The theoretical principles of the ESR technique and its application in the field of molecular
sieve science are reviewed. The first part of this chapter focuses on the basic principles
and instrumentation of the ESR, ENDOR, ESE and ESEEM techniques. Special attention will be
given to spectral simulation and quantitative analysis of ESR spectra. In the second part, the
general features of the ESR spectra of transition metal ions and paramagnetic clusters in
molecular sieves are presented and discussed. In addition, some remarks will be made about
the use of paramagnetic molecules, such as NO
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