Microscopic Surface Change of Polycrystalline Aluminum duringTensile Plastic Deformation

Roughening on free surface of polycrystalline metal during plastic deformation is closely related to the inhomogeneous deformation in the respective grain at the surface. Uniaxial tensile tests are carried out on annealed pure aluminum sheet specimens with various averaged grain sizes. The roughening is measured by a 3-dimensional stylus instrument to examine the roughness change in both sides of specimen surfaces at each strain. The irregularities on one side are reversed on the backside, when the averaged grain size is as large as the thickness of the specimen. Discussions are made on the relation between the surface shapes of both sides adopting the cross correlation factor. The strains of respective grains are also measured from the grain boundary shape before and after plastic deformation. There are some deviations in the strains of the grains and their standard deviation increases with the applied strain

Microscopic Observation of Tensile Deformation Behavior of Polycrystalline Titanium with Scanning Probe Microscope

The change in the surface morphology of polycrystalline titanium during tensile plastic deformation is studied, using the scanning probe microscope as well as the laser scanning microscope. The observation shows that the slip occurs mainly near grain boundary at the strain range of ε < 0.05. The slip develops with the applied strain, and the slip on the second slip system or the crossing of slip lines appear. The surface roughness increases linearly with the applied strain. The height difference between the grain boundary area and the inner grain area also increases with the applied strain, though the increase rate becomes low after the applied strain of about 0.3. The nano-scale height difference of the surface step of slip lines increases with the applied strain, though it remains almost constant after the applied strain of 0.4. The averaged surface roughness measured with the scanning probe microscope is in good agreement with that measured with the laser scanning microscope

Observation of Orientation Change During Plastic Deformation of Polycrystalline Copper by EBSD Method

Change in crystal orientation and strain of individual grains during tensile plastic deformation are studied to clarify on the microscopic deformation behavior of polycrystalline copper. The orientation of grain is measured by electron backscatter diffraction (EBSD) technique in the scanning electron microscope. The principal strain of grain is also measured by obtaining the approximated ellipse of strain distribution. The deformation of grains dependent on their initial orientation and the rotation of the principal strain during uniaxial tension are clarified

Free reflection multiarrangements and quasi-invariants

To a complex reflection arrangement with an invariant multiplicity function one can relate the space of logarithmic vector fields and the space of quasi-invariants, which are both modules over invariant polynomials. We establish a close relation between these modules. Berest-Chalykh freeness results for the module of quasi-invariants lead to new free complex reflection multiarrangements. K. Saito's primitive derivative gives a linear map between certain spaces of quasi-invariants. We also establish a close relation between non-homogeneous quasi-invariants for root systems and logarithmic vector fields for the extended Catalan arrangements. As an application, we prove the freeness of Catalan arrangements corresponding to the non-reduced root system $BC_N$.Comment: 26 pages; small change

Plant Mitochondrial-Targeted Gene Delivery by Peptide/DNA Micelles Quantitatively Surface-Modified with Mitochondrial Targeting and Membrane-Penetrating Peptides

Plant mitochondria play essential roles in metabolism and respiration. Recently, there has been growing interest in mitochondrial transformation for developing crops with commercially valuable traits, such as resistance to environmental stress and shorter fallow periods. Mitochondrial targeting and cell membrane penetration functions are crucial for improving the gene delivery efficiency of mitochondrial transformation. Here, we developed a peptide-based carrier, referred to as Cytcox/KAibA-Mic, that contains multifunctional peptides for efficient transfection into plant mitochondria. We quantified the mitochondrial targeting and cell membrane-penetrating peptide modification rates to control their functions. The modification rates were easily determined from high-performance liquid chromatography chromatograms. Additionally, the gene carrier size remained constant even when the mitochondrial targeting peptide modification rate was altered. Using this gene carrier, we can quantitatively investigate the relationships between various peptide modifications and transfection efficiency and optimize the gene carrier conditions for mitochondrial transfection

Preparation of Polyrotaxane Fibers. Part II: Tensile Properties of Polyrotaxane Fibers Treated with Two Cross-linking Reagents

Polyrotaxane fibers prepared with wet spinning of polyrotaxane consisting of poly(ethylene glycol) and cyclodextrins were cross-linked with two different cross-linking reagents, i.e., divinyl sulfone (DVS) and ethylene glycol diglycidyl ether (EGDE), to improve the tensile properties of the fibers. By cross-linking with DVS, the values for the tenacity at break and the initial modulus were increased with cross-linking time, while the elongation at break was improved only moderately. On the other hand, drastic improvements in elongation at break were observed after EGDE cross-linking, up to 645% of its original length, although the tenacity at break and the initial modulus showed only slight improvements. After cross-linking, only minor changes in the degree of crystallinity of the fibers were observed by wide-angle X-ray scattering measurements.ArticleTEXTILE RESEARCH JOURNAL. 80(12):1131-1137 (2010)journal articl

Spin-Dependent Dynamics of Photocarrier Generation in Electrically Detected Nitrogen-Vacancy-Based Quantum Sensing

Electrical detection of nitrogen-vacancy (N-V) centers in diamond is advantageous for developing and integrating quantum information processing devices and quantum sensors and has the potential to achieve a higher collection efficiency than that of optical techniques. However, the mechanism for the electrical detection of N-V spins is not fully understood. In this study, we observe positive contrast in photocurrent detected magnetic resonance (PDMR). Note that negative PDMR contrast is usually observed. To discuss the sign of the PDMR contrast, we numerically analyze the dynamics of photocarrier generation by N-V centers using a seven-level rate model. It is found that the sign of the PDMR contrast depends on the difference in the photocurrent generated from the excited states and the metastable state of N-V centers. Furthermore, we demonstrate ac magnetic field sensing using spin coherence with the PDMR technique. ac magnetic field measurement with the PDMR technique is still challenging because the noise from a fluctuating magnetic environment is greater than the measured signal. Here, we introduce noise suppression using a phase-cycling-based noise-canceling technique. We demonstrate electrically detected ac magnetic field sensing with a sensitivity of 29 nT Hz[−1/2]. Finally, we discuss sensitivity enhancement based on the proposed model

99mTc generator using molybdenum nanoparticles

The version of record of this article, first published in Journal of Radioanalytical and Nuclear Chemistry, is available online at Publisher’s website: https://doi.org/10.1007/s10967-023-09173-