Surface enhanced Raman spectroscopy using a single mode nanophotonic-plasmonic platform

Surface Enhanced Raman Spectroscopy (SERS) is a well-established technique for enhancing Raman signals. Recently photonic integrated circuits have been used, as an alternative to microscopy based excitation and collection, to probe SERS signals from external metallic nanoparticles. However, in order to develop quantitative on-chip SERS sensors, integration of dedicated nanoplasmonic antennas and waveguides is desirable. Here we bridge this gap by demonstrating for the first time the generation of SERS signals from integrated bowtie nanoantennas, excited and collected by a single mode waveguide, and rigorously quantify the enhancement process. The guided Raman power generated by a 4-Nitrothiophenol coated bowtie antenna shows an 8 x 10^6 enhancement compared to the free-space Raman scattering. An excellent correspondence is obtained between the theoretically predicted and observed absolute Raman power. This work paves the way towards fully integrated lab-on-a-chip systems where the single mode SERS-probe can be combined with other photonic, fluidic or biological functionalities.Comment: Submitted to Nature Photonic

In situ characterization of two wireless transmission schemes for ingestible capsules

We report the experimental in situ characterization of 30-40 MHz and 868 MHz wireless transmission schemes for ingestible capsules, in porcine carcasses. This includes a detailed study of the performance of a magnetically coupled near-field very high-frequency (VHF) transmission scheme that requires only one eighth of the volume and one quarter of the power consumption of existing 868-MHz solutions. Our in situ measurements tested the performance of four different capsules specially constructed for this study (two variants of each transmission scheme), in two scenarios. One mimicked the performance of a body-worn receiving coil, while the other allowed the characterization of the direction-dependent signal attenuation due to losses in the surrounding tissue. We found that the magnetically coupled near-field VHF telemetry scheme presents an attractive option for future, miniturized ingestible capsules for medical applications

Wireless Sensors and Actuators for Structural Health Monitoring of Fiber Composite Materials

This work evaluates and investigates the wireless generation and detection of Lamb-waves on fiber-reinforced materials using surface applied or embedded piezo elements. The general target is to achieve wireless systems or sensor networks for Structural Health Monitoring (SHM), a type of Non-Destructive-Evaluation (NDE). In this sense, a fully wireless measurement system that achieves power transmission implementing inductive coils is reported. This system allows a reduction of total system weight as well as better integration in the structure. A great concern is the characteristics of the material, in which the system is integrated, because the properties can have a direct impact on the strength of the magnetic field. Carbon-Fiber-Reinforced-Polymer (CFRP) is known to behave as an electrical conductor, shielding radio waves with increasing worse effects at higher frequencies. Due to the need of high power and voltage, interest is raised to evaluate the operation of piezo as actuators at the lower frequency ranges. To this end, actuating occurs at the International Scientific and Medical (ISM) band of 125 kHz or low-frequency (LF) range. The feasibility of such system is evaluated extensively in this work. Direct excitation, is done by combining the actuator bonded to the surface or embedded in the material with an inductive LF coil and setting the circuit in resonance. A more controlled possibility, also explored, is the use of electronics to generate a Hanning-windowed-sine to excite the PWAS in a narrow spectrum. In this case, only wireless power is transmitted to the actuator node, and this lastly implements a Piezo-driver to independently excite Lamb-waves. Sensing and data transfer, on the other hand, is done using the high-frequency (HF) 13.56 MHz. The HF range covers the requirements of faster sampling rate and lower energy content. A re-tuning of the antenna coils is performed to obtain better transmission qualities when the system is implemented in CFRP. Several quasi-isotropic (QI) CFRP plates with sensor and actuator nodes were made to measure the quality of transmission and the necessary energy to stimulate the actuator-sensor system. In order to produce baselines, measurements are prepared from a healthy plate under specific temperature and humidity conditions. The signals are evaluated to verify the functionality in the presence of defects. The measurements demonstrate that it is possible to wirelessly generate Lamb-waves while early results show the feasibility to determine the presence of structural failure. For instance, progress has been achieved detecting the presence of a failure in the form of drilled holes introduced to the structure. This work shows a complete set of experimental results of different sensor/-actuator nodes

Source Localization via Near Field Signal Processing

This thesis is in support of the Precision Personnel Locator (PPL) project being conducted by Worcester Polytechnic Institute (WPI). The overall goal of the PPL project is to locate firemen and other emergency personnel in buildings using Radio Frequency (RF) techniques. The aspiration is to prevent a tragedy similar to the Worcester Cold Storage fire of 1999. The Mantenna homing wand is a spinoff of the PPL system which uses the Near Field properties of Very Low Frequency (VLF band) waves. The Mantenna has been used to successfully demonstrate the ability to locate targets inside harsh RF environments and other radio opaque environments where normal radiation field based systems have degraded performance, such as commercial, industrial, and apartment buildings. This thesis builds upon the Mantenna rescue device by construction of a transmitter subsystem which is physically smaller than the previous version by redesign of the compact VLF antenna. Additionally, exploitation of the approach used by the Mantenna for homing purposes is explored for full location estimation. This work provides the theoretical background and proof of concept test of a Near Field based location system. Simulation and test results are compared for a minimal configuration involving a single receiver

Wireless Corrosion Monitoring for Reinforced Concrete Structures and Concrete Repair

Substantial efforts are put in preservation projects, but often little care is given once the project is finished. How do we know when we need to go back and repair the building again? A long-term monitoring system can provide invaluable information about the conditions of a building and building materials. Such information may help owners, architects, engineers and conservators to understand what the cause of the problem is, when and where the repair is needed, and what type of intervention is necessary. This can help prevent small problems from becoming large problems. This thesis will evaluate wireless monitoring systems for reinforced concrete structures. Using wireless sensors as monitoring devices is not a new technique. In fact, there are already several wireless sensors being used to monitor various types of structures, materials and conditions. However, most of the existing wireless sensors have short service lives due to limited battery capacity and issues with durability. This thesis research focuses on prototyping and evaluating a wireless and battery-less sensing device named Intelligent Aggregate (IA) and Intelligent Aggregate System (IAS). Intelligent Aggregate is based on the technology of passive RFID (Radio Frequency Identification) tags, which can wirelessly communicate with RFID readers through Ultra High Frequency (UHF) electromagnetic waves emitted from the readers. There are several advantages of using RFID devices over existing battery powered wireless sensors, which are bulky in size due to batteries and expensive to maintain due to the need to retrieve the sensors for occasional battery change. On the other hand, IA can operate as long as they can harvest energy from the RFID reader. Another advantage of using IA is the ability to easily and inexpensively build Wireless Sensing Networks (WSNs). By strategically deploying hundreds or thousands, if necessary, wireless sensing devices in a building, we can collect extensive information about the condition of buildings and materials in real-time. Such information would greatly help us to wisely use time, money, and other resources

Next Generation Auto-Identification and Traceability Technologies for Industry 5.0: A Methodology and Practical Use Case for the Shipbuilding Industry

[Abstract] Industry 5.0 follows the steps of the Industry 4.0 paradigm and seeks for revolutionizing the way industries operate. In fact, Industry 5.0 focuses on research and innovation to support industrial production sustainability and place the well-being of industrial workers at the center of the production process. Thus, Industry 5.0 relies on three pillars: it is human-centric, it encourages sustainability and it is aimed at developing resilience against disruptions. Such core aspects cannot be fully achieved without a transparent end-to-end human-centered traceability throughout the value chain. As a consequence, Auto-Identification (Auto-ID) technologies play a key role, since they are able to provide automated item recognition, positioning and tracking without human intervention or in cooperation with industrial operators. Although the most popular Auto-ID technologies provide a certain degree of security and productivity, there are still open challenges for future Industry 5.0 factories. This article analyzes and evaluates the Auto-ID landscape and delivers a holistic perspective and understanding of the most popular and the latest technologies, looking for solutions that cope with harsh, diverse and complex industrial scenarios. In addition, it describes a methodology for selecting Auto-ID technologies for Industry 5.0 factories. Such a methodology is applied to a specific use case of the shipbuilding industry that requires identifying the main components of a ship during its construction and repair. To validate the outcomes of the methodology, a practical evaluation of passive and active UHF RFID tags was performed in an Offshore Patrol Vessel (OPV) under construction, showing that a careful selection and evaluation of the tags enables product identification and tracking even in areas with a very high density of metallic objects. As a result, this article serves as a useful guide for industrial stakeholders, including future developers and managers that seek for deploying identification and traceability technologies in Industry 5.0 scenarios.This work was supported in part by the Auto-Identication for Intelligent Products Research Line of the Navantia-Universidade da Coruña Joint Research Unit under Grant IN853B-2018/02, and in part by the Centro de Investigación de Galicia ``CITIC,'' funded by Xunta de Galicia and the European Union (European Regional Development Fund-Galicia 2014_2020 Program) under Grant ED431G 2019/01Xunta de Galicia; IN853B-2018/02Xunta de Galicia; ED431G 2019/0

Automated Attendance System using Active RFID

The main focus ofthis project is to enhance the integrity and the authenticity ofdata, whereby, conventional system couldn't ensure the safety of the data. As the result, many employees neglect the importance of attitude in working environment. This project offers a safety towards the data, and in the same time helping in monitoring the movement of employees. Given a number of time, this project will undergo several phases which are planning, analysis, design and implementation. Lastly, the success ofthis project will be determined, and a conclusion should be made based on the result obtained, whether the objective has been met or not

Definition, Characteristics and Determining Parameters of Antennas in Terms of Synthesizing the Interrogation Zone in RFID Systems

The radio frequency identification (RFID) systems are gaining in popularity in automated processes of object identification in various socioeconomic areas. However, despite the existing belief, there is no universal RFID system on the commercial market that could be used in all user applications. All components of a developed solution should be carefully selected or designed according to the specification of objects being recognized and characteristics of their environment. In order to determine parameters of propagation or inductively coupled system, especially when it is dedicated to uncommon applications, a multiaspect analysis has to be taken into consideration. Due to complexity, the problem is reduced to analytical or experimental determination of RFID system operation range and a “trial and error” method is mostly used in the industry practice. In order to cope with the barriers existing in the RFID technology, the authors give the review of latest achievements in this field. They focus on the definition, comprehensive characteristics and determination of the antenna parameters. They also pay attention to the 3D interrogation zone (IZ) that is the main parameter in which multitude technical aspects of the RFID systems are gathered simultaneously, as regards the theoretical synthesis as well as market needs

Dissipative Materials Enabled Subwavelength Nanophotonics

Properly structuring materials at subwavelength scale allows for strong light-matter interaction, thereby enhancing near-field effects and engineering far-field scattering through intermodal interference. A majority of such effects are associated with plasmonics where electromagnetic waves created in the vicinity of metallic nanostructures is able to give rise to a variety of novel phenomena and fascinating applications. In the recent years, dielectric nanoparticles with high refractive index based on optically induced electric and magnetic Mie resonances attract a plethora of attention. In this rapidly developing field, dissipative loss in optical materials is considered one of the major challenges. Here, in this dissertation, we show that, counter-intuitively, it contributes positively to sub-wavelength scale light enhancement and confinement, and also improves scattering efficiency in the far field. In the first part of this dissertation, near field enhancement in dissipative dielectric antennas is demonstrated to be orders of magnitude higher than their lossless dielectric counterparts, which is particularly favorable in deep UV applications where metals are plasmonically inactive and transparent dielectrics always have low index. The loss facilitated field enhancement is the result of large material permittivity contrast and electric field discontinuity. These dissipative dielectric nanostructures can be easily achieved with a great variety of dielectrics at their Lorentz oscillation frequencies, thus having the potential to build a completely new material platform boosting light-matter interaction over broader frequency ranges, with advantages such as bio-compatibility, CMOS compatibility and harsh environment endurance. Additionally, manipulation of ultra-violet light through metasurface in the far field utilizing the silicon loss is then presented. We experimentally demonstrate Si metasurfaces working effectively over a broad band down to 290nm, with efficiencies comparable to plasmonic metasurface performance in the infrared regime. And for the first time, we show photolithography enabled by metasurface-generated ultraviolet holograms. We attribute such performance enhancement to the large scattering cross-sections of Si antennas in the ultraviolet range, which is adequately modeled via a circuit model. Our new platform will deepen our understanding of the role of material dissipation and introduce even more material options to broadband metaphotonic applications, including those in integrated photonics and holographic lithography technologies.Dynamically tunable far field with subwavlength nanostructures is always desired for practical applications. In the last section of this dissertation, we introduce a lithography free and field-programmable photonic metacanvas. Previous attempts of realizing such idea used micro-mechanical metamaterials or amorphous-crystalline phase transition materials, which are limited in terms of the functionalities, efficiency, cost, and high working temperature (> 600oC). It is much desired to reconfigure photonic devices in a fast, large-scale, cost-effective, reliable, and free-style way at or near room temperature. Here, we present a completely rewritable meta-canvas on which arbitrary photonic devices can be rapidly written, erased and rewritten. The writing is with a low-power (1 mW) continuous laser and the entire process stays below ~ 90oC. Using these devices we demonstrate dynamical manipulation of optical waves for light propagation, reconstruction and polarization. Such meta-canvas supports physical (re)compilation of photonic operators akin to that of FPGA, opening up possibilities where a single photonic element can be field-programmed to deliver complex, system-level functionalities