SiGeC alloy layer formation by high-dose C + implantations into pseudomorphic metastable Ge0.08Si0.92 on Si(100)

Dual-energy carbon implantation (1 × 1016/cm2 at 150 and at 220 keV) was performed on 260-nm-thick undoped metastable pseudomorphic Si(100)/ Ge0.08Si0.92 with a 450-nm-thick SiO2 capping layer, at either room temperature or at 100 °C. After removal of the SiO2 the samples were measured using backscattering/channeling spectrometry and double-crystal x-ray diffractometry. A 150-nm-thick amorphous layer was observed in the room temperature implanted samples. This layer was found to have regrown epitaxially after sequential annealing at 550 °C for 2 h plus at 700 °C for 30 min. Following this anneal, tensile strain, believed to result from a large fraction of substitutional carbon in the regrown layer, was observed. Compressive strain, that presumably arises from the damaged but nonamorphized portion of the GeSi layer, was also observed. This strain was not significantly affected by the annealing treatment. For the samples implanted at 100 °C, in which case no amorphous layer was produced, only compressive strain was observed. For samples implanted at both room temperature and 100 °C, the channelled backscattering yield from the Si substrate was the same as that of the virgin sample

Influence of calcination conditions on structural and solid‐state kinetic properties of iron oxidic species supported on SBA‐15

Iron oxidic species supported on silica SBA-15 were synthesized with various iron loadings using two different FeIII precursors. The effect of varying powder layer thickness during calcination on structural and solid-state kinetic properties of FexOy/SBA-15 samples was investigated. Calcination was conducted in thin (0.3 cm) or thick (1.3 cm) powder layer. Structural characterization of resulting FexOy/SBA-15 samples was performed by nitrogen physisorption, X-ray diffraction, and DR-UV/Vis spectroscopy. Thick powder layer during calcination induced an increased species size independent of the precursor. However, a significantly more pronounced influence of calcination mode on species size was observed for the FeIII nitrate precursor compared to the FeIII citrate precursor. Temperature-programmed reduction (TPR) experiments revealed distinct differences in reducibility and reduction mechanism dependent on calcination mode. Thick layer calcination of the samples obtained from FeIII nitrate precursor resulted in more pronounced changes in TPR profiles compared to samples obtained from FeIII citrate precursor. TPR traces were analyzed by model-dependent Coats-Redfern method and model-independent Kissinger method. Differences in solid-state kinetic properties of FexOy/SBA-15 samples dependent on powder layer thickness during calcination correlated with differences in iron oxidic species size.TU Berlin, Open-Access-Mittel - 201

Reversal of the extraordinary Hall effect polarity in thin Co/Pd multilayers

Thin Co/Pd multilayers, with room temperature perpendicular anisotropy and an enhanced surface scattering, were studied for the possible use in the extraordinary Hall effect (EHE) - based magnetic memory devices. Polarity of the EHE signal was found to change from negative in thick samples to positive in thin ones. Reversal of EHE sign was also observed in thick samples with aging. The effect is argued to be related to the dominance of surface scattering having the EHE polarity opposite to that of the bulk

Do the nearby BHB stars belong to the Thick Disk or the Halo?

We study the Milky Way region Z<3.0 kpc, where the thick disk and inner halo overlap, by using the kinematics of local blue horizontal branch (BHB) stars (within 1 kpc) and new samples of BHB stars and A-type stars from the Century Survey. We derive Galactic U,V,W velocities for these BHB and A-type star samples using proper motions from the NOMAD catalog. The mean velocities and the velocity dispersions of the BHB samples (Z<3 kpc) are characteristic of the halo, while those of the Century Survey A-type stars are characteristic of the thick disk. There is no evidence from our samples that the BHB stars rotate with the thick disk in the region Z<3 kpc. Nearly a third of the nearby local RR Lyrae stars have disk kinematics and are more metal-rich than [Fe/H]~-1. Only a few percent of the Century Survey BHB stars have these properties. Only one nearby BHB star (HD 130201) is likely to be such a disk star but selection based on high proper motions will have tended to exclude such stars from the local sample. The scale height derived from a sample of local RR Lyrae stars agrees with that of the Century Survey BHB stars. The local samples of BHB stars and metal-weak red giants are too incomplete for a similar comparison.Comment: 14 pages, accepted to A

Superconductivity devices: Commercial use of space

High T sub C superconducting thick film were prepared by a screen printing process. Y-based (YBa2Cu3O(7-x) superconducting thick film were printed on 211/Al2O3, SNT/Al2O3, and YSZ substrates. Because of poor adhesion of the superconductor thick films to 211/Al2O3 and SNT/Al2O3 substrates, relatively low T sub C and J sub C values were obtained from the films printed on these substrates. Critical temperatures (T sub C) of YBa2Cu3O(7-x) thick films deposited on 211/Al2O3 and SNT/Al2O3 substrates were about 80 K. The critical current densities (J sub C) of these films were less than 2 A/sq cm. Higher T sub C and J sub C YBa2Cu3O(7-x) thick films were printed on YSZ substrates. A YBa2Cu3O(7-x) thick film with T sub C=86.4 and J sub C= 50.4 A/sq cm was prepared by printing the film on YSZ substrate and firing at 990 C for 10 minutes. Multiple-lead samples were also prepared on the YSZ substrates. The multiple-lead samples showed lower T sub C and/or J sub C values than those of the plain samples. The electrical properties of YBa2Cu3O(7-x) thick films were determined by the microstructures of the films. The YBa2Cu3O(7-x) thick films printed on the YSZ substrates, which had the best properties among the films printed on the three different kinds of substrates, had the highest density and the best particle interconnection. The YBa2Cu3O(7-x) thick films with preferred orientation in (001) direction were obtained on the YSZ substrates. Cracks, which retard the properties of the films, were found from the films deposited on the YSZ substrates. Currently, a MSZ (Magnesium Stabilized Zirconia) substrate, which had higher thermal expansion coefficient than the YSZ substrate, is used as substrate for the YBa2Cu3O(7-x) thick film in order to eliminate the cracks on the film. Bi-based superconductor thick films were printed on polycrystalline MgO and YSZ substrates. Interactions between BSCCO thick films and the YSZ substrates were observed. Various buffer layer materials were applied onto the substrates in order to avoid the interactions between the BSCCO thick films and the ZrO2-based substrates. So far, a BSCCO printed on MgO substrate with T Sub C=89K was obtained. The J sub C of the film was lower than 0.1 A/sq cm by reason of poor interconnectivity of the BSCCO particles

Video-rate 3D Particle Tracking with Extended Depth-of-field in Thick Biological Samples

We present a single-aperture 3D particle localisation and tracking technique with a vastly increased depth-of-field without compromising optical resolution and throughput. Flow measurements in a FEP capillary and a zebrafish blood vessel are demonstrated experimentally

Magnetic and microwave properties of (Ni,Co)Fe2O4-ferroelectric and (La,Ca,Sr)MnO3-ferroelectric multilayer structures

Structural, magnetic and ferromagnetic resonance characterization studies have been performed on lay-ered ferromagnetic-ferroelectric oxides that show strong magnetoelectric coupling. The samples contained thick films of ferrites or substituted lanthanum manganites for the ferromagnetic phase and lead zirconate titanate for the ferroelectric phase, and were sintered high temperatures. Results indicate defect free ferrites, but deterioration of manganite parameters due to diffusion at the interface and accounts for poor magnetoelectric coupling in manganite-PZT samples