576 research outputs found

    Analysis of Temporal Features of Gamma Ray Bursts in the Internal Shock Model

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    In a recent paper we have calculated the power density spectrum of Gamma-Ray Bursts arising from multiple shocks in a relativistic wind. The wind optical thickness is one of the factors to which the power spectrum is most sensitive, therefore we have further developed our model by taking into account the photon down-scattering on the cold electrons in the wind. For an almost optically thick wind we identify a combination of ejection features and wind parameters that yield bursts with an average power spectrum in agreement with the observations, and with an efficiency of converting the wind kinetic energy in 50-300 keV emission of order 1%. For the same set of model features the interval time between peaks and pulse fluences have distributions consistent with the log-normal distribution observed in real bursts.Comment: ApJ in press, 2000; with slight revisions; 12 pag, 6 fi

    On the effect of Ti on Oxidation Behaviour of a Polycrystalline Nickel-based Superalloy

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    Titanium is commonly added to nickel superalloys but has a well-documented detrimental effect on oxidation resistance. The present work constitutes the first atomistic-scale quantitative measurements of grain boundary and bulk compositions in the oxide scale of a current generation polycrystalline nickel superalloy performed through atom probe tomography. Titanium was found to be particularly detrimental to oxide scale growth through grain boundary diffusion

    Atom probe characterisation of segregation driven Cu and Mn-Ni-Si co-precipitation in neutron irradiated T91 tempered-martensitic steel

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    The T91 grade and similar 9Cr tempered-martensitic steels (also known as ferritic-martensitic) are leading candidate structural alloys for fast fission nuclear and fusion power reactors. At low temperatures (300 to 400 ^\circC) neutron irradiation hardens and embrittles these steels, therefore it is important to investigate the origin of this mode of life limiting property degradation. T91 steel specimens were separately neutron irradiated to 2.14 dpa at 327 ^\circC and 8.82 dpa at 377 ^\circC in the Idaho National Laboratory Advanced Test Reactor. Atom probe tomography was used to investigate the segregation driven formation of Mn-Ni-Si-rich (MNSPs) and Cu-rich (CRP) co-precipitates. The precipitates increase in size and, slightly, in volume fraction at the higher irradiation temperature and dose, while their corresponding compositions were very similar, falling near the Si(Mn,Ni) phase field in the Mn-Ni-Si projection of the Fe-based quaternary phase diagram. While the structure of the precipitates has not been characterized, this composition range is distinctly different than that of the typically cited G-phase. The precipitates are composed of CRP with MNSP appendages. Such features are often observed in neutron irradiated reactor pressure vessel (RPV) steels. However, the Si, Ni, Mn, P and Cu solutes concentrations are lower in the T91 than in typical RPV steels. Thus, in T91 precipitation primarily takes place in solute segregated regions of line and loop dislocations. These results are consistent with the model for radiation induced segregation driven precipitation of MNSPs proposed by Ke et al. Cr-rich alpha prime (α\alpha') phase formation was not observed.Comment: Pre-print (not peer reviewed

    Multi-scale microscopy of Reactive Sintered Boride (RSB) neutron shielding materials

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    Protecting superconducting magnets from neutron irradiation is critically important when demonstrating the utility of spherical tokamaks. Reactive Sintered Borides (RSBs) are promising radiation-dense materials and excellent attenuators of slow (< 10 keV) neutrons. No experimental radiation data yet exists on RSBs, hence the need to establish a baseline of RSB microstructure prior to studies on radiation response and aging of RSBs in an active fusion environment. This work investigates the structure and composition of RSB materials over 5 orders of magnitude. SEM, TEM-EDX, atom probe tomography (APT) and XRD were evaluated the microstructure of a selection of RSB compositions. Sintered RSBs were observed to be dominated by FeWB/FeW2B2 bodies, mixed tungsten borides and WC as the key hard phases present. TEM and SEM detected a complex Fe-rich alloy with near-pure Fe interstitial phases. Key findings from this work are that (i) carbon balance is as significant as boron content when considering microstructure and phase presence;(ii) FeWB/FeW2B2 growth is highly temperature dependant and (iii) dense, coherent RSB formation is contingent on the total boron and carbon atomic percentage (B + C)at% is 40% < x ≤ 50%

    Nanomagnetic properties of the meteorite cloudy zone.

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    Meteorites contain a record of their thermal and magnetic history, written in the intergrowths of iron-rich and nickel-rich phases that formed during slow cooling. Of intense interest from a magnetic perspective is the "cloudy zone," a nanoscale intergrowth containing tetrataenite-a naturally occurring hard ferromagnetic mineral that has potential applications as a sustainable alternative to rare-earth permanent magnets. Here we use a combination of high-resolution electron diffraction, electron tomography, atom probe tomography (APT), and micromagnetic simulations to reveal the 3D architecture of the cloudy zone with subnanometer spatial resolution and model the mechanism of remanence acquisition during slow cooling on the meteorite parent body. Isolated islands of tetrataenite are embedded in a matrix of an ordered superstructure. The islands are arranged in clusters of three crystallographic variants, which control how magnetic information is encoded into the nanostructure. The cloudy zone acquires paleomagnetic remanence via a sequence of magnetic domain state transformations (vortex to two domain to single domain), driven by Fe-Ni ordering at 320 °C. Rather than remanence being recorded at different times at different positions throughout the cloudy zone, each subregion of the cloudy zone records a coherent snapshot of the magnetic field that was present at 320 °C. Only the coarse and intermediate regions of the cloudy zone are found to be suitable for paleomagnetic applications. The fine regions, on the other hand, have properties similar to those of rare-earth permanent magnets, providing potential routes to synthetic tetrataenite-based magnetic materials.European Research Counci
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