Flexural behavior of carbon and glass fiber composite laminates reinforced with Nylon 6,6 electrospun nanofibers

Nylon 6,6 nanofibers manufactured by means of electrospinning have been used to interleave Mode II fracture mechanics glass and carbon uni-directional (UD) fiber composite specimens. The aim of this work was to study the effect of the nanofibers materials in their ability to reinforce the interleave. Experimental testing was carried out on specimens with a nanofibrous mat interleaved into a delaminated interface. Specimens of 10, 16 and 18 layers were manufactured and tested. Results demonstrated that the effect of nanofibers was different between the two materials and that the fibers material plays an important role in the reinforcement mechanism of the nanofibers

The effect of thickness of Nylon 6,6 nanofibrous mat on Modes I-II fracture mechanics of UD and woven composite laminates

This paper presents an experimental investigation on epoxy resin-carbon bers composites interleaved with Nylon 6,6 nanobers. In particular, the paper focuses on the eect of the thickness of the nanoreinforce into two types of laminae: unidirectional (UD) and plain wave (PW). The eectiveness of the nanoreinforce has been addressed by comparing critical and propagation energy release rates, calculated by testing samples under Mode I and Mode II fracture mechanic loads. Experiments show a general improvement in delamination resistance when the nanobers are interleaved. Nevertheless slightly dierent behaviour has been found between the two types of lamina: micrographs of crack paths have been used to explain the reinforce mechanisms and such dierences, suggest- ing a strong interaction between the nature of the fabric and the thickness of the nanointerlayer

Pattern recognition of acoustic emission signal during the mode I fracture mechanisms in carbon- epoxy composite

The aim of the paper is to use Acoustic Emission technique to distinguish the micro/macro failure mechanisms of carbon-epoxy composite laminates during Double Cantilever Beam (DCB) tests. In order to recognize and detect different damage mechanisms, Self-Organizing Map (SOM) method has been used to cluster the AE signals according with the fracture mode that originated them. In addition, most significate Learning vector quantization (LVQ) program has been applied to verify the signals. Five AE features were selected as main parameters: Rise-time, Counts, Energy, Duration and Amplitude. The results highlighted that different signals can be recognized and classified related to their origin. The failure mechanisms detected are Matrix cracking, delamination, and fiber breakage. Scanning Electron Microscopy (SEM) images validate the results. Mathematics data and experimental results confirmed a good converging of AE dat

Electrospun nanofibers as reinforcement for composite laminates materials – a review

In the last few decades nanofibers have been developed and introduced in a vast number of industrial and research applications. One of their most effective use is as interleaved reinforcement for composite laminate materials against delamination. Nanofibrous mats have the ideal morphology to be embedded between two plies of a laminate, and a vast and deep research has been carried out investigating their effect on the global behaviour of a composite laminate. This review is the first of its kind to date which presents a detailed state-of-the-art on the effect of nanofibrous interleaves into composite laminates with focus on the mechanical performances and behaviours of nanomodified materials. A detailed description of the working mechanisms of the nanointerleave under different load cases is presented, and a comparative analysis between papers in literature will provide readers with a powerful tool to understand and use nanofibers for reinforcing purposes

Cohesive zone modelling of delamination response of a composite laminate with interleaved nylon 6,6 nanofibres

This work simulates numerically Double Cantilever Beam and End Notched Flexure experiments on Carbon Fibre Epoxy Resin specimens that have been performed by some of the authors in a previous work. Specimens have been nanomodified by interleaving plies with a layer of electrospun nanofibres in the delaminated interface. Eight different configurations of nanofibres have been used as interleave, for a total of 9 configurations (8 nanomodified plus the virgin one) to be simulated for both kind of tests to identify the cohesive zone parameters corresponding to the effect of nanofibre diameter, nanolayer thickness and nanofibre orientation on the delamination behaviour of the composite. Results showed that a bilinear damage law is necessary for almost all nanomodified configurations, and presented a clear relationship between nanomat layer parameters and the cohesive energy of the interface

Supervised and non-supervised AE data classification of nanomodified CFRP during DCB tests

Aim of the paper is to use acoustic emissions to study the effect of electrospun nylon 6,6 Nanofibrous mat on carbon-epoxy composites during Double Cantilever beam (DCB) tests. In order to recognize the effect of the nanofibres and to detect different damage mechanisms, k-means clustering of acoustic emission signals applied to rise time, count, energy, duration and amplitude of the events is used. Supervised neural network (NN) is then applied to verify clustered signals. Results showed that clustered acoustic emission signals are a reliable tool to detect different damage mechanisms; neural network showed the method has a 99% of accuracy

Fracture mechanics of laser sintered cracked polyamide for a new method to induce cracks by additive manufacturing

This paper presents an experimental investigation on specimens manufactured by Selective Laser Sintering (SLS), with the purposes of giving designers advice when designing 3D printed parts, and laying the basis for a step forward in the field of fracture mechanics of 3D complex parts. The aim is to investigate the effect of building direction in Polyamide (PA) 3D printed samples and to assess whether a crack can be initiated directly from the sintering process for fracture mechanics study purposes. Six different configurations of Mode I Compact Tension (CT) specimens were manufactured and tested; the experiments were monitored by Digital Image Correlation (DIC) and fractured surfaces were analyzed using microscopy. Results showed that samples with better mechanical performance are those in which all the layers contain a portion of the crack. On the other hand, those with layers parallel to the crack plan offer a preferential pathway for the crack to propagate. DIC and fractography investigations showed that, under certain conditions, small-radius geometries, or too-close surfaces may glue depending on printer resolution. Experiments also showed that SLS is capable of printing specimens with internal cracks that can be used to study fracture mechanics of complex parts or parts with internal cracks

Focus on the use of resveratrol in bladder cancer

Bladder cancer is the most common tumor of the urinary system, with a high incidence in the male population. Surgery and intravesical instillations can eradicate it, although recurrences are very common, with possible progression. For this reason, adjuvant therapy should be considered in all patients. Resveratrol displays a biphasic dose response both in vitro and in vivo (intravesical application) with an antiproliferative effect at high concentrations and antiangiogenic action in vivo (intraperitoneal application) at a low concentration, suggesting a potential role for it in clinical management as an adjuvant to conventional therapy. In this review, we examine the standard therapeutical approach to bladder cancer and the preclinical studies that have investigated resveratrol in xenotransplantation models of bladder cancer. Molecular signals are also discussed, with a particular focus on the STAT3 pathway and angiogenic growth factor modulation