X-ray powder diffraction of high-absorption materials at the XRD1 beamline off the best conditions: Application to (Gd,Nd)5Si4 compounds

Representative compounds of the new family of magnetic materials Gd5-xNdxSi4 were analyzed by X-ray diffraction at the XRD1 beamline at LNLS. To reduce X-ray absorption, thin layers of the powder samples were mounted outside the capillaries and measured in Debye-Scherrer geometry as usual. The X-ray diffraction analyses and the magnetometry results indicate that the behavior of the magnetic transition temperature as a function of Nd content may be directly related to the average of the four smallest interatomic distances between different rare earth sites of the majority phase of each compound. The quality and consistency of the results show that the XRD1 beamline is able to perform satisfactory X-ray diffraction experiments on high-absorption materials even off the best conditions.Comment: 12 pages, 3 figures, 3 table

Adubação foliar da cultura do milho utilizando produtos multinutrientes.

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Intra-industry trade and labor costs: The smooth adjustment hypothesis

We study a situation in which, owing to the exhaustion of non-renewable energy sources, conventional motor vehicles will turn out of use. We consider two scenarios: recycling or dismantling these motor vehicles. M|G|∞ queue system is used to study the process. Through it, we conclude that if the rate of dismantling and recycling of motor vehicles is greater than the rate at which they become idle, the system will tend to get balanced. The model allows also performing a brief study about the recycling or dismantling economic interest.

Anisotropic superconducting properties of aligned MgB2 crystallites

Samples of aligned MgB2 crystallites have been prepared, allowing for the first time the direct identification of an upper critical field anisotropy Hc2^{ab}/Hc2^{c}= xi_{ab}/xi_{c} ~ 1.73; with xi_{o,ab} ~ 70 A, xi_{o,c} ~ 40 A, and a mass anisotropy ratio m_{ab}/m_{c} ~ 0.3. A ferromagnetic background signal was identified, possibly related to the raw materials purity.Comment: 4 pages, 4 figures; Revised version to appear in Phys. Rev. Let

Pressure induced magnetic and magnetocaloric properties in NiCoMnSb Heusler alloy

The effect of pressure on the magnetic and the magnetocaloric properties around the martensitic transformation temperature in NiCoMnSb Heusler alloy has been studied. The martensitic transition temperature has significantly shifted to higher temperatures with pressure, whereas the trend is opposite with the application of applied magnetic field. The maximum magnetic entropy change around the martensitic transition temperature for Ni45Co5Mn38Sb12 is 41.4 J/kg K at the ambient pressure, whereas it is 33 J/kg K at 8.5 kbar. We find that by adjusting the Co concentration and applying suitable pressure, NiCoMnSb system can be tuned to achieve giant magnetocaloric effect spread over a large temperature span around the room temperature, thereby making it a potential magnetic refrigerant material for applications.Comment: 16 pages, 5 figure