Fault location and diagnosis in a medium voltage EPR power cable

This paper presents a case study on fault location, characterization and diagnosis in a length of shielded 11 kV medium voltage ethylene-propylene rubber (EPR) power cable. The defect was identified on-site as a low resistance fault occurring between the sheath and the core. A 43 m section was removed for further analysis. The fault resistance was characterized and the location of the defect pinpointed to within a few cm using a combination of time-difference-of-arrival location and infra-red imaging. A combination of X-ray computed tomography, scanning electron microscopy and energy dispersive X-ray spectroscopy were then applied to characterize any abnormalities in the dielectric surrounding the breakdown region. A significant number of high density contaminants were found to be embedded in the dielectric layer, having an average diameter of the order of 100 um, a maximum diameter of 310 um and an average density of 1 particle per 2.28 mm3 . Scanning electron microscopy and energy-dispersive X-ray spectroscopy were used to determine the geometry and elemental composition of some initial contaminant samples. It was concluded that contamination of the EPR layer, combined with an observed eccentricity of the cable’s core and sheath resulting in a reduced insulation gap, may have led to an electric field concentration in the region of the defect sufficient to initiate breakdown. Preventative strategies are discussed for similar families of cables, including more stringent dielectric testing requirements at the manufacturing stage and PD monitoring to detect incipient failure

Quantitative micro-luminescence and related studies of fine and/or glassy lunar surface materials

Papers on Raman and soft X-ray spectroscopy of lunar glasses and electron microscopy of lunar fines are presented. Individual particles of glasses from Apollo 11, 12, 14, and 15 samples were analyzed separately. Silicon emission shifts vary between parent rock types and can be interpreted as a range of Si-O distances from 1.612 to 1.637 A. Aluminum emission shifts relate to the amount of 4- and 6-coordinated Al in the glass. Raman spectra show broadened bands. Certain bands recur in many specimens and relate to the main normative minerals for the glass bulk composition, olivine, pyroxene, and anorthite. Quantitative size and shape analyses were carried out on six Apollo 14 and 15 samples of fines by computer evaluation of scanning electron microspace images. For the size range of 0.50 to 30 micron diameter, the distributions are log-normal on a number count basis. Aspect ratios range from 0.1 to 1.0 with an average value of about 0.6. The aspect ratios and a shape complexity factor vary only slightly among the samples

Secondary Electron Imaging in the Scanning Transmission Electron Microscope

The detailed correlation of surface morphology and subsurface microstructure has been made possible by the scanning transmission electron microscope. This instrument provides the capability for simultaneous and independent secondary electron and transmitted electron imaging from the same sample area. This includes the ability to generate mixed secondary/transmitted electron images, which form a concise visual presentation of the information in the two component images. Correlative surface and through-volume specimen examination of this type has most frequently been applied to backthinned samples, which are specifically prepared in a way which produces electron-transparent material in the immediate vicinity of a surface of interest on the original bulk sample. However, the technique has also been found to be useful for relating local microstructural features to the overall structure of the sample, and for determining the local specimen geometry for microanalysis by energy dispersive x-ray spectrometry. The formation of a mixed secondary/transmitted electron image also serves as a novel means of signal processing which reduces the difficulty of forming a transmitted image from regions adjacent to the edges of a thin foil sample

Particulate airborne impurities

The cumulative effects of air pollutants are of principal concern in research on environmental protection in Sweden. Post-industrial society has imposed many limits on emitted air pollutants, yet the number of reports on the negative effects from them is increasing, largely due to human activity in the form of industrial emissions and increased traffic flows. Rising concerns over the health effects from airborne particulate matter (PM) stem from in vitro, in vivo, and cohort studies revealing effects of mostly negative nature. Full insight into the health effects from PM can only be achieved through practical investigation of the mode of toxicity from distinct types of particles and requires techniques for their identification, monitoring, and the production of model fractions for health studies. To this effect, comprehensive collection and chemical analysis of particulates at the origin of emission was performed in order to provide clearer insight into the nature of the particulates at exposure and add detail to aid risk assessment. Methods of capturing particles and analyzing their chemical nature were devised using scanning electron microscopy coupled with energy dispersive spectroscopy (SEM-EDS). Furthermore, taking the approach of in vitro cytotoxicity testing, nanoparticles of types typical to automotive emissions, were synthesized and extensively characterized using SEM-EDS, X-ray diffraction (XRD), transmission electron microscopy (TEM),dynamic light scattering (DLS), and nanoparticle tracking analysis (NTA). The produced model magnetite and palladium nanoparticles were found to induce toxicity in human pulmonary epithelial cells (A549 and PBEC) as well as impact severely on immunological and renal cells (221 B- and 293T-cells) in a dose-dependent manner

Corrosion-fatigue interactions of high-temperature nickel alloys

Corrosion and fatigue aspects of high temperature turbine components made from Alloy 720Li and RR1000 have been studied with a view to understanding the potential failure mechanisms occurring in these materials. Understanding of such failure mechanisms is important in order to make safety improvements and significant cost savings by reducing engine downtime. Some exservice discs currently exhibit pit-like features at a specific location on the firtree lobes, which potentially may lead to more serious alloy fissuring. Shot peening is currently employed to improve fatigue resistance at the surface of components. This work aims to fully characterise these pits and fissure features in addition to shot peening, and the components in general, using advanced analytical techniques, in order that the failure mechanism(s) can be determined and mitigated against. [Continues.

New techniques for imaging and analyzing lung tissue.

The recent technological revolution in the field of imaging techniques has provided pathologists and toxicologists with an expanding repertoire of analytical techniques for studying the interaction between the lung and the various exogenous materials to which it is exposed. Analytical problems requiring elemental sensitivity or specificity beyond the range of that offered by conventional scanning electron microscopy and energy dispersive X-ray analysis are particularly appropriate for the application of these newer techniques. Electron energy loss spectrometry, Auger electron spectroscopy, secondary ion mass spectrometry, and laser microprobe mass analysis each offer unique advantages in this regard, but also possess their own limitations and disadvantages. Diffraction techniques provide crystalline structural information available through no other means. Bulk chemical techniques provide useful cross-checks on the data obtained by microanalytical approaches. It is the purpose of this review to summarize the methodology of these techniques, acknowledge situations in which they have been used in addressing problems in pulmonary toxicology, and comment on the relative advantages and disadvantages of each approach. It is necessary for an investigator to weigh each of these factors when deciding which technique is best suited for any given analytical problem; often it is useful to employ a combination of two or more of the techniques discussed. It is anticipated that there will be increasing utilization of these technologies for problems in pulmonary toxicology in the decades to come