Implementation of an effective time-saving two-stage methodology for microstructural characterization of cemented carbides

Linear intercept on scanning electron microscopy micrographs is the most commonly used measurement method to determine carbide grain size and contiguity in WC–Co cemented carbides (hardmetals). However, it involves manual time-consuming measurements and is critically dependent on the quality of the micrographs as well as on the identification and definition of grain boundaries. In this study a two-stage methodology for microstructural characterization of hardmetals is presented. First, a digital semi-automatic image analysis procedure for grain size determination of the carbide phase is presented. It involves an experimental assessment of grain size on processed images corresponding to a series of WC–Co and WC–Ni cemented carbide grades with different microstructural characteristics. Obtained results are then compared to the values obtained by means of the linear intercept technique. A good correlation between the mean grain sizes determined following both measurement techniques was attained. Based on experimental findings, a series of empirical relations were found to correlate grain size distributions obtained following both methods. Second, an empirical relation for estimating carbide contiguity in WC–Co cemented carbides is proposed. This relation considers simultaneously the influence of the binder content and the experimentally determined mean grain size on contiguity. The proposed equation for contiguity estimation is based on extensive data collection from open literature. An excellent agreement was attained between contiguity values estimated from such equation and those obtained using the linear intercept technique. This validates the two-stage procedure as an effective time-saving methodology for microstructural characterization of WC–Co cemented carbides.Peer ReviewedPostprint (author's final draft

Ice morphology modification and solute recovery improvement by heating and annealing during block freeze-concentration of coffee extracts

Several treatments on ice blocks can be applied during block freeze-concentration to increase the solute recovery from the ice. In the present study, the changes in the ice block’s temperature and the application of annealing during the block freeze-concentration of aqueous coffee extracts were studied. The ice block was subjected to heating and annealing prior to the thawing stage. The effect of coolant temperature during ice block heating (T = -10 and -5 °C) and the application of annealing (+, -) on solute recovery and ice structure morphology was evaluated. The use of annealing during block freeze-concentration modified the ice crystal morphology and increased the solute recovery only when it is applied at the highest temperature. In general, the annealing process increased the size and circularity of the ice crystals, consequently improving the solute recovery. Thus, annealing can be used to increase the solute recovery during block freeze-concentration.Postprint (published version

Reformulating Space Syntax: The Automatic Definition and Generation of Axial Lines and Axial Maps

Space syntax is a technique for measuring the relative accessibility of different locations in a spatial system which has been loosely partitioned into convex spaces.These spaces are approximated by straight lines, called axial lines, and the topological graph associated with their intersection is used to generate indices of distance, called integration, which are then used as proxies for accessibility. The most controversial problem in applying the technique involves the definition of these lines. There is no unique method for their generation, hence different users generate different sets of lines for the same application. In this paper, we explore this problem, arguing that to make progress, there need to be unambiguous, agreed procedures for generating such maps. The methods we suggest for generating such lines depend on defining viewsheds, called isovists, which can be approximated by their maximum diameters,these lengths being used to form axial maps similar to those used in space syntax. We propose a generic algorithm for sorting isovists according to various measures,approximating them by their diameters and using the axial map as a summary of the extent to which isovists overlap (intersect) and are accessible to one another. We examine the fields created by these viewsheds and the statistical properties of the maps created. We demonstrate our techniques for the small French town of Gassin used originally by Hillier and Hanson (1984) to illustrate the theory, exploring different criteria for sorting isovists, and different axial maps generated by changing the scale of resolution. This paper throws up as many problems as it solves but we believe it points the way to firmer foundations for space syntax

Use of GIS for planning visual surveillance installations

11-14 September, 2005, Denver, CO, USA. Visual Surveillance is now commonplace in modern societies. Generally, the layout of observers in artificial visual surveillance (e.g., CCTV camera) involves an iterative, manual and gut-feel process of trying various layouts until a satisfactory solution has been found. This paper proposes how a GIS, can be used to identify the optimal number and locations of observers, ensuring complete visual coverage using an automated technique, namely Rank and Overlap Elimination (ROPE). The ROPE technique is a greedy-search method, which iteratively selects the most visibly dominant observer with minimum overlapping vistas. The paper also proposes measurements to characterise the shape of open spaces, relevant in assessing natural surveillance. The paper demonstrates an extension, called Isovist Analyst, to the popular ArcView for planning artificial and natural surveillance in indoor and outdoor open spaces, with arbitrary geometry and topology

Form Accuracy Analysis of Cylindrical Parts Produced by Rapid Prototyping

Solid Freeform fabrication processes are being considered for creating fit and assembly nature functional parts. It is extremely important that these parts are within allowable dimensional and geometric tolerance. The part accuracy produced by rapid prototyping process is greatly affected by the relative orientation of build and face normal directions. A systematic method is needed to find the reliability of the created product. This paper discusses the work done in this area and the effect of build orientation on the part form accuracy analysis of each specified tolerance like circularity and cylindricity. Feasible build direction that can be used to satisfy those tolerances is identified. It will help process engineer in selecting a build direction that can satisfy a mathematical model of form tolerance.Mechanical Engineerin

Relating cell shape and mechanical stress in a spatially disordered epithelium using a vertex-based model

Using a popular vertex-based model to describe a spatially disordered planar epithelial monolayer, we examine the relationship between cell shape and mechanical stress at the cell and tissue level. Deriving expressions for stress tensors starting from an energetic formulation of the model, we show that the principal axes of stress for an individual cell align with the principal axes of shape, and we determine the bulk effective tissue pressure when the monolayer is isotropic at the tissue level. Using simulations for a monolayer that is not under peripheral stress, we fit parameters of the model to experimental data for Xenopus embryonic tissue. The model predicts that mechanical interactions can generate mesoscopic patterns within the monolayer that exhibit long-range correlations in cell shape. The model also suggests that the orientation of mechanical and geometric cues for processes such as cell division are likely to be strongly correlated in real epithelia. Some limitations of the model in capturing geometric features of Xenopus epithelial cells are highlighted.Comment: 29 pages, 10 figures, revisio