R factor = 0.037; wR factor = 0.106; data-to-parameter ratio = 9.4. The title compound, C5H9O4PS, was synthesized by the reaction of pentaerythritol with thiophosphoryl chloride. In the crystal structure, the three six-membered rings all adopt boat conformations. Molecules form chains along the c axis via intermolecular O—H O hydrogen bonds
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