Control of a train of high purity distillation columns for efficient production of 13C isotopes

It is well-known that high-purity distillation columns are difficult to control due to their ill-conditioned and strongly nonlinear behaviour. The fact that these processes are operated over a wide range of feed compositions and flow rates makes the control design even more challenging. This paper proposes the most suitable control strategies applicable to a series of cascaded distillation column processes. The conditions for control and input-output relations are discusssed in view of the global control strategy. The increase in complexity with increased number of series cascaded distillation column processes is tackled. Uncertainty in the model parameters is discussed with respect to the dynamics of the global train distillation process. The main outcome of this work is insight into the possible control methodologies for this particular class of distillation processes

FAST : a fault detection and identification software tool

The aim of this work is to improve the reliability and safety of complex critical control systems by contributing to the systematic application of fault diagnosis. In order to ease the utilization of fault detection and isolation (FDI) tools in the industry, a systematic approach is required to allow the process engineers to analyze a system from this perspective. In this way, it should be possible to analyze this system to find if it provides the required fault diagnosis and redundancy according to the process criticality. In addition, it should be possible to evaluate what-if scenarios by slightly modifying the process (f.i. adding sensors or changing their placement) and evaluating the impact in terms of the fault diagnosis and redundancy possibilities. Hence, this work proposes an approach to analyze a process from the FDI perspective and for this purpose provides the tool FAST which covers from the analysis and design phase until the final FDI supervisor implementation in a real process. To synthesize the process information, a very simple format has been defined based on XML. This format provides the needed information to systematically perform the Structural Analysis of that process. Any process can be analyzed, the only restriction is that the models of the process components need to be available in the FAST tool. The processes are described in FAST in terms of process variables, components and relations and the tool performs the structural analysis of the process obtaining: (i) the structural matrix, (ii) the perfect matching, (iii) the analytical redundancy relations (if any) and (iv) the fault signature matrix. To aid in the analysis process, FAST can operate stand alone in simulation mode allowing the process engineer to evaluate the faults, its detectability and implement changes in the process components and topology to improve the diagnosis and redundancy capabilities. On the other hand, FAST can operate on-line connected to the process plant through an OPC interface. The OPC interface enables the possibility to connect to almost any process which features a SCADA system for supervisory control. When running in on-line mode, the process is monitored by a software agent known as the Supervisor Agent. FAST has also the capability of implementing distributed FDI using its multi-agent architecture. The tool is able to partition complex industrial processes into subsystems, identify which process variables need to be shared by each subsystem and instantiate a Supervision Agent for each of the partitioned subsystems. The Supervision Agents once instantiated will start diagnosing their local components and handle the requests to provide the variable values which FAST has identified as shared with other agents to support the distributed FDI process.Per tal de facilitar la utilització d'eines per la detecció i identificació de fallades (FDI) en la indústria, es requereix un enfocament sistemàtic per permetre als enginyers de processos analitzar un sistema des d'aquesta perspectiva. D'aquesta forma, hauria de ser possible analitzar aquest sistema per determinar si proporciona el diagnosi de fallades i la redundància d'acord amb la seva criticitat. A més, hauria de ser possible avaluar escenaris de casos modificant lleugerament el procés (per exemple afegint sensors o canviant la seva localització) i avaluant l'impacte en quant a les possibilitats de diagnosi de fallades i redundància. Per tant, aquest projecte proposa un enfocament per analitzar un procés des de la perspectiva FDI i per tal d'implementar-ho proporciona l'eina FAST la qual cobreix des de la fase d'anàlisi i disseny fins a la implementació final d'un supervisor FDI en un procés real. Per sintetitzar la informació del procés s'ha definit un format simple basat en XML. Aquest format proporciona la informació necessària per realitzar de forma sistemàtica l'Anàlisi Estructural del procés. Qualsevol procés pot ser analitzat, només hi ha la restricció de que els models dels components han d'estar disponibles en l'eina FAST. Els processos es descriuen en termes de variables de procés, components i relacions i l'eina realitza l'anàlisi estructural obtenint: (i) la matriu estructural, (ii) el Perfect Matching, (iii) les relacions de redundància analítica, si n'hi ha, i (iv) la matriu signatura de fallades. Per ajudar durant el procés d'anàlisi, FAST pot operar aïlladament en mode de simulació permetent a l'enginyer de procés avaluar fallades, la seva detectabilitat i implementar canvis en els components del procés i la topologia per tal de millorar les capacitats de diagnosi i redundància. Per altra banda, FAST pot operar en línia connectat al procés de la planta per mitjà d'una interfície OPC. La interfície OPC permet la possibilitat de connectar gairebé a qualsevol procés que inclogui un sistema SCADA per la seva supervisió. Quan funciona en mode en línia, el procés està monitoritzat per un agent software anomenat l'Agent Supervisor. Addicionalment, FAST té la capacitat d'implementar FDI de forma distribuïda utilitzant la seva arquitectura multi-agent. L'eina permet dividir sistemes industrials complexes en subsistemes, identificar quines variables de procés han de ser compartides per cada subsistema i generar una instància d'Agent Supervisor per cadascun dels subsistemes identificats. Els Agents Supervisor un cop activats, començaran diagnosticant els components locals i despatxant les peticions de valors per les variables que FAST ha identificat com compartides amb altres agents, per tal d'implementar el procés FDI de forma distribuïda.Postprint (published version

Fractional transformation-based decentralized robust control of a coupled-tank system for industrial applications

Petrochemical and dairy industries, waste management, and paper manufacturing fall under the category of process industries where flow and liquid control are essential. Even when liquids are mixed or chemically treated in interconnected tanks, the fluid and flow should constantly be observed and controlled, especially when dealing with nonlinearity and imperfect plant models. In this study, we propose a nonlinear dynamic multiple-input multiple-output (MIMO) plant model. This model is then transformed through linearization, a technique frequently utilized in the analysis and modeling of fractional processes, and decoupling for decentralized fixed-structure H-infinity robust control design. Simulation tests based on MATLAB and SIMULINK are subsequently executed. Numerous assessments are conducted to evaluate tracking performance, external disturbance re jection, and plant parameter fluctuations to gauge the effectiveness of the proposed model. The objective of this work is to provide a framework that anticipates potential outcomes, paving the way for implementing a reliable controller synthesis for MIMO-connected tanks in real-world scenarios.This research was partially funded by FONDECYT grant number 1200525 (V.L.) from the National Agency for Research and Development (ANID) of the Chilean government under the Ministry of Science, Technology, Knowledge, and Innovation; and by Portuguese funds through the CMAT—Research Centre of Mathematics of University of Minho—within projects UIDB/00013/2020 and UIDP/00013/2020 (C.C.)

Marshall Space Flight Center Research and Technology Report 2019

Today, our calling to explore is greater than ever before, and here at Marshall Space Flight Centerwe make human deep space exploration possible. A key goal for Artemis is demonstrating and perfecting capabilities on the Moon for technologies needed for humans to get to Mars. This years report features 10 of the Agencys 16 Technology Areas, and I am proud of Marshalls role in creating solutions for so many of these daunting technical challenges. Many of these projects will lead to sustainable in-space architecture for human space exploration that will allow us to travel to the Moon, on to Mars, and beyond. Others are developing new scientific instruments capable of providing an unprecedented glimpse into our universe. NASA has led the charge in space exploration for more than six decades, and through the Artemis program we will help build on our work in low Earth orbit and pave the way to the Moon and Mars. At Marshall, we leverage the skills and interest of the international community to conduct scientific research, develop and demonstrate technology, and train international crews to operate further from Earth for longer periods of time than ever before first at the lunar surface, then on to our next giant leap, human exploration of Mars. While each project in this report seeks to advance new technology and challenge conventions, it is important to recognize the diversity of activities and people supporting our mission. This report not only showcases the Centers capabilities and our partnerships, it also highlights the progress our people have achieved in the past year. These scientists, researchers and innovators are why Marshall and NASA will continue to be a leader in innovation, exploration, and discovery for years to come

Design and Construction of Liquid Level Measurement System

Industrial tank system play important role in industrial application such as in food processing, pharmaceutical industry, chemical industry, water purification system and many more. Today we can see a lot of varieties in different level measurement technologies on the market like ultrasonic level sensor, capacitance level sensor, microwave sensor, and others. One of the frequent used industrial tank systems is couple tank system. The main interest of the use PID is to ensure the supply of liquid is at constant rate. This paper will discuss on the system based on microcontroller unit design to measure and control liquid level accurately to improve the efficiency of motor pumping unit. To developed this system, ATMEGA32 starter kit board is use to control pumping unit (motor), continuous fluid level sensor to measure the liquid level with LED display circuit, and temperature sensor is used to measure the current temperature of liquid inside tank. The system software is written in C language, interrupt routines are used to record and deal with the time data to count the liquid level accurately. This system supposedly can measure the water level up to 25cm and work at 5V supply voltage range

Control and operation of a spinning disc reactor

PhD ThesisThe aim of the present research is to assess the control and operation of a Spinning Disc Reactor (SDR), carried out via four separate investigations. Firstly, the effect of equipment size reduction on control is studied by comparing the performance of a PID controller applied to simulated intensified and conventional processes. It was found that superior control performance in terms of Integral of Absolute Error (IAE) is achieved for the simulated intensified system. However, the results showed that intensified systems are more susceptible to disturbances and the controlled variable exhibits larger overshoots. Furthermore, the frequency response analysis of the two systems showed that the simulated intensified system has reduced stability margins. The second part of the research investigates the task of pH control in a SDR using a PID controller by means of simulation and experimental studies. The effectiveness of a disturbance observer (DO) and a pH characteriser to compensate for the severe pH system nonlinearity is also explored in detail. The experimental studies showed that a PID controller provides adequate setpoint tracking and disturbance rejection performances. However, sluggish transient responses prevailed and the effluent pH limit cycled around the setpoint. There were indications of unstable behaviour at lower flowrates, which implied more advanced control schemas may be required to adapt to various operating regions dictated by the complex thin film hydrodynamics. The addition of the DO scheme improved the control performance by reducing the limit cycles. In the third segment of the investigations, the potential of exploiting the disc rotational speed as a manipulated variable is assessed for the process of barium sulphate precipitation. A PI controller is successfully used to regulate the conductivity of the effluent stream by adjusting the disc rotational speed. The results are immensely encouraging and show that the disc speed may be used as an extra degree of freedom in control system design. Finally, the flow regimes and wave characteristics of thin liquid films produced in a SDR are investigated by means of a thermal imaging camera. The film hydrodynamics strongly affect the heat and mass transfer processes within the processing films, and thus the intensification aspects of SDRs. Therefore, effective control and operation of such units is significantly dependent on the knowledge of film hydrodynamics and the underlying impact of the operating parameters and the manipulated variables on a given process. The results provided an interesting insight and unveiled promising potentials for characterisation of thin liquid film flow and temperature profiles across the disc by means of thermographic techniques. The present study reveals both challenges and opportunities regarding the control aspects of SDRs. It is recommended that equipment design and process control need to be considered simultaneously during the early stages of the future developments. Furthermore, intensified sensors and advanced controllers may be required to achieve an optimum control capability. Currently, the control performance is inhibited by the lack of sufficient considerations during the SDR design and manufacturing stages, and also by the characteristics of the commercially available instrumentation.EPSRC Doctoral Training Awar

On-line method for optimal tuning of PID controllers using standard OPC interface

Introduction− The controlled PID is the most widely used mathematical algorithm as a regulatory control strategy in industrial environments. The applications are varied; however, its answer depends on the proper calculation of its three parameters: the proportional, the derivative, and the integral. Analytical tuning and experimental methods solve the problem, but new tuning possibilities are now enabled within the digital and process integration context. Objective− Automatically and remotely obtain the optimal parameters of the PID controller, taking advantage of an online connection via the OPC communication protocol to analyze the transient response of the system. Methodology− The study is carried out in three main phases; it begins with a PD3 SMAR thermal process with connection via OPC; in this phase, the mathematical model of the process is built analytically based on fundamental laws. In the second phase, using an analytical tuning method, the PID control architecture is created on which the online experimentation is carried out. In the third phase, the genetic algorithms for automatic tuning are implemented, extracting performance measures from the PID controller through the transient response of the process and optimally determining the values for the proportional, derivative, and integral parameters. Results− The automatic tuning method was tested with two properly instrumented industrial processes. The potential for application can be seen due to its good result and because it does not require specific mathematical knowledge compared to conventional tuning methods. Conclusions− The automatic tuning method can be used remotely to calculate the optimal parameters of a PID controller. The parameters are calculated from the transient response and the definition of design criteria adaptable to any need for control, response, and process