18 research outputs found

    The effect of the addition of acrylonitrile-butadiene styrene on the mechanical properties of bismaleimide/carbon composites

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    The objective of the work was to investigate the effect of addition of various weight percentages of Acrylonitrile-Butadiene-Styrene in to Bismaleimide resin on mechanical properties. Matrix material and their blends were characterized for viscosity and glass transition temperature. Modified and unmodified carbon composites were prepared and tested for tensile, flexural and impact strengths. Tensile (11%) and impact properties (29%) were found to be highest at 6% weight of ABS. In the case of flexural strength was found to be increasing with increase of ABS. The morphology of the BMI modified resin systems were also studied by scanning electron microscopy

    Electrical and thermal properties of twin-screw extruded multiwalled carbon nanotube/epoxy composites

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    This paper presents the experimental results of dispersing multiwalled carbon nanotubes (MWNTs) into epoxy (space grade structural adhesive) nanocomposites using co-rotating twin screw extrusion process. Two sets of specimens were prepared; set 1 with ultrasonication for predispersing MWNT before extrusion and set 2 direct dispersion of MWNT in the extruder. MWNT was loaded up to 8 vol.% in both the sets. The specimens were characterized for room temperature volume and surface resistivities as per ASTM D257 using Keithley Model 6517 and for thermal conductivity in the temperature range −50 to 150 °C as per ASTM E 1530 using Thermal Conductivity Instrument (TCI) 2022 SX211. The volume resistivity of sets 1 and 2 decreased to an extent of 1011 and 109 respectively. The surface resistivity drop was of the order of 109 for both the sets. These drops corresponded to the maximum MWNT loading of 8 vol.%. Electrical conductivity values of the specimens were fitted into the Power Law Model to evaluate the critical exponent. Both sets 1 and 2 showed increase in thermal conductivity with increase in temperature in the testing range. Thermal conductivity increased with increase in filler loading and the maximum increase was 60% at 150 °C in case of 8 vol.% MWNT nanocomposites for set 1. The corresponding value for the set 2 was 25%. Thermal conductivity values were predicted using Lewis Nielson model. DSC of the specimens showed increase in glass transition temperature with increase in filler loading. The dispersion of the nanofillers was studied using SEM and the surface morphology using AFM

    Effect of amine functionalization of CNF on electrical, thermal, and mechanical properties of epoxy/CNF composites

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    This paper presents experimental results of the effect of amine functionalization of carbon nanofibers (CNF) on the electrical, thermal, and mechanical properties of CNF/epoxy composites. The functionalized and non-functionalized CNFs (up to 3 wt%) were dispersed into epoxy using twin screw extruder. The specimens were characterized for electrical resistivities, thermal conductivity (K), UTS, and Vicker's microhardness. The properties of the nanocomposites were compared with that of neat epoxy. The volume conductivity of the specimens increased by E12 S/cm and E09 S/cm in f-CNF/epoxy and CNF/epoxy, respectively, at 3 wt% filler loading. The increase in K for former was 106% at 150 °C, while for the latter it was only 64%. Similarly, UTS increased by 61% vs. 45% and hardness 65% vs. 43%. Tg increased with increase in filler content. SEM examinations showed that functionalization resulted in better dispersion of the nanofibers and hence greater improvement in the studied properties of the nanocomposites

    The processing and characterization of MWCNT/Epoxy and CB/Epoxy nanocomposites using twin screw extrusion

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    This paper presents results of the processing of nanocomposites based on epoxy and nanofillers, namely multiwalled carbon nanotubes (up to 10wt%) and carbon black (up to 15wt%). The twin screw extruded nanocomposites showed increases in electrical and thermal conductivities, tensile strength, microhardness and glass transition temperature. Electrical conductivity increased on the order of 1011 at 10wt% of nanotubes loading and at 15wt% of carbon black. Greater increases in thermal and mechanical properties were observed in cases of nanotube-dispersed composites more so than others. SEM and AFM were used to examine the dispersion of the fillers

    Photocatalytic degradation of textile effluent using hydrothermally synthesised titania supported molybdenum oxide photocatalyst

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    The photocatalytic degradation of textile effluent using hydrothermally synthesised titania supported molybdenum oxide photocatalyst at 200 degrees C with an autogenous pressure and experimental duration of 24 h has been reported. A control over the particle size, morphology and crystallinity of the photocatalyst has been studied with respect to the experimental parameters such as nutrient composition, solvent, pH, experimental duration, temperature and pressure. The products synthesised were characterised using XRD, SEM, FTIR, etc. The photodegradation of textile effluent using these composite was investigated under both solar and ultraviolet irradiation. The degradation of textile effluent was checked by the following parameters: chemical oxygen demand (COD), percentage transmission (%T), irradiation time and duration. The preliminary results are highly encouraging and further work is being carried out for the use of these photocatalytic compounds for other organic decomposition
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