8 research outputs found
Drilling bits in percussive-rotary drilling technology (down the hole DTH)
This paper addresses the issue of drillbits for drilling normal and large diameter boreholes with the use of percussion-rotary method. The most important elements of drillbits, i.e. sintered carbide inserts of different shapes have been described. The hardness of the drilled rock determines the shape of used sintered carbide inserts and the shape of the drillbit face. The cluster hammers, used for drilling large diameter DTH, have been also presented
The role and position of iron in 0.8CaZrO3-0.2CaFe2O4
The aim of the study was to characterize the 0.8CaZrO3-0.2CaFe2O4 composite structure with particular
emphasis on the role and position of iron in the function of sintering temperature. The paper presents
the results of 57Fe Mössbauer effect at room temperature. It was found that the increase of sintering temperature
causes an increase in the amount of incorporated iron ions in the CaZrO3-crystal structure. Based on Mössbauer
spectroscopy analysis, it was found that three different environments of Fe3+ ions were observed in the obtained
materials. Two of them corresponded to CaFe2O4 phase and one was associated with the substitution of Zr4+
by Fe3+ in the CaZrO3 structure
Position of Fe ions in MgO crystalline structure
Magnesium oxide (MgO) is one of the most important raw materials in many branches of industry.
Magnesium oxide is a popular refractory raw material because of its high refractoriness and high resistance to
basic slags and environment. In many cases, use of MgO is limited by its properties, especially the presence of
secondary phases like iron oxides. The amount and distribution of iron oxides can strongly infl uence the technological
properties of MgO and depend on the manufacturing method, particularly the heat-treatment process.
The aim of the study was to evaluate the infl uence of the heat-treatment process on amount and distribution of
iron ions in a magnesium oxide lattice. The 57Fe Mössbauer effect measurements of fused and sintered magnesium
oxide samples doped by the iron oxide were conducted. Investigation reveals in both cases the presence
of Fe2+ as well as Fe3+ ions. Fe2+ ions occupy Mg2+ octahedral sites in the MgO lattice, whereas the Fe3+ ions
are located in highly distorted octahedral coordination. The amount of Fe2+ varies from around 66% for fused
samples to 30% for sintered samples
The role and position of iron in 0.8CaZrO3-0.2CaFe2O4
The aim of the study was to characterize the 0.8CaZrO3-0.2CaFe2O4 composite structure with particular
emphasis on the role and position of iron in the function of sintering temperature. The paper presents
the results of 57Fe Mössbauer effect at room temperature. It was found that the increase of sintering temperature
causes an increase in the amount of incorporated iron ions in the CaZrO3-crystal structure. Based on Mössbauer
spectroscopy analysis, it was found that three different environments of Fe3+ ions were observed in the obtained
materials. Two of them corresponded to CaFe2O4 phase and one was associated with the substitution of Zr4+
by Fe3+ in the CaZrO3 structure
Low Temperature Processing of Nanostructures Based on II-VI Semiconductors Quantum Wells
We report the first results of electron beam lithography processes performed on polymethyl methacrylate (PMMA) and hydrogen silsesquioxane (HSQ) resists, which have been pre-backed in vacuum at T ≤ 90°C. For such low temperature processing the lithographical resolution is reduced as compared to standard procedures, however, the exposure contrast and adhesion to CdTe and HgTe substrates have been sufficient for the fabrication of sub-μ m quantum devices. Furthermore, the new method of electrical microcontact forming is proposed, based on the local melting and annealing of an indium metal layer, performed with the application of accelerated electron beam. The method has been tested for CdTe/CdMgTe quantum wells using the lithography techniques, the exposure parameters have been optimized by inspecting the morphology of annealed metal film via the in situ imaging