sufficiently small and rare, which leads to the conclusion that printed conductive tracks can function as interconnects in conjunction with UAM, for the fabrication of novel smart metal components

Additive manufacturing using extra-terrestrial multi-component ceramic materials

Powder Bed Fusion (PBF) based Additive Manufacturing (AM) is a category of advanced manufacturing technologies that can fabricate three-dimensional assets directly from CAD data, on a successive layer-by-layer strategy by using thermal energy from a laser source, to irradiate and fuse particles on a powder bed. The aim of this research was to investigate the application of this advanced manufacturing technique to laser process ceramic multicomponent materials into 3D layered structures. These ceramic materials matched those found on the Lunar and/or Martian surface. These indigenous extra-terrestrial materials could potentially be used for manufacturing physical assets onsite (i.e. off World) on future planetary exploration missions and could cover a range of potential applications including infrastructure, radiation shielding, thermal storage, etc. JSC-1A Lunar and JSC-Mars-1A Martian soil simulants, mimicking the mineralogical and basic properties of these planetary indigenous materials were used for the purpose of this study and processed with commercially available laser additive manufacturing equipment. The results of the laser processing were investigated and quantified through mechanical hardness testing, optical and scanning electron microscopy (SEM) and energy dispersive x-ray spectroscopy (EDS). The research resulted in the identification of a range of parameters that resulted in the successful manufacture of three-dimensional components from Lunar and Martian ceramic multicomponent simulant materials. The feasibility of using thermal based additive manufacturing with multi-component ceramic materials has therefore been established which represents a potential solution to off-world bulk structure manufacture due to there being no requirement for additional materials and resources other than the manufacturing equipment to be shipped off-world

Additive manufacturing of physical assets by using ceramic multicomponent extra-terrestrial materials

Powder Bed Fusion (PBF) is a range of advanced manufacturing technologies that can fabricate three-dimensional assets directly from CAD data, on a successive layer-by-layer strategy by using thermal energy, typically from a laser source, to irradiate and fuse particles within a powder bed.The aim of this paper was to investigate the application of this advanced manufacturing technique to process ceramic multicomponent materials into 3D layered structures. The materials used matched those found on the Lunar and Martian surfaces. The indigenous extra-terrestrial Lunar and Martian materials could potentially be used for manufacturing physical assets onsite (i.e., off-world) on future planetary exploration missions and could cover a range of potential applications including: infrastructure, radiation shielding, thermal storage, etc.Two different simulants of the mineralogical and basic properties of Lunar and Martian indigenous materials were used for the purpose of this study and processed with commercially available laser additive manufacturing equipment. The results of the laser processing were investigated and quantified through mechanical hardness testing, optical and scanning electron microscopy, X-ray fluorescence spectroscopy, thermo-gravimetric analysis, spectrometry, and finally X-ray diffraction.The research resulted in the identification of a range of process parameters that resulted in the successful manufacture of three-dimensional components from Lunar and Martian ceramic multicomponent simulant materials. The feasibility of using thermal based additive manufacturing with multi-component ceramic materials has therefore been established, which represents a potential solution to off-world bulk structure manufacture for future human space exploration

Assessing extraterrestrial regolith material simulants for in-situ resource utilization based 3D printing

This research paper investigates the suitability of ceramic multicomponent materials, which are found on the Martian and Lunar surfaces, for 3D printing (aka Additive Manufacturing) of solid structures. 3D printing is a promising solution as part of the cutting edge field of future in‐situ space manufacturing applications. 3D printing of physical assets from simulated Martian and Lunar regolith was successfully performed during this work by utilising laser‐based powder bed fusion equipment. Extensive evaluation of the raw regolith simulants was conducted via Optical and Electron Microscopy (SEM), Visible‐Near Infrared/Infrared (Vis‐NIR/IR) Spectroscopy and thermal characterisation via Thermogravimetric Analysis (TGA) and Differential Scanning Calorimetry (DSC). The analysis results led to the characterisation of key properties of these multicomponent ceramic materials with regards to their processability via powder bed fusion 3D printing. The Lunar and Martian simulant regolith analogues demonstrated spectral absorbance values of up to 92% within the Vis‐NIR spectra. Thermal analysis demonstrated that these materials respond very differently to laser processing, with a high volatility (30% weight change) for the Martian analogue as opposed to its less volatile Lunar counterpart (<1% weight change). Results also showed a range of multiple thermal occurrences associated with melting, glass transition and crystallisation reactions. The morphological features of the powder particles are identified as contributing to densification limitations for powder bed fusion processing. This investigation has shown that – provided that the simulants are good matches for the actual regoliths – the lunar material is a viable candidate material for powder bed fusion 3D printing, whereas Martian regolith is not