Location of Repository

1,4-Dihex­yloxy-2,5-bis­(2-nitro­phen­yl)benzene

By Norma Wrobel, Dieter Schollmeyer and Heiner Detert

Abstract

The title compound, C30H36N2O6, was prepared via twofold Suzuki coupling of a diboronic acid with bromo­nitro­benzene. The mol­ecule is located on a crystallographic inversion centre. The lateral benzene ring and the central ring make a dihedral angle of 48.75 (14)° and the nitro group is twisted by 41.47 (13)° out of the plane of the benzene ring. The nitro and hex­yloxy groups are in close proximity and the hex­yloxy chain adopts an all-anti conformation

Topics: Organic Papers
Publisher: International Union of Crystallography
OAI identifier: oai:pubmedcentral.nih.gov:3343986
Provided by: PubMed Central
Download PDF:
Sorry, we are unable to provide the full text but you may find it at the following location(s):
  • http://www.pubmedcentral.nih.g... (external link)
  • Suggested articles

    Preview

    Citations

    1. (s), 123.9 (d), 113.4 (d), 69.1 (t), 31.3 (t), 28.8 (t), 25.4 (t), 22.5 (t), 13.8 (q). IR (ATR): ν =
    2. (2012). Fractional atomic coordinates and isotropic or equivalent isotropic displacement parameters (Å2) xy zU iso*/Ueq
    3. (2012). organic compounds o1022 Wrobel et al. doi:10.1107/S1600536812009944 Acta Cryst.

    To submit an update or takedown request for this paper, please submit an Update/Correction/Removal Request.