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(E)-4-[(4-Nitrophenyl)diazenyl]phenyl

By Mo K Radiation, Mark A. Rodriguez, A Jessica L. Nichol, B Thomas Zifer, Andrew L. Vance and C Bryan M. Wong C

Abstract

R factor = 0.043; wR factor = 0.100; data-to-parameter ratio = 11.9. In the title compound, C27H17N3O4, the azo group displays a trans conformation and the dihedral angles between the central benzene ring and the pendant anthracene and nitrobenzene rings are 82.94 (7) and 7.30 (9) , respectively. In the crystal structure, weak C—H O hydrogen bonds, likely associated with a dipole moment present on the molecule, help to consolidate the packing. Related literature This structure is similar to the perviously reported compound (E)-2-{Ethyl[4-(4-nitrophenyldiazenyl)phenyl]amino}ethyl anthracene-9-carboxylate (Rodriguez, et al., 2008). For general background, see: Atassi et al. (1998); Becke (1993). Experimental Crystal data C 27H 17N 3O 4 M r = 447.44 Data collection Bruker SMART CCD area-detector diffractometer Absorption correction: multi-sca

Topics: wR(F 2) = 0.100
Year: 2008
OAI identifier: oai:CiteSeerX.psu:10.1.1.352.79
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