A Ti-15Mo/TiB metal matrix composite was produced by the spark plasma sintering process at 1400°C using a Ti-14.25 wt.% Mo-5 wt.% TiB2 powder mixture. The microstructure and mechanical properties of the composite were studied after non-isothermal rolling of specimens heated to 1000°C to a thickness strain of ~0.7. Transmission and scanning electron microscopy, as well as X-ray analysis were used for microstructure examinatio