X-ray microtomography to evaluate the efficacy of paraffin wax coating for soil bulk density evaluation

The paraffin-coated method is a well-used approach to measure the soil bulk density (BD). BD is a physical property of great importance for studies of soil quality and health. Therefore, representative measurements of this property are highly valued. Resin and paraffin wax are utilized to coat soil samples; however, if these materials ingress into the sample it could affect the representativeness of BD evaluation. The advance in three-dimensional (3D) image analysis techniques such as X-ray microtomography (μCT) offers a great opportunity to visualize and quantify the possible penetration of paraffin wax into clod samples. In this paper we investigated porous system morphological properties of soil samples coated with paraffin wax. The morphological properties of the pores filled with paraffin wax inside the samples were also studied. We observed qualitatively that samples with large pores close to their borders were more susceptible to the penetration of paraffin wax. Samples with pores >10 mm3 had the highest amount of paraffin wax into them. Triaxial shaped and complexly pores also offered less resistance to the ingress of paraffin wax. Positive relations between the amount of paraffin wax inside the samples and the volume of pores measured, pore tortuosity and degree of anisotropy were found. Conversely, the soil pore connectivity was not correlated with the penetration of paraffin wax into the samples, at least for the region of interest (≈27.3 cm3) studied. Finally, an analysis of the impact of paraffin wax ingress inside the samples in measured BD showed increments of ≈0.09 and ≈0.11 g cm−3 in this property when the paraffin wax penetrates into the large pores

X-ray microtomography analysis of soil pore structure dynamics under wetting and drying cycles

The soil water retention curve is one of the most important properties used to predict the amount of water available to plants, pore size distribution and hydraulic conductivity, as well as knowledge for drainage and irrigation modeling. Depending on the method of measurement adopted, the water retention curve can involve the application of several wetting and drying (W-D) cycles to a soil sample. The method assumes soil pore structure is constant throughout however most of the time soil structure is dynamic and subjected to change when submitted to continuous W-D. Consequently, the pore size distribution, as well as other soil morphological properties can be affected. With this in mind, high resolution X-ray Computed micro-Tomography was utilized to evaluate changes in the soil pore architecture following W-D cycles during the procedure of the water retention curve evaluation. Two different soil sample volumes were analyzed: ROIW (whole sample) and ROIHC (the region close to the bottom of the sample). The second region was selected due to its proximity to the hydraulic contact of the soil with the water retention curve measurement apparatus. Samples were submitted to the following W-D treatments: 0, 6 and 12 W-D. Results indicated the soil changed its porous architecture after W-D cycles. The image-derived porosity did not show differences after W-D cycles for ROIW; while for ROIHC it increased porosity. The porosity was also lower in ROIHC in comparison to ROIW. Pore connectivity improved after W-D cycles for ROIHC, but not for ROIW. W-D cycles induced more aligned pores for both ROIs as observed by the tortuosity results. Pore shape showed changes mainly for ROIW for the equant and triaxial shaped pores; while pore size was significantly influenced by the W-D cycles. Soil water retention curve measurements showed that W-D cycles can affect water retention evaluation and that the changes in the soil morphological properties can play an important role in it