Techniques for In Situ Monitoring the Performance of Organic Coatings and Their Applicability to the Pre-Finished Steel Industry: A Review

A review is carried out in this paper into techniques that currently exist for, of have the potential to be used for, monitoring the performance of organic coating. Specific attention is paid to the applicability of each method to pre-finished steel used in the construction industry as these are rarely monitored in situ and their expected performance is often only estimated from lab-based accelerated corrosion testing. Monitoring could allow more accurate estimates of building cladding lifespan and required maintenance schedules; provide customers with active performance data; additionally, with a better understanding of performance, more appropriate coatings or coating weights could be selected for a construction project, offering economic benefits as part of smart building developments. An introduction to coatings, their use for corrosion protection, failure mechanisms, and relevant monitoring techniques is given before current assessment techniques are described in terms of their working principles. Examples of recent work are presented for the techniques that have been investigated for monitoring or directly relatable purposes. The review concludes that there are several good reasons why an optimum corrosion monitoring technology does not currently exist, however, promising research is emerging in the field of wireless and embedded sensor design which is providing optimistic results

Development of sensors and non-destructive techniques to determine the performance of coatings in construction

The primary objective of this work was to examine and develop techniques for monitoring the degradation of Organically Coated Steel (OCS) in-situ. This included the detection of changes associated with the weathering to both the organic coating and metallic substrate. Initially, a review of current promising techniques was carried out however many were found to be unsuitable for this application and the adaptation of current techniques and the development of new techniques was considered. A brief concept investigation, based on initial testing and considerations, was used to determine a number of sensing techniques to examine. These included embedded, Resonant Frequency Identification (RFID), Magnetic Flux Leakage (MFL) and dielectric sensing. Each of these techniques were assessed for the application, prototyped, and tested against a range of samples to determine the accuracy and sensitivity of degradation detection provided. A range of poorly and highly durable coated samples were used in conjunction with accelerated weathering testing for this aim. Track based electronic printed sensors were presented as both a cut edge corrosion tracking and coating capacitance measurement method. While suffering somewhat from electrical paint compatibility issues both concepts showed merit in initial trials however the capacitive sensor ultimately proved insufficiently responsive to coating changes. The embedded, progressive failure-based, cut edge corrosion sensor was produced and tested in modern coating systems with moderate success. Novel applications of RFID and MLF techniques were considered and proved capable of detecting large changes in substrate condition due to significant corrosion. However, there was a lack of sufficient sensitivity when considering early-stage corrosion of durable modern OCS products. Finally, it was shown that a chipless antenna could be designed and optimised for novelly monitoring the changes to the dielectric properties of a paint layer due to degradation. However, ultimately this test, due to equipment requirements, lent itself more to lab testing than in-situ. Due to some of these limitations a different approach was considered in which the environmental factors influencing degradation were examined with the aim of relating these to performance across a building. It was observed that a combination of high humidity and the build-up of aggressive natural deposits contributed to high degradation rates in sheltered regions, such as building eaves, where microclimates were created. The build-up of deposits and their effect was presented as a key degradation accelerant during in-use service. A unique numerical simulation approach was developed to predict the natural washing, via rain impact and characteristics of the building analysed. This approach showed promise for determining areas unlikely to be naturally washed, and therefore subjected to a degradation accelerating, build-up of deposits. Given these understandings coated wetness sensors were considered as a realistic live-monitoring device capable of determining deposit build up and ultimately OCS lifetime

Development of Non-Destructive Testing by Eddy Currents for Highly Demanding Engineering Applications

Defect detection with Non-Destructive Testing (NDT) is essential in accidents prevention, requiring R&TD to generate new scientific and procedural knowledge for new products with high safety requirements. A current challenge lies in the detection of surface and sub-surface micro defects with NDT by Eddy Currents (EC). The main objective of this work was the development of applied research, technological innovation and experimental validation of EC customized systems for three highly demanding inspection scenarios: micro defects in tubular geometries; brazed joints for the automotive industry; and high-speed moving composite materials. This objective implied starting from the scientific fundamentals of NDT by EC to design and simulate EC probes and the prototypes developed were tested in industrial environment, reaching a TRL ≈ 5. Another objective, of a more scientific and disruptive nature, was to test a new technique for the creation of EC in the materials to be inspect, named Magnetic Permeability Pattern Substrate (MPPS). This technique consists on the development of substrates/films with patterns of different magnetic permeabilities rather than the use of excitation bobbin coils or filaments of complex geometry. The experimental results demonstrated that the prototypes developed for the three industrial applications studied outperformed the state of the art, allowing the detection of target defects with a very good signal-to-noise ratio: in tubular geometries defects with depth of 0.5 mm and thickness of 0.2 mm in any scanning position; in the laser brazed weld beads pores with 0.13 mm diameter and internal artificial defects 1 mm from the weld surface; in composite materials defects under 1 mm at speeds up to 4 m/s and 3 mm lift-off. The numerical simulations assisted the probe design, allowing to describe and characterize electrical and magnetic phenomena. The new MPPS concept for the introduction of EC was validated numerically and experimentally

Passive low frequency RFID for non-destructive evaluation and monitoring

Ph. D ThesisDespite of immense research over the years, defect monitoring in harsh environmental conditions still presents notable challenges for Non-Destructive Testing and Evaluation (NDT&E) and Structural Health Monitoring (SHM). One of the substantial challenges is the inaccessibility to the metal surface due to the large stand-off distance caused by the insulation layer. The hidden nature of corrosion and defect under thick insulation in harsh environmental conditions may result in it being not noticed and ultimately leading to failures. Generally electromagnetic NDT&E techniques which are used in pipeline industries require the removal of the insulation layer or high powered expensive equipment. Along with these, other limitations in the existing techniques create opportunities for novel systems to solve the challenges caused by Corrosion under Insulation (CUI). Extending from Pulsed Eddy Current (PEC), this research proposes the development and use of passive Low Frequency (LF) RFID hardware system for the detection and monitoring of corrosion and cracks on both ferrous and non-ferrous materials at varying high temperature conditions. The passive, low cost essence of RFID makes it an enchanting technique for long term condition monitoring. The contribution of the research work can be summarised as follows: (1) implementation of novel LF RFID sensor systems and the rig platform, experimental studies validating the detection capabilities of corrosion progression samples using transient feature analysis with respect to permeability and electrical conductivity changes along with enhanced sensitivity demonstration using ferrite sheet attached to the tag; (2) defect detection using swept frequency method to study the multiple frequency behaviour and further temperature suppression using feature fusion technique; (3) inhomogeneity study on ferrous materials at varying temperature and demonstration of the potential of the RFID system; (4) use of RFID tag with ceramic filled Poly-tetra-fluoro-ethyulene (PTFE) substrate for larger applicability of the sensing system in the industry; (5) lift-off independent defect monitoring using passive sweep frequency RFID sensors and feature extraction and fusion for robustness improvement. This research concludes that passive LF RFID system can be used to detect corrosion and crack on both ferrous and non-ferrous materials and then the system can be used to compensate for temperature variation making it useful for a wider range of applications. However, significant challenges such as permanent deployment of the tags for long term monitoring at higher temperatures and much higher standoff distance, still require improvement for real-world applicability.Engineering and Physical Sciences Research Council (EPSRC) CASE, National Nuclear Laboratory (NNL)

Index to 1981 NASA Tech Briefs, volume 6, numbers 1-4

Short announcements of new technology derived from the R&D activities of NASA are presented. These briefs emphasize information considered likely to be transferrable across industrial, regional, or disciplinary lines and are issued to encourage commercial application. This index for 1981 Tech Briefs contains abstracts and four indexes: subject, personal author, originating center, and Tech Brief Number. The following areas are covered: electronic components and circuits, electronic systems, physical sciences, materials, life sciences, mechanics, machinery, fabrication technology, and mathematics and information sciences