Rotating sample magnetometer for cryogenic temperatures and high magnetic fields

We report on the design and implementation of a rotating sample magnetometer (RSM) operating in the variable temperature insert of a cryostat equipped with a high-field magnet. The limited space and the cryogenic temperatures impose the most critical design parameters: the small bore size of the magnet requires a very compact pick-up coil system and the low temperatures demand a very careful design of the bearings. Despite these difficulties the RSM achieves excellent resolution at high magnetic field sweep rates, exceeding that of a typical vibrating sample magnetometer by about a factor of ten. In addition the gas-flow cryostat and the high-field superconducting magnet provide a temperature and magnetic field range unprecedented for this type of magnetometer.Comment: 10 pages, 5 figure

Neutron irradiation of coated conductors

Various commercial coated conductors were irradiated with fast neutrons in order to introduce randomly distributed, uncorrelated defects which increase the critical current density, Jc, in a wide temperature and field range. The Jc-anisotropy is significantly reduced and the angular dependence of Jc does not obey the anisotropic scaling approach. These defects enhance the irreversibility line in not fully optimized tapes, but they do not in state-of-the-art conductors. Neutron irradiation provides a clear distinction between the low field region, where Jc is limited by the grain boundaries, and the high field region, where depinning leads to dissipation

Magnetic measurement of the critical current anisotropy in coated conductors

We determine the critical current anisotropy at maximum Lorentz force from hysteresis loops in a vibrating sample magnetometer. To eliminate the signal of spurious variable Lorentz force currents it is sufficient to cut the sample to a specific length, which is calculated from the position dependent sensitivity of the instrument. The procedure increases the resolution of the measurement and the results compare well to transport data on the same sample. As the electric field in magnetisation measurements is lower than in transport experiments the anisotropy at high currents (low temperatures and fields) can be measured without the need of making current contacts or any special sample preparation.Comment: 11 pages, 6 figure

Anisotropic critical currents in FeSe0.5Te0.5 films and the influence of neutron irradiation

We report on measurements of the superconducting properties of FeSe05Te05 thin films grown on lanthanum aluminate. The films have high transition temperatures (above 19 K) and sharp resistive transitions in fields up to 15 T. The temperature dependence of the upper critical field and the irreversibility lines are steep and anisotropic, as recently reported for single crystals. The critical current densities, assessed by magnetization measurements in a vector VSM, were found to be well above 10^9 Am-2 at low temperatures. In all samples, the critical current as a function of field orientation has a maximum, when the field is oriented parallel to the film surface. The maximum indicates the presence of correlated pinning centers. A minimum occurs in three films, when the field is applied perpendicular to the film plane. In the forth film, instead, a local maximum caused by c-axis correlated pinning centers was found at this orientation. The irradiation of two films with fast neutrons did not change the properties drastically, where a maximum enhancement of the critical current by a factor of two was found

A Novel Magnetoscan Setup

Due to a modification in the original magnetoscan setup, a significant improvement in resolution was obtained. The paper focuses on experimental results which should support the idea of the new setup using two magnets with opposite direction of magnetization. This contribution to the characterization techniques of melt-grown bulk superconductors should promote the easy installation of this technique in industry. The improved magnetoscan technique may further help to investigate growth-induced inhomogeneities of the top-seeded-melt-growth process in the submillimeter range, and it offers new possibilities to the characterization of smaller structures such as superconducting films or coated conductors.Comment: 7 pages, 7 figure