89 research outputs found

    Highly Porous Ceramic Material and Method of using and Forming the Same

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    The present invention generally relates to porous ceramic material and to methods of making and using the material. More particularly, the invention relates to methods of forming ceramic materials by depositing material, using atomic layer deposition, onto a sacrificial substrate and to ceramic materials having controlled wall thickness, relatively large pores, and high surface area by weight

    Flash sintering of zirconia/alumina powders

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    Yttria-stabilized cubic zirconia (YSZ) is the most-common electrolyte material for solid oxide fuel cells due to its reasonable oxygen-ion conductivity and chemical stability. To achieve suitable ionic conductivities, YSZ ceramics must be near theoretical density, requiring sintering temperatures around 1450°C. In 2011, it was demonstrated that flash sintering densifies YSZ in a few seconds at 750°C.1 During flash sintering, an electric field is applied across the sample and at a certain threshold temperature, the sample conductivity and power dissipation rapidly increase causing densification. Since densification occurs in just a few seconds, grain growth can be difficult to control. During conventional sintering of YSZ ceramics, researchers have demonstrated that the addition of a small quantity of aluminum oxide (Al2O3) pins grain boundaries, reducing YSZ grain size.2 However, the effect of small quantities of Al2O3 addition on the grain growth of flash sintered YSZ has not been studied. Please click Additional Files below to see the full abstract

    EXPERIMENTS AND MODELLING OF MICRO-JET ASSISTED FLUIDIZATION OF NANOPARTICLES

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    The fluidization of nanoparticle agglomerates can be largely improved by using downward pointing micronozzles, creating a high-velocity jet, as experimentally shown. By discrete particle simulations – treating the agglomerates as single particles – we show that the main reason is probably the reduction of the agglomerate size by agglomerate-agglomerate collisions

    Experiments and Modelling of Micro-Jet Assisted Fluidization of Nanopowder

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    The fluidization of nanoparticle agglomerates can be largely improved by using downward pointing micronozzles, creating a high-velocity jet, as experimentally shown. By discrete particle simulations – treating the agglomerates as single particles – we show that the microjet strongly reduces the amount of gas in voids

    Fluidized Bed Polymer Particle ALD Process for Producing HDPE/Alumina Nanocomposites

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    Micron-sized High Density Polyethylene (HDPE) particles were coated with ultrathin alumina (Al2O3) films in a Fluidized Bed Reactor (FBR) by Atomic Layer Deposition (ALD) at 77 ºC. Al2O3 films on the HDPE particles were confirmed by different methods. These particles were extruded conventionally with the ceramic shells mixing intimately in the polymer matrix. The successful dispersion of the Al2O3 shells in the polymer matrix following extrusion was confirmed using cross sectional Transmission Electron Microscopy (TEM)
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