Rapid and tunable growth of well-ordered hexagonal nanoporous anodic aluminum oxide (AAO) structure by two step high temperature anodization

In this study, we have developed a swift and well-ordered growth of the Anodic Aluminum Oxide (AAO) nanoporous structure by two-step high temperature anodization of pure Aluminum substrate. The pre-anodization surface treatment of the aluminum substrate assists in the formation of well-organized nanoporous structures. The two-step anodization process was performed in 0.3 M of oxalic acid at 20 C for 40 V and 45 V to obtain tunable pore diameters. The high temperature of the electrolyte solution helps in the rapid growth of the AAO nanoporous structure. The top surface image of AAO shows a well-ordered nanoporous structure with an average pore diameter of 70 nm at 40 V and 100 nm at 45 V. The SEM cross sectional view also illustrates the well-ordered nano channel and the elemental mapping elaborates the presence of aluminum and oxygen. The thickness of the AAO nanoporous structure was determined by using SEM for three anodization time spans (20, 24 and 28 hours), in which an increasing trend was observed. The fabricated AAO has a higher thickness and a well-ordered nanoporous structure that shows it can be used as a template for fabricating nanostructured materials.The accepted manuscript in pdf format is listed with the files at the bottom of this page. The presentation of the authors' names and (or) special characters in the title of the manuscript may differ slightly between what is listed on this page and what is listed in the pdf file of the accepted manuscript; that in the pdf file of the accepted manuscript is what was submitted by the author

The Influence of Nanoparticle Dispersions on Mechanical and Thermal Properties of Polymer Nanocomposites Using SLA 3D Printing

The synergistic integration of nanocomposites and 3D printing has opened a gateway to the future and is soon expected to surpass its rivalry with traditional manufacturing techniques. However, there is always a challenge associated with preparing a nanocomposite resin for polymerization-based 3D printing, which is the agglomeration of nanoparticles. Due to the high surface-area-to-volume ratio, the nanoparticles form clusters in the composite matrix, which affects the final properties. This paper aims to analyze the effects of graphene oxide (GO) dispersion on the mechanical and thermal properties of 3D-printed nanocomposites. In particular, a well-dispersed sonication dispersion route is employed for analyzing high and poor GO dispersions and their effects on different properties. After different microscopic analyses and testing, the optimum sonication condition was 30 min at an amplitude of 70%. In terms of mechanical properties, both tensile and compression strength first increased and then decreased gradually with different dispersions as well as varying GO concentrations. Furthermore, there was less or no effect on thermal stability. GO of 0.05 wt.% had the highest compression and tensile strength, while beyond 0.05 to 0.5 wt.%, both strengths reduced slowly. These 3D-printed nanocomposites have found their application in automotive, sports, and biomedical fields

A review on vibration characteristics of additively manufactured metal alloys

The advent of additive manufacturing (AM) has dramatically shifted the manufacturing sector conceptualization, design, and creation of products. AM can facilitate the production of complicated geometries and create functioning components with distinctive features for aerospace and automotive applications. However, defects such as pores, voids, interfaces, and inclusions can impair the quality and functionality of AM components. Vibration analysis (VA) has become a popular tool for the dynamic qualification and testing of products and nondestructive testing, but the literature lacks a comprehensive review of VA applied to AM. Hence, in this article, recent advances in the application of VA for identifying and characterizing flaws in metal alloys, including titanium, aluminum, and nickel-based alloys produced by AM, are summarized. In this review, studies on defects such as porosity, cracks, and inclusions and their effect on VA are also included. Herein, this article concludes with a discussion of the limitations of VA for defect characterization and future research directions. Overall, VA is a promising nondestructive testing method for quality assurance in AM and offers insights on overcoming the difficulties for further development and application of this technology.H2020 Marie Skłodowska-Curie Actions. Grant Number: 101034425 Türkiye Bilimsel ve Teknolojik Araştırma Kurumu. Grant Number: 120C15