6 research outputs found
A New Portable XRD/XRF Instrument for Non-destructive Analysis
A new integrated portable apparatus capable of in situ X-ray diffraction (XRD) and X-ray fluorescence (XRF) measurements is presented. The instrument equipment is based on a Theta-Theta horizontal goniometer projected and developed in order to optimize stability and reliability for apparatus of such a reduced size and capable of capturing both XRF and XRD information. The simultaneous XRD/XRF data collection is achieved by using a Si solid state detector counting the X-ray photons scattered from the sample as a function of both the energy and the angular step. The instrument is also equipped with a software developed in order to provide both ease of operation in the data collection and a complete and fast characterization of the materials in the data analysis
Control of silver-polymer aggregation mechanism by primary particle spatial correlations in dynamic fractal-like geometry
Silver nanocrystals have been prepared by reacting silver nitrate with
ascorbic acid in aqueous solution containing a low concentration of a
commercial polynaphtalene sulphonate polymer (Daxad 19). Various crystalline
morphologies have been obtained simply by tuning the reaction temperature. We
have investigated the nanoparticle formation mechanism at three different
temperatures by in situ and time resolved Small Angle X ray Scattering
measurements. By modeling the scattering intensity with interacting spherical
particles in a fractal-like polymer-Ag matrix, we found signatures of
nucleation, growth and assembly of primary particles of about 15-20 nm. We
observed how the time evolution of both spatial correlations between primary
particles and the dynamic fractal geometry of the polymer-Ag matrix could
influence and determine both the aggregation mechanism and the morphology of
forming nanostructures in solution
Conceptual Design of a Soft Xâray SASEâFEL Source
FELs based on SASE are believed to be powerful tools to explore the frontiers of basic sciences, from physics to chemistry to biology. Intense R&D programs have started in the USA and Europe in order to understand the SASE physics and to prove the feasibility of these sources. The allocation of considerable resources in the Italian National Research Plan (PNR) brought about the formation of a CNRâENEAâINFNâUniversity of Roma "Tor Vergata" study group. A conceptual design study has been developed and possible schemes for linac sources have been investigated, bringing to the SPARX proposal. We report in this paper the results of a preliminary start to end simulation concerning one option we are considering based on an Sâband normal conducting linac with high brightness photoinjector integrated in a RF compressor