Index to NASA Tech Briefs, 1975

This index contains abstracts and four indexes--subject, personal author, originating Center, and Tech Brief number--for 1975 Tech Briefs

The NASA SBIR product catalog

The purpose of this catalog is to assist small business firms in making the community aware of products emerging from their efforts in the Small Business Innovation Research (SBIR) program. It contains descriptions of some products that have advanced into Phase 3 and others that are identified as prospective products. Both lists of products in this catalog are based on information supplied by NASA SBIR contractors in responding to an invitation to be represented in this document. Generally, all products suggested by the small firms were included in order to meet the goals of information exchange for SBIR results. Of the 444 SBIR contractors NASA queried, 137 provided information on 219 products. The catalog presents the product information in the technology areas listed in the table of contents. Within each area, the products are listed in alphabetical order by product name and are given identifying numbers. Also included is an alphabetical listing of the companies that have products described. This listing cross-references the product list and provides information on the business activity of each firm. In addition, there are three indexes: one a list of firms by states, one that lists the products according to NASA Centers that managed the SBIR projects, and one that lists the products by the relevant Technical Topics utilized in NASA's annual program solicitation under which each SBIR project was selected

High-temperature infrared emissivity of materials for alternative energy applications

xxv, 171 p.La emisividad es una propiedad termofísica que relaciona la cantidad de radiación térmica que emite un material con la radiada por un cuerpo negro. Se trata de una propiedad de gran importancia en ámbitos industriales y científicos, ya que condiciona las transferencias de calor en situaciones de alta temperatura o alto vacío. La presente tesis se divide en dos apartados fundamentales: por una parte, el desarrollo y mejora de métodos de medida de emisividad y, por otra, la aplicación de dichos métodos a la caracterización de materiales de interés industrial en el sector de las energías alternativas (solar térmica y nuclear de fusión). En primer lugar, se ha llevado a cabo una profunda revisión del aparato singular de medida de emisividad en la UPV/EHU, incluyendo mejoras instrumentales y metodológicas, así como un renovado análisis de sus fuentes de error. En segundo lugar, se han estudiado tres tipos de materiales: absorbentes solares selectivos multicapa para centrales solares térmicas de tubo, recubrimientos negros no selectivos para centrales de torre y una familia de aleaciones de vanadio para futuros reactores nucleares de fusión. El objetivo global de este trabajo es mejorar nuestro conocimiento sobre las propiedades de transferencia de calor por radiación de materiales clave para estos procesos energéticos alternativo

Advances in Plastic Forming of Metals

The forming of metals through plastic deformation comprises a family of methods that produce components through the re-shaping of input stock, oftentimes with little waste. Therefore, forming is one of the most efficient and economical manufacturing process families available. A myriad of forming processes exist in this family. In conjunction with their countless existing successful applications and their relatively low energy requirements, these processes are an indispensable part of our future. However, despite the vast accumulated know-how, research challenges remain, be they related to the forming of new materials (e.g., for light-weight transportation applications), pushing the boundaries of what is doable, reducing the intermediate steps and/or scrap, or further enhancing the environmental friendliness. The purpose of this book is to collect expert views and contributions on the current state-of-the-art of plastic forming, thus highlighting contemporary challenges and offering ideas and solutions

Precise nanoscale characterisation of novel Heusler thermoelectrics via analytical electron microscopy

Thermoelectric power generation presents an opportunity to `scavenge' energy that would otherwise be wasted as heat. Heusler alloys, a class of materials often comprising inexpensive, non-toxic elements, are promising for practical use in a new generation of thermoelectric devices. Recently, efficient thermoelectric Heusler alloys have overcome a performance-limiting thermal conductivity through the introduction of nanostructures that scatter phonons and impede thermal transport. However, the nature and stability of nanostructures can be difficult to discern, especially the minor compositional variations that derive from inhomogeneous phase segregation. Throughout this thesis TiNiSn, which forms the basis for some of the most promising n-type half-Heusler thermoelectrics, is studied through a unique combination of elemental and diffractive analysis in the scanning transmission electron microscope (STEM). Epitaxial thin films of TiNiSn are grown by pulsed laser deposition and FIB-prepared cross-sections of these are characterised in STEM with a focus on aberration-corrected STEM-EELS spectrum imaging and scanning precession electron diffraction (SPED), yielding precise chemical and structural quantification with nanoscale spatial resolution. The results throughout this thesis demonstrate the importance of STEM for quantitative studies of thermoelectric materials, as it can provide the analytical precision required for accurate identification of minority phases in TiNiSn specimens that would otherwise be overlooked in bulk analytical techniques. Sensitivity to very small elemental concentrations is a cornerstone of the use of STEM-EELS for chemical characterisation. Precisions of 0.3 % were achieved through adoption and development of refined, reference-based, absolute elemental quantification protocols which were essential in overcoming difficulties with large uncertainties posed by conventional methods. The success of this approach, in part, is due to advances made in characterisation of experimental conditions including, for the first time, an automated, standard-less approach to the measurement and correction of energy dispersion non-uniformities. Dispersion correction enables reliable, absolute calibration of energy-loss in spectra to yield a precision better than 0.1 eV. These developments in STEM-EELS were then used in three investigations of TiNiSn thin films exploring aspects of nanostructuring, phase segregation and crystrallographic strain and coherency. We discovered the spontaneous formation of nanostructures during thin film growth, gaining some insight into the phase segregation mechanisms that lead to their nucleation. Novel in situ STEM studies of phase segregation facilitated direct observations of the thermal evolution of nanoscale phases and results enabled characterisation of diffusion rates of Ni migration between full- and half-Heusler phases, for which the activation energy was calculated as 0.3~eV. Combining SPED with advances in detector technology, STEM structural investigations highlighted an interesting strain texture associated with nanostructuring of the half-Heusler thin films. Finally, combining SPED results with STEM-EELS measurements is proposed as a route to `correlative-STEM' analysis, which unifies nanoscale chemical and structural information for greater insights into the impact of nanostructures in thermoelectrics