71 research outputs found

    A novel and facile method for silica nanoparticles synthesis from high temperature vulcanization (HTV) silicon

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    This study is introducing a facile and novel method for synthesis of amorphous silica nanoparticles. Silica nanoparticles were synthesized by pyrolysis and combustion of high temperature vulcanization (HTV) silicone at 700 oC for 1 h. The products were investigated employing transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), dynamic light scattering (DLS), X-ray diffraction (XRD), Brunauer Emmett and Teller (BET) test and Fourier Transform Infrared (FTIR) Spectroscopy. The results indicated that the method is capable of synthesis of amorphous silica nanoparticles with sizes of mostly between 10 and 50 nm

    A novel and facile method for silica nanoparticles synthesis from high temperature vulcanization (HTV) silicon

    Get PDF
    This study is introducing a facile and novel method for synthesis of amorphous silica nanoparticles. Silica nanoparticles were synthesized by pyrolysis and combustion of high temperature vulcanization (HTV) silicone at 700 oC for 1 h. The products were investigated employing transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), dynamic light scattering (DLS), X-ray diffraction (XRD), Brunauer Emmett and Teller (BET) test and Fourier Transform Infrared (FTIR) Spectroscopy. The results indicated that the method is capable of synthesis of amorphous silica nanoparticles with sizes of mostly between 10 and 50 nm

    The Relationship between Blood Lead Levels and Clinical Features among Multiple Sclerosis Patients in Isfahan, Iran

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    Lead (Pb) is one of the most likely toxicants that could be potentially a risk factor in the development of Multiple Sclerosis (MS) through changes in the immune system. The purpose of the study was to describe the clinical features of MS in general and for sub-groups stratified for gender, age, residence, disease duration, disability degree, clinical diagnosis in Isfahan, Iran and also, to elucidate the relationship between the blood Pb level and the development of MS. Blood samples of 48 patients (20 to 57 years) were selected from the department of neurology of the Kashani hospital in Isfahan, Iran and were analyzed for Pb using anodic stripping voltammetry (ASV). The clinical and demographic characteristics in our study were similar to those in other reports. The blood Pb level in 70.83% of the total population wa

    Green synthesis, characterization and antibacterial activity of silver nanoparticles from root extract of Lepidium draba weed

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    In the present study, Lepidium draba root was used to fabricate silver nanoparticles (Ag NPs). The NPs produced with different amounts of this weed root extract were analyzed by Fourier transform-IR spectroscopy. X-ray diffraction analysis and FE-SEM and TEM techniques were also used to morphologically investigate the particles’ crystal structure. Staphyloccocus aureus, Bacillus cereus, Salmonella typhimurium, and Escherichia coli were then utilized to evaluate the antibacterial activity of the Ag NPs. SEM showed the formation of Ag NPs dispersed within the size range of 20–80 nm. X-ray diffraction analysis showed that the average crystalline size of synthesized Ag NPs was 24 nm. The results indicated that by increasing the concentrations of the root extract of L. draba, one can obtain smaller sized Ag NPs. The antimicrobial activity of those Ag NPs that had undergone green synthesis was more effective than that of corresponding silver ions

    A novel and facile method for silica nanoparticles synthesis from high temperature vulcanization (HTV) silicon

    No full text
    This study is introducing a facile and novel method for synthesis of amorphous silica nanoparticles. Silica nanoparticles were synthesized by pyrolysis and combustion of high temperature vulcanization (HTV) silicone at 700 oC for 1 h. The products were investigated employing transmission electron microscopy (TEM), field emission scanning electron microscopy (FESEM), dynamic light scattering (DLS), X-ray diffraction (XRD), Brunauer Emmett and Teller (BET) test and Fourier Transform Infrared (FTIR) Spectroscopy. The results indicated that the method is capable of synthesis of amorphous silica nanoparticles with sizes of mostly between 10 and 50 nm
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