328 research outputs found
Optimum Arrangement of Resonator in Micro-bunch Free Electron Laser(III. Accelerator, Synchrotron Radiation, and Instrumentation)
Using a short-bunched beam of electrons from a linear accelator, the output of the micro-bunch FEL has been studied experimentally to clarify the optimum arrangement of an open resonator on the electron orbit. The output depends sharply on the arrangement, and the maximum output is observed when the resonator axis intersects the electron orbit with the angle of 3°
Gibbs free‐energy difference between the glass and crystalline phases of a Ni‐Zr alloy
Observation of millimeter-wave radiation generated by the interaction between an electron beam and a photonic crystal
Ferromagnetism at 300 K in spin-coated anatasea and rutile Ti0.95Fe0.05O2 films
Thin films of Ti1-xFexO2 (x=0 and 0.05) have been prepared on sapphire
substrates by spin-on technique starting from metal organic precursors. When
heat treated in air at 550 and 700 degrees C respectively, these films present
pure anatase and rutile structures as shown both by X-ray diffraction and Raman
spectroscopy. Optical absorption indicate a high degree of transparency in the
visible region. Such films show a very small magnetic moment at 300 K. However,
when the anatase and the rutile films are annealed in a vacuum of 1x10-5 Torr
at 500 degrees C and 600 degrees C respectively, the magnetic moment, at 300 K,
is strongly enhanced reaching 0.46 B/Fe for the anatase sample and 0.48
B/Fe for the rutile one. The ferromagnetic Curie temperature of these
samples is above 350 K.Comment: 13 october 200
Effects of crystallization and dopant concentration on the emission behavior of TiO2:Eu nanophosphors
Uniform, spherical-shaped TiO2:Eu nanoparticles with different doping concentrations have been synthesized through controlled hydrolysis of titanium tetrabutoxide under appropriate pH and temperature in the presence of EuCl3·6H2O. Through air annealing at 500°C for 2 h, the amorphous, as-grown nanoparticles could be converted to a pure anatase phase. The morphology, structural, and optical properties of the annealed nanostructures were studied using X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray spectroscopy [EDS], and UV-Visible diffuse reflectance spectroscopy techniques. Optoelectronic behaviors of the nanostructures were studied using micro-Raman and photoluminescence [PL] spectroscopies at room temperature. EDS results confirmed a systematic increase of Eu content in the as-prepared samples with the increase of nominal europium content in the reaction solution. With the increasing dopant concentration, crystallinity and crystallite size of the titania particles decreased gradually. Incorporation of europium in the titania particles induced a structural deformation and a blueshift of their absorption edge. While the room-temperature PL emission of the as-grown samples is dominated by the 5D0 - 7Fj transition of Eu+3 ions, the emission intensity reduced drastically after thermal annealing due to outwards segregation of dopant ions
Poly(m-Phenylenediamine) Nanospheres and Nanorods: Selective Synthesis and Their Application for Multiplex Nucleic Acid Detection
In this paper, we demonstrate for the first time that poly(m-phenylenediamine) (PMPD) nanospheres and nanorods can be selectively synthesized via chemical oxidation polymerization of m-phenylenediamine (MPD) monomers using ammonium persulfate (APS) as an oxidant at room temperature. It suggests that the pH value plays a critical role in controlling the the morphology of the nanostructures and fast polymerization rate favors the anisotropic growth of PMPD under homogeneous nucleation condition. We further demonstrate that such PMPD nanostructures can be used as an effective fluorescent sensing platform for multiplex nucleic acid detection. A detection limit as low as 50 pM and a high selectivity down to single-base mismatch could be achieved. The fluorescence quenching is attributed to photoinduced electron transfer from nitrogen atom in PMPD to excited fluorophore. Most importantly, the successful use of this sensing platform in human blood serum system is also demonstrated
Influence of Supporting Electrolytes on RO 16 Dye Electrochemical Oxidation Using Boron Doped Diamond Electrodes
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