Experimental studies of parameters affecting the heat generation in friction stir welding process

Heat generation is a complex process of transformation of a specific type of energy into heat. During friction stir welding, one part of mechanical energy delivered to the welding tool is consumed in the welding process, another is used for deformational processes etc., and the rest of the energy is transformed into heat. The analytical procedure for the estimation of heat generated during friction stir welding is very complex because it includes a significant number of variables and parameters, and many of them cannot be fully mathematically explained. Because of that, the analytical model for the estimation of heat generated during friction stir welding defines variables and parameters that dominantly affect heat generation. These parameters are numerous and some of them, e. g. loads, friction coefficient, torque, temperature, are estimated experimentally. Due to the complex geometry of the friction stir welding process and requirements of the measuring equipment, adequate measuring configurations and specific constructional solutions that provide adequate measuring positions are necessary. This paper gives an overview of the process of heat generation during friction stir welding, the most influencing parameters on heat generation, constructional solutions for the measuring equipment needed for these experimental researches and examples of measured values

The influence of powder particle size on properties of Cu-Al2O3 composites

Inert gas atomized prealloyed copper powder containing 2 wt.% Al (average particle size ≈ 30 μm) and a mixture consisting of copper (average particle sizes ≈ 15 μm and 30 μm) and 4 wt.% of commercial Al2O3 powder particles (average particle size ≈ 0.75 μm) were milled separately in a high-energy planetary ball mill up to 20 h in air. Milling was performed in order to strengthen the copper matrix by grain size refinement and Al2O3 particles. Milling in air of prealloyed copper powder promoted formation of finely dispersed nano-sized Al2O3 particles by internal oxidation. On the other side, composite powders with commercial micro-sized Al2O3 particles were obtained by mechanical alloying. Following milling, powders were treated in hydrogen at 400 0C for 1h in order to eliminate copper oxides formed on their surface during milling. Hot-pressing (800 0C for 3 h in argon at pressure of 35 MPa) was used for compaction of milled powders. Hot-pressed composite compacts processed from 5 and 20 h milled powders were additionally subjected to high temperature exposure (800°C for 1 and 5h in argon) in order to examine their thermal stability. The results were discussed in terms of the effects of different size of starting powders, the grain size refinement and different size of Al2O3 particles on strengthening, thermal stability and electrical conductivity of copper-based composites

Phenolic Compounds and Peroxidases in Sunflower Near-Isogenic Lines After Downy Mildew Infection

Two near-isogenic lines of sunflower, resistant (+Pl6 gene) and susceptible (-P16 gene) to downy mildew were used in this paper. Secondary infection with a suspension of Plasmopara halstedii spores was done on the plants in the phase of first pair of leaves. In the samples taken 12 h after infection, content of phenolic compounds in methanolic extracts from frozen leaves was analysed by HPLC. POD activity was determined spectrophotmetrically and POD isoforms by isoelectrophoresis. Constitutive level of phenolic compounds and their accumulation after infection were higher in the susceptible than in the resistant line. Increased POD amount in leaf, constitutively present in NS-H-26R, was in correlation with increased guaiacol-dependent POD activity and low total phenolics contents. After infection, guaiacol- and chlorogenic acid-dependent POD activity significantly increased in both lines. Scopoletin-dependent POD activity was induced upon infection only in NS-H-26R. IEF electrophoresis revealed existance of four anionic isoforms of peroxidase in leaves of both lines. The main isoform with pI 5 was particularly intesified in the resistant line. In conclusion, scopoletin-dependent POD activity that was induced upon infection only in resistant NIL indicates a specific role of POD in coumarin metabolism that is possibly connected with the presence of Pl6 gene

Transport of F- ions in gaseous environment for technological applications

Negativni halogeni joni su zastupljeni u različitim neravnotežnim plazmama koje su zastupljene u biomedicinskim uređajima, nanotehnologijama, električnim pražnjenjima i hemiji atmosfere. Prikazani su podaci za modelovanje niskotemperaturnih plazmi koje sadrže F- jone primenom globalnih i drugih plazma modela. Ovaj jon je izabran zbog svoje izuzetno velike elektronegativnosti, veoma je jak nukleofilni reagent i formira veoma jake veze sa Luisovim kiselinama u gasnoj fazi. Sa druge strane, neizbežan je u proizvodnji c-BN filmova. Efikasni preseci za rasejanje F- jona na atomima Ar i molekulima F2, CF4 i BF3 dobijeni su primenom Nanbuove teorije u kojoj je moguće razdvojiti elastične od reaktivnih sudarnih procesa. Kako bi se uočili efekti nekonzervativnih sudarnih procesa na brzine drifta, proračuni su rađeni do visokih vrednosti E/N (1000Td).In this work we present swarm data obtained for F- ions in atomic and molecular gases necessary to form the global models for the complex collisional plasmas. We also present the new results for the simple scattering cross section set and proposed transport coefficients for F- ions in BF3 that can be used in such models. Nanbu’s theory based on thermodynamic threshold energies and separating elastic and reactive collisions is used to calculate cross sections for binary collisions of ions with atoms and molecules. For the cases in which the measured transport coefficients were available Momentum Transfer theory (MTT) was applied in order to unfold the cross sections from the measured transport data. Direct Monte Carlo method is applied to obtain swarm parameters at the temperature of T=300 K

Cross-Sections and Transport Properties of F- Ions in F-2

We present the new results for the simple scattering cross-section set and proposed transport coefficients for F- ions in F-2 that can be used in such models. Nanbu's theory based on thermodynamic threshold energies and separating elastic and reactive collisions is used to calculate cross-sections for binary collisions of ions with atoms and molecules. Direct MC method is applied to obtain swarm parameters at temperature of T = 300 K

Cross-Sections and Transport Properties of F- Ions in F-2

We present the new results for the simple scattering cross-section set and proposed transport coefficients for F- ions in F-2 that can be used in such models. Nanbu's theory based on thermodynamic threshold energies and separating elastic and reactive collisions is used to calculate cross-sections for binary collisions of ions with atoms and molecules. Direct MC method is applied to obtain swarm parameters at temperature of T = 300 K

Synthesis for Polynomial Lasso Programs

We present a method for the synthesis of polynomial lasso programs. These programs consist of a program stem, a set of transitions, and an exit condition, all in the form of algebraic assertions (conjunctions of polynomial equalities). Central to this approach is the discovery of non-linear (algebraic) loop invariants. We extend Sankaranarayanan, Sipma, and Manna's template-based approach and prove a completeness criterion. We perform program synthesis by generating a constraint whose solution is a synthesized program together with a loop invariant that proves the program's correctness. This constraint is non-linear and is passed to an SMT solver. Moreover, we can enforce the termination of the synthesized program with the support of test cases.Comment: Paper at VMCAI'14, including appendi

Transport Parameters of F- Ions in BF3

In this work we presented the new results for energy dependent cross-sections and transport coefficients as a function of E/N for F- ions in BF3 gas. Results were obtained by using the Monte Carlo technique for cross-section set determined on the basis of the Nanbu theory. Monte Carlo method is applied to obtain swarm parameters at temperature of T = 300 K