31 research outputs found

    Hemijski sastav ekstrakta semenki bele ribizle

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    From the seeds of white currant (Ribes rubrum, cv. White Champagne), a new sesquiterpenoid glycoside 1 was isolated, along with two known compounds: dihydrophaseic acid 3'-O-beta-D-glucopyranoside (2), and 3-carboxymethyl-indole-1-N-beta-D-glucopyranoside (3). The structure of the new compound was identified as dihydrophaseic acid 3'-O-beta-gentiobioside, based on extensive NMR and MS spectral studies.Iz semena bele ribizle (Ribes rubrum, cv. bela Å”ampanjska) izolovan je novi seskviterpenski glukozid (1), zajedno sa dva poznata jedinjenja: 3'-O-b-D-glukopiranozidom dihidrofazeinske kiseline (2) i 3-karboksimetilindol-1-N-b-D-glukopiranozidom (3). Na osnovu detaljnih NMR i MS studija, struktura novog jedinjenja je određena kao 3'-O-b-genciobiozid dihidrofazeinske kiseline

    Flavonoidi iz nadzemnih delova Onobrychis montana subsp. scardica

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    Rutin (1, main constituent) and two flavone C-glycosides, vitexin (2) and vitexin 2 ''-O-alpha-rhamnopyranoside (3) were isolated from the aerial parts of Onobrychis montana subsp. scardica. They were identified by (1)H-NMR, (13)C-NMR and UV-Vis spectroscopy (procedure with shift reagents), and high resolution ESI-MS. A relatively high content of 1 (5.27 mg/g of dry plant material), measured by HPLC, indicated O. montana subsp. scardica as a new natural source of this biologically active compound. The isolated flavonoid compounds might be of value as chemotaxonomic markers.Iz nadzemnih delova Onobrychis montana subsp. scardica izolovani su rutin (1, glavni sastojak) i dva flavonoidna S-glikozida, viteksin (2) i njegov 2''-O-Ī±-ramnopiranozid (3). Njihova struktura je određena primenom 1H-NMR, 13C-NMR i UV spektroskopije (procedura sa reagensima UV-pomeranja) i masene spektrometrije visokog razlaganja (HR-ESI-MS). Relativno visok sadržaj rutina (5.27 mg/g suvog materijala) određen pomoću tečne hromatografije (HPLC), ukazuje na O. montana subsp. scardica kao nov prirodni izvor ovog bioloÅ”ki aktivnog jedinjenja. Izolovana jedinjenja mogu biti i od vrednosti kao hemotaksonomski markeri

    Supplementary data for article: Andelkovic, B.; Vujisić, L. V.; Vučković, I. M.; TeÅ”ević, V.; Vajs, V.; Godevac, D. Metabolomics Study of Populus Type Propolis. Journal of Pharmaceutical and Biomedical Analysis 2017, 135, 217ā€“226. https://doi.org/10.1016/j.jpba.2016.12.003

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    Supplementary material for: [https://doi.org/10.1016/j.jpba.2016.12.003]Related to published version: [http://cherry.chem.bg.ac.rs/handle/123456789/2386]Related to accepted version: [http://cherry.chem.bg.ac.rs/handle/123456789/3017

    Supplementary data for article: Andelkovic, B.; Vujisić, L. V.; Vučković, I. M.; TeÅ”ević, V.; Vajs, V.; Godevac, D. Metabolomics Study of Populus Type Propolis. Journal of Pharmaceutical and Biomedical Analysis 2017, 135, 217ā€“226. https://doi.org/10.1016/j.jpba.2016.12.003

    Get PDF
    Supplementary material for: [https://doi.org/10.1016/j.jpba.2016.12.003]Related to published version: [http://cherry.chem.bg.ac.rs/handle/123456789/2386]Related to accepted version: [http://cherry.chem.bg.ac.rs/handle/123456789/3017
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