Fracture toughness and crack-resistance curve behavior in metallic glass-matrix composites

Nonlinear-elastic fracture mechanics methods are used to assess the fracture toughness of bulk metallic glass (BMG) composites; results are compared with similar measurements for other monolithic and composite BMG alloys. Mechanistically, plastic shielding gives rise to characteristic resistance-curve behavior where the fracture resistance increases with crack extension. Specifically, confinement of damage by second-phase dendrites is shown to result in enhancement of the toughness by nearly an order of magnitude relative to unreinforced glass

Thermal shock testing for assuring reliability of glass-sealed microelectronic packages

Tests were performed to determine if thermal shocking is destructive to glass-to-metal seal microelectronic packages and if thermal shock step stressing can compare package reliabilities. Thermal shocking was shown to be not destructive to highly reliable glass seals. Pin-pull tests used to compare the interfacial pin glass strengths showed no differences between thermal shocked and not-thermal shocked headers. A 'critical stress resistance temperature' was not exhibited by the 14 pin Dual In-line Package (DIP) headers evaluated. Headers manufactured in cryogenic nitrogen based and exothermically generated atmospheres showed differences in as-received leak rates, residual oxide depths and pin glass interfacial strengths; these were caused by the different manufacturing methods, in particular, by the chemically etched pins used by one manufacturer. Both header types passed thermal shock tests to temperature differentials of 646 C. The sensitivity of helium leak rate measurements was improved up to 70 percent by baking headers for two hours at 200 C after thermal shocking

Measurements of the Rate Capability of Various Resistive Plate Chambers

Resistive Plate Chambers (RPCs) exhibit a significant loss of efficiency for the detection of particles, when subjected to high particle fluxes. This rate limitation is related to the usually high resistivity of the resistive plates used in their construction. This paper reports on measurements of the performance of three different glass RPC designs featuring a different total resistance of the resistive plates. The measurements were performed with 120 GeV protons at varying beam intensitie

Observation of a superconducting glass state in granular superconducting diamond

The magnetic field dependence of the superconductivity in nanocrystalline boron doped diamond thin films is reported. Evidence of a glass state in the phase diagram is presented, as demonstrated by electrical resistance and magnetic relaxation measurements. The position of the phase boundary in the H-T plane is determined from resistance data by detailed fitting to zero-dimensional fluctuation conductivity theory. This allows determination of the boundary between resistive and non-resistive behavior to be made with greater precision than the standard ad hoc onset/midpoint/offset criterion

Electrical Resistance Tomography of Conductive Thin Films

The Electrical Resistance Tomography (ERT) technique is applied to the measurement of sheet conductance maps of both uniform and patterned conductive thin films. Images of the sheet conductance spatial distribution, and local conductivity values are obtained. Test samples are tin oxide films on glass substrates, with electrical contacts on the sample boundary, some samples are deliberately patterned in order to induce null conductivity zones of known geometry while others contain higher conductivity inclusions. Four-terminal resistance measurements among the contacts are performed with a scanning setup. The ERT reconstruction is performed by a numerical algorithm based on the total variation regularization and the L-curve method. ERT correctly images the sheet conductance spatial distribution of the samples. The reconstructed conductance values are in good quantitative agreement with independent measurements performed with the van der Pauw and the four-point probe methods.Comment: IEEE Transactions on Instrumentation and Measuremen

Unusual magneto-transport of YBa2Cu3O7-d films due to the interplay of anisotropy, random disorder and nanoscale periodic pinning

We study the general problem of a manifold of interacting elastic lines whose spatial correlations are strongly affected by the competition between random and ordered pinning. This is done through magneto-transport experiments with YBa2Cu3O7-d thin films that contain a periodic vortex pinning array created via masked ion irradiation, in addition to the native random pinning. The strong field-matching effects we observe suggest the prevalence of periodic pinning, and indicate that at the matching field each vortex line is bound to an artificial pinning site. However, the vortex-glass transition dimensionality, quasi-2D instead of the usual 3D, evidences reduced vortex-glass correlations along the vortex line. This is also supported by an unusual angular dependence of the magneto-resistance, which greatly differs from that of Bose-glass systems. A quantitative analysis of the angular magnetoresistance allows us to link this behaviour to the enhancement of the system anisotropy, a collateral effect of the ion irradiation

Ageing effects around the glass and melting transitions in poly(dimethylsiloxane) visualized by resistance measurements

The process of ageing in rubbers requires monitoring over long periods (days to years). To do so in non-conducting rubbers, small amounts of carbon-black particles were dispersed in a fractal network through the rubber matrix, to make the rubber conducting without modifying its properties. Continuous monitoring of the resistance reveals the structural changes around the glass and melting transitions and especially details about the hysteresis and ageing processes. We illustrate the method for the semicrystalline polymer poly(dimethylsiloxane) (PDMS).Comment: 4 pages, 4 figure

A broadband microwave Corbino spectrometer at 3^3He temperatures and high magnetic fields

We present the technical details of a broadband microwave spectrometer for measuring the complex conductance of thin films covering the range from 50 MHz up to 16 GHz in the temperature range 300 mK to 6 K and at applied magnetic fields up to 8 Tesla. We measure the complex reflection from a sample terminating a coaxial transmission line and calibrate the signals with three standards with known reflection coefficients. Thermal isolation of the heat load from the inner conductor is accomplished by including a section of NbTi superconducting cable (transition temperature around 8 $-$ 9 K) and hermetic seal glass bead adapters. This enables us to stabilize the base temperature of the sample stage at 300 mK. However, the inclusion of this superconducting cable complicates the calibration procedure. We document the effects of the superconducting cable on our calibration procedure and the effects of applied magnetic fields and how we control the temperature with great repeatability for each measurement. We have successfully extracted reliable data in this frequency, temperature and field range for thin superconducting films and highly resistive graphene samples