1,837 research outputs found

    DESIGN AND MIXING PERFORMANCE OF PASSIVE MICROMIXERS: A CRITICAL REVIEW

    Get PDF
    This study extracts and reports notable findings on passive micromixers by conducting an exhaustive review of designs, their features, and mixing performance. The study has covered the relevant articles on passive micromixers published from 2010 to 2020. The analysis of filtered and selected articles sums up passive micromixers into four categories: designed inlets, designed mixing-channel, lamination-based, and flow obstacles-based. The prominent mixing channel categories identified in the study are split-and-recombine (SAR), convergent-divergent (C-D), and mixed (SAR, C-D, and others). Moreover, differences in mixing channel designs, number of inlets, and evaluation methods have been used in comparing the mixing performance of passive micromixers. The SAR and the obstacles-based micromixers were found to outperform the others. The designs covered in the present review show significant improvements in the mixing index. However, these studies were conducted in an isolated environment, and most of the time, their fabrication and device integration issues were ignored. The assortment and critical analysis of micromixers based on their design features and flow parameters will be helpful to researchers interested in designing new passive micromixers for microfluidic applications

    Process development using oscillatory baffled mesoreactors

    Get PDF
    PhD ThesisThe mesoscale oscillatory baffled reactor (meso-OBR) is a flow chemistry platform whose niche is the ability to convert long residence time batch processes to continuous processes. This reactor can rapidly screen reaction kinetics or optimise a reaction in flow with minimal waste. In this work, several areas were identified that could be addressed to broaden the applicability of this platform. Four main research themes were subsequently formulated and explored: (I) development of deeper understanding of the fluid mechanics in meso-OBRs, (II) development of a new hybrid heat pipe meso-OBR for improved thermal management, (III) further improvement of continuous screening using meso-OBRs by removing the solvent and employing better experiment design methodologies, and (IV) exploration of 3D printing for rapid reactor development. I. The flow structures in a meso-OBR containing different helical baffle geometries were studied using computational fluid dynamics simulations, validated by particle image velocimetry (PIV) experiments for the first time. It was demonstrated, using new quantification methods for the meso-OBR, that when using helical baffles swirling is responsible for providing a wider operating window for plug flow than other baffle designs. Further, a new flow regime resembling a Taylor-Couette flow was discovered that further improved the plug flow response. This new double vortex regime could conceivably improve multiphase mixing and enable flow measurements (e.g. using thermocouples inside the reactor) to be conducted without degrading the mixing condition. This work also provides a new framework for validating simulated OBR flows using PIV, by quantitatively comparing turbulent flow features instead of qualitatively comparing average velocity fields. II. A new hybrid heat pipe meso-OBR (HPOBR) was prototyped to provide better thermal control of the meso-OBR by exploiting the rapid and isothermal properties of the heat pipe. This new HPOBR was compared with a jacketed meso-OBR (JOBR) for the thermal control of an exothermic imination reaction conducted without a solvent. Without a solvent or thermal control scheme, this reaction exceeded the boiling point of one of the reactants. A central composite experiment design explored the effects of reactant net flow rate, oscillation intensity and cooling capacity on the thermal and chemical response of the reaction. The HPOBR was able to passively control the temperature below the boiling point of the reactant at all conditions through heat spreading. Overall, a combined 260-fold improvement in throughput was demonstrated compared to a reactor requiring the use of a solvent. Thus, this ii wholly new reactor design provides a new approach to achieving green chemistry that could be theoretically easily adapted to other reactions. III. Analysis of in situ Fourier transform infrared (FTIR) spectroscopic data also suggested that the reaction kinetics of this solventless imination case study could be screened for the first time using the HPOBR and JOBR. This was tested by applying flow-screening protocols that adjusted the reactant molar ratio, residence time, and temperature in a single flow experiment. Both reactor configurations were able to screen the Arrhenius kinetics parameters (pre-exponential factors, activation energies, and equilibrium constants) of both steps of the imination reaction. By defining experiment conditions using design of experiments (DoE) methodologies, a theoretical 70+% reduction in material usage/time requirement for screening was achieved compared to the previous state-of-the-art screening using meso-OBRs in the literature. Additionally, it was discovered that thermal effects on the reaction could be inferred by changing other operating conditions such as molar ratio and residence time. This further simplifies the screening protocols by eliminating the need for active temperature control strategies (such as a jacket). IV. Finally, potential application areas for further development of the meso-OBR platform using 3D printing were devised. These areas conformed to different “hierarchies” of complexity, from new baffle structures (simplest) to entirely new methods for achieving mixing (most complex). This latter option was adopted as a case study, where the passively generated pulsatile flows of fluidic oscillators were tested for the first time as a means for improving plug flow. Improved plug flow behaviour was indeed demonstrated in three different standard reactor geometries (plain, baffled and coiled tubes), where it could be inferred that axial dispersion was decoupled from the secondary flows in an analogous manner to the OBR. The results indicate that these devices could be the basis for a new flow chemistry platform that requires no moving parts, which would be appealing for various industrial applications. It is concluded that, for the meso-OBR platform to remain relevant in the next era of tailor-made reactors (with rapid uptake of 3D printing), the identified areas where 3D printing could benefit the meso-OBR should be further explored

    On the design and simulation of an airlift loop bioreactor with microbubble generation by fluidic oscillation

    Get PDF
    Microbubble generation by a novel fluidic oscillator driven approach is analyzed, with a view to identifying the key design elements and their differences from standard approaches to airlift loop bioreactor design. The microbubble generation mechanism has been shown to achieve high mass transfer rates by the decrease of the bubble diameter, by hydrodynamic stabilization that avoids coalescence increasing the bubble diameter, and by longer residence times offsetting slower convection. The fluidic oscillator approach also decreases the friction losses in pipe networks and in nozzles/diffusers due to boundary layer disruption, so there is actually an energetic consumption savings in using this approach over steady flow. These dual advantages make the microbubble generation approach a promising component of a novel airlift loop bioreactor whose design is presented here. The equipment, control system for flow and temperature, and the optimization of the nozzle bank for the gas distribution system are presented. (C) 2009 The Institution of Chemical Engineers. Published by Elsevier B.V All rights reserved

    Analysis, Design and Fabrication of Micromixers, Volume II

    Get PDF
    Micromixers are an important component in micrototal analysis systems and lab-on-a-chip platforms which are widely used for sample preparation and analysis, drug delivery, and biological and chemical synthesis. The Special Issue "Analysis, Design and Fabrication of Micromixers II" published in Micromachines covers new mechanisms, numerical and/or experimental mixing analysis, design, and fabrication of various micromixers. This reprint includes an editorial, two review papers, and eleven research papers reporting on five active and six passive micromixers. Three of the active micromixers have electrokinetic driving force, but the other two are activated by mechanical mechanism and acoustic streaming. Three studies employs non-Newtonian working fluids, one of which deals with nano-non-Newtonian fluids. Most of the cases investigated micromixer design

    A Review of Recent Passive Heat Transfer Enhancement Methods

    Full text link
    [EN] Improvements in miniaturization and boosting the thermal performance of energy conservation systems call for innovative techniques to enhance heat transfer. Heat transfer enhancement methods have attracted a great deal of attention in the industrial sector due to their ability to provide energy savings, encourage the proper use of energy sources, and increase the economic efficiency of thermal systems. These methods are categorized into active, passive, and compound techniques. This article reviews recent passive heat transfer enhancement techniques, since they are reliable, cost-effective, and they do not require any extra power to promote the energy conversion systems' thermal efficiency when compared to the active methods. In the passive approaches, various components are applied to the heat transfer/working fluid flow path to improve the heat transfer rate. The passive heat transfer enhancement methods studied in this article include inserts (twisted tapes, conical strips, baffles, winglets), extended surfaces (fins), porous materials, coil/helical/spiral tubes, rough surfaces (corrugated/ribbed surfaces), and nanofluids (mono and hybrid nanofluids).Ajarostaghi, SSM.; Zaboli, M.; Javadi, H.; Badenes Badenes, B.; Urchueguía Schölzel, JF. (2022). A Review of Recent Passive Heat Transfer Enhancement Methods. Energies. 15(3):1-55. https://doi.org/10.3390/en1503098615515

    Fluid technology (selected components, devices, and systems): A compilation

    Get PDF
    Developments in fluid technology and hydraulic equipment are presented. The subjects considered are: (1) the use of fluids in the operation of switches, amplifiers, and servo devices, (2) devices and data for laboratory use in the study of fluid dynamics, and (3) the use of fluids as controls and certain methods of controlling fluids

    Experimental study of helical milling on CFRP (carbon fibre reinforced polymer) for the hole making process

    Get PDF
    Generate borehole by helical milling process may be used effectively since accurate location of the hole may be secured by means of the feed screw graduations. Fiber delamination which is the main defect occurred during hole making process on carbon fiber reinforced polymer (CFRP) were investigate throughout an experimental study. Effects of thrust force (Fz), delamination factor (Fd) and surface roughness are evaluated. Objective of the experiment are to find best cutting parameter and tool design suitable to performed helical milling operation on CFRP. Two types of end mill with 4 flutes were used and results are evaluated. It was found that tool design 2-1 has higher performance on CFRP

    Advanced flow technologies for the controlled & continuous manufacture of nanoscale materials

    Get PDF
    Batch processes have been successfully used in the process industry over two centuries. However, changing customer demands and discovery of novel products have led the scientists and engineers to develop new manufacturing methods for the process industry. High-value products such as nanomaterials, smart and functional materials require precise process control for the entire product. Controlling of particle size and shape becomes more difficult in the large scale batch processes. Therefore, over the past few decades, there has been an increasing interest in the flow processing techniques due to their inherent benefits, such as better heat and mass transfer and small control volumes. Continuous Oscillatory Baffled Reactor (COBR) is a novel type of flow reactor. COBR combines oscillatory motion and periodically placed baffled flow channels to generate plug flow conditions, providing better mixing control similar to microreactors. Plug flow conditions can be achieved with the combination of optimum net flow, oscillatory amplitude and frequency using COBRs. With this new reactor and mixing concept, high-value products can be manufactured more efficiently using uniform mixing conditions and better temperature control. This will decrease the reaction time and production cost of novel products, use less energy, and increase time-to-market of novel products. The aim of this research is to develop a scalable and continuous manufacturing platform using continuous oscillatory baffled reactors to produce high-value products in low cost. The focus of this study includes developing modular oscillatory baffled reactors, characterisation of modular oscillatory baffled reactors using experimental methods, developing scale-up methodology from laboratory scale to industrial production size and demonstration of nanomaterial synthesis using modular oscillatory flow reactor...[cont.]Manufacturin

    Flow distribution and heat transfer coefficients inside gas holes discharging

    Get PDF
    Fluid flow and heat transfer coefficient associated with flow inside short holes (L/D=1) discharging orthogonally into a crossflow was investigated experimentally and numerically for (Re) Ě… ranging from 0.5Ă—105 to 2Ă—105, and blowing ratio ranging from 1.3 to 3.2. The basic configuration studied consists of a feed tube with five orthogonally located gas holes. Four different hole configurations were studied. The transient heat transfer study employs an IR-camera to determine the local heat transfer coefficient inside each hole. Velocity measurements and numerical flow simulation were used to better understand the measured heat transfer distribution inside the hole. The Nusselt number distribution along the hole surface exhibits significant circumferential non-uniformity associated with impingement and separation, with localized high heat transfer regions caused by flow impingement. The heat transfer coefficient was observed to be a strong function of the Reynolds number, but a weak function of the blowing ratio. Moreover, Fluid flow and heat transfer coefficient inside gas holes was improved by changing the plenum geometry for (Re) Ě…=1.7Ă—105, and blowing ratio of 2.65. To improve the flow structure understanding inside plenum and gas holes, numerical simulation using FLUENT code was employed and verified by experimental measurements. Heat Transfer coefficient contour maps inside gas holes was measured experimentally using IR-camera thermography to investigate the effect of plenum geometry modifications on thermal stresses generated inside gas holes. Results indicate that placing straight baffles at the upstream of cooling holes inlet inside the plenum eliminates vortex generation in the gas holes for H/S=1. The recirculation bubble at the back of each baffle guides air to flow smoothly into cooling holes. Also, by varying baffle height, plenum mass flow rate can be distributed evenly among all gas holes

    High Temperature Heat Exchanger Project: Quarterly Progress Report April 1, 2007 through June 30, 2007

    Full text link
    • Ceramatec Sulfuric Acid Decomposer. Modeling with different reacting flow channel configurations (ribbed-surface channels, hexagonal channels, and diamond-shaped channels) was performed. The probability of failure for the one channel geometry with different reacting flow channel configurations was calculated to be zero in the three principal directions for all of the cases. • Bayonet Heat Exchanger. The Matlab code for calculating the probability of failure using a two-dimensional axisymmetric model of the bayonet decomposer was developed. The probability of failure was calculated for the inner and outer SiC walls, and the intermediate quartz wall of the decomposer and found to be zero for all of the walls. The exact temperatures of the external wall measured from the experiment at SNL were applied to the thermal boundary conditions and used to calculate flow, heat transfer and chemical reactions. Geometry of one-fourth of the packed bed region with cylindrical and spherical pellets was created, and the periodic boundary conditions were applied. Calculations of fluid flow and heat transfer with cylindrical and spherical pellets in the packed bed region were performed
    • …
    corecore