Characterization Of Thermal Stresses And Plasticity In Through-Silicon Via Structures For Three-Dimensional Integration

Through-silicon via (TSV) is a critical element connecting stacked dies in three-dimensional (3D) integration. The mismatch of thermal expansion coefficients between the Cu via and Si can generate significant stresses in the TSV structure to cause reliability problems. In this study, the thermal stress in the TSV structure was measured by the wafer curvature method and its unique stress characteristics were compared to that of a Cu thin film structure. The thermo-mechanical characteristics of the Cu TSV structure were correlated to microstructure evolution during thermal cycling and the local plasticity in Cu in a triaxial stress state. These findings were confirmed by microstructure analysis of the Cu vias and finite element analysis (FEA) of the stress characteristics. In addition, the local plasticity and deformation in and around individual TSVs were measured by synchrotron x-ray microdiffraction to supplement the wafer curvature measurements. The importance and implication of the local plasticity and residual stress on TSV reliabilities are discussed for TSV extrusion and device keep-out zone (KOZ).Microelectronics Research Cente

Stress-Induced Delamination Of Through Silicon Via Structures

Continuous scaling of on-chip wiring structures has brought significant challenges for materials and processes beyond the 32 nm technology node in microelectronics. Recently three-dimensional (3-D) integration with through-silicon-vias (TSVs) has emerged as an effective solution to meet the future interconnect requirement. Thermo-mechanical reliability is a key concern for the development of TSV structures used in die stacking as 3-D interconnects. This paper examines the effect of thermal stresses on interfacial reliability of TSV structures. First, the three-dimensional distribution of the thermal stress near the TSV and the wafer surface is analyzed. Using a linear superposition method, a semi-analytic solution is developed for a simplified structure consisting of a single TSV embedded in a silicon (Si) wafer. The solution is verified for relatively thick wafers by comparing to numerical results obtained by finite element analysis (FEA). Results from the stress analysis suggest interfacial delamination as a potential failure mechanism for the TSV structure. Analytical solutions for various TSV designs are then obtained for the steady-state energy release rate as an upper bound for the interfacial fracture driving force, while the effect of crack length is evaluated numerically by FEA. Based on these results, the effects of TSV designs and via material properties on the interfacial reliability are elucidated. Finally, potential failure mechanisms for TSV pop-up due to interfacial fracture are discussed.Aerospace Engineerin

Microstructure and processing effects on stress and reliability for through-silicon vias (TSVs) in 3D integrated circuits

Copper (Cu) Through-silicon via (TSV) is a key enabling element that provides the vertical connection between stacked dies in three-dimensional (3D) integration. The thermal expansion mismatch between Cu and Si induces complex stresses in and around the TSV structures, which can degrade the performance and reliability of 3DICs and are key concerns for technology development. In this dissertation, the effects of Cu microstructure and processing conditions on the stress characteristics and reliability of the TSV structure are studied. First, the stress characteristics of Cu TSV structures are investigated using the substrate curvature method. The substrate curvature measurement was supplemented by microstructure and finite element analyses (FEA) to investigate the mechanisms for the linear and nonlinear stress-temperature behaviors observed for the TSV structure. Implications of the near surface stress on carrier mobility change and device keep-out zone (KOZ) are discussed. Second, via extrusion, an important yield and reliability issue for 3D integration, is analyzed. Synchrotron x-ray microdiffraction technique was introduced for direct measurements of local stress and material behaviors in and around the TSV. Local plasticity near the top of the via was observed which provided direct experimental evidence to support the plasticity mechanism of via extrusion. An analytical model and FEA were used to analyze via extrusion based on local plasticity. Next, the effect of Cu microstructure effect on the thermomechanical behaviors of TSVs is investigated. The contribution from grain boundary and interfacial diffusion on via extrusion and the relaxation mechanisms are discussed. Potential approaches to minimize via extrusion are proposed. Finally, the stress characteristics of 3D die stack structures are studied using synchrotron x-ray microdiffraction. High resolution stress mappings were performed and verified by finite element analysis (FEA). FEA was further developed to estimate the stress effect on device mobility changes and the warpage of the integrated structure.Materials Science and Engineerin

Thermo-Mechanical Effects Of Thermal Cycled Copper Through Silicon Vias

The semiconductor industry is currently facing transistor scaling issues due to fabrication thresholds and quantum effects. In this \u27More-Than-Moore\u27 era, the industry is developing new ways to increase device performance, such as stacking chips for three-dimensional integrated circuits (3D-IC). The 3D-IC\u27s superior performance over their 2D counterparts can be attributed to the use of vertical interconnects, or through silicon vias (TSV). These interconnects are much shorter, reducing signal delay. However TSVs are susceptible to various thermo-mechanical reliability concerns. Heating during fabrication and use, in conjunction with coefficient of thermal expansion mismatch between the copper TSVs and silicon substrate, create harmful stresses in the system. The purpose of this work is to evaluate the signal integrity of Cu-TSVs and determine the major contributing factors of the signal degradation upon in-use conditions. Two series of samples containing blind Cu-TSVs embedded in a Si substrate were studied, each having different types and amounts of voids from manufacturing. The samples were thermally cycled up to 2000 times using three maximum temperatures to simulate three unique in-use conditions. S11 parameter measurements were then conducted to determine the signal integrity of the TSVs. To investigate the internal response from cycling, a protocol was developed for cross-sectioning the copper TSVs. Voids were measured using scanning electron microscope and focused ion beam imaging of the cross-sections, while the microstructural evolution of the copper was monitored with electron backscattering diffraction. An increase in void area was found to occur after cycling. This is thought to be the major contributing factor in the signal degradation of the TSVs, since no microstructural changes were observed in the copper

Numerical Modeling Analysis of Wafer Warpage and Carrier Mobility Change due to Tapered Through-Silicon-Via Geometry

Three-dimensional integration is a solution that vertically stacks multiple layers of silicon chips by Through-Silicon-Vias (TSVs) to enhance the performance of microelectronic devices. The tapered TSV profile can help to overcome the technical difficulties. However, an easily overlooked issue is that tapered TSV can cause wafer warpage during the fabrication processes. Wafer warpage can cause chip misalignment and impose additional deformation. In an effort to investigate the TSV geometric effect, a large number of finite element analysis (FEA) simulations were performed to quantify the thermal stress distribution and the thermally induced curvature. It was found that the tapered geometry alone can induce significant wafer bending, which has not been reported by other researchers. The effect of taper angle, TSV radius, TSV pitch, and wafer thickness were quantitatively studied. In addition, the incorporations of anisotropic silicon property and intermediate layers between the copper TSV and silicon into the numerical models were assessed. Thermally induced stress concentration around copper TSV near the wafer surface can lead to degradation of the device performance by affecting the carrier mobility in transistors. This piezoresistivity effect can cause serious reliability concerns. The size of keep-out zone (KOZ), which is identified as a threshold of 5% carrier mobility change, was also quantified for various transistor types in different channel directions

Thermo-mechanical stress measurement and analysis in three dimensional interconnect structures

Three-dimensional (3-D) integration is effective to overcome the wiring limit imposed on device density and performance with continued scaling. The application of TSV (Through-Silicon Via) is essential for 3D IC integration. TSVs are embedded into the silicon substrate to form vertical, electrical connections between stacked IC chips. However, due to the large CTE mismatch between Silicon and Copper, thermal stresses are induced by various thermal histories from the device processing, and they have caused serious concerns regarding the thermal-mechanical reliability. Firstly, a semi-analytic approach is introduced to understand stress distributions in TSV structures. This is followed by application of finite element analysis for more accurate prediction of stress behavior according to the real geometry of the sample. The conventional Raman method is used to measure the linear combination of in-plane stress components near silicon top surface Secondly, the limitation of conventional Raman method is discussed: only certain linear combination of in-plane stress, instead of separate value for each stress components, can be obtained. Two different kinds of innovative Raman measurements have been developed and employed to study the normal stress components separately. Both of them take advantages of different laser polarization profiles to resolve the normal stress components separately based on experimental data. The top-down Raman measurements utilize so called “high NA effect” to obtain additional information, and can resolve all 3 normal stress components. Independent bending beam experiments are used to validate the results from cross-section Raman measurement on the same sample. The correlation between top-down Raman measurement and cross-section Raman measurement are investigated as well. Lastly, as a typical example of 3D IC package, a stack-die memory package is presented. Finite element analysis combined with cross-section Raman measurement and high resolution moiré interferometry were employed to investigate the thermal-mechanical reliability and chip-package interaction of the stack-die memory structure.Physic

Tunable Copper Microstructures in Blanket Films and Trenches Using Pulsed Electrodeposition

Copper interconnects in microelectronics have long been plagued with thermo-mechanical reliability issues. Control over the copper deposition process and resulting microstructure can dictate its material properties and reduce stresses as well as defects that form in the copper. In this thesis, pulse electrodeposition processing parameters were evaluated for their impact on the copper microstructure (grain size, texture, and twin density and stress state) through electron backscattering diffraction and wafer curvature measurements. Varying levels of constraint were also investigated for their effect on the copper microstructure to better understand the microstructures of more complex three-dimensional interconnects. Highly texture blanket copper films were deposited with various pulse frequencies and duty cycle, which was found to control grain size, orientation, and twin density. Higher twin densities were also observed in the films with lower residual stress. The findings from blanket film studies were carried over to trench deposited samples, where the influence of organic additives, typically used in the electrolytic bath to produce defect-free filling of advanced geometries, on the copper microstructure was studied. With the addition of organic additives, depositions produced finer grained structures with an increased contribution from the microstructure of the trench sidewall seed layer, especially with increasing trench aspect ratio. In addition, the increased constraint of the copper, resulted in larger stresses within the features and higher twin densities. The core of this dissertation demonstrated the ability to alter the resulting Cu microstructure through variations in pulse electrodeposition parameters

Methodology for analysis of TSV stress induced transistor variation and circuit performance

As continued scaling becomes increasingly difficult, 3D integration with through silicon vias (TSVs) has emerged as a viable solution to achieve higher bandwidth and power efficiency. Mechanical stress induced by thermal mismatch between TSVs and the silicon bulk arising during wafer fabrication and 3D integration, is a key constraint. In this work, we propose a complete flow to characterize the influence of TSV stress on transistor and circuit performance. First, we analyze the thermal stress contour near the silicon surface with single and multiple TSVs through both finite element analysis (FEA) and linear superposition methods. Then, the biaxial stress is converted to mobility and threshold voltage variations depending on transistor type and geometric relation between TSVs and transistors. Next, we propose an efficient algorithm to calculate circuit variation corresponding to TSV stress based on a grid partition approach. Finally, we discuss a TSV pattern optimization strategy, and employ a series of 17-stage ring oscillators using 40 nm CMOS technology as a test case for the proposed approach