21,994 research outputs found

    A portable MBE system for in situ X-Ray investigations at synchrotron beamlines

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    A portable synchrotron MBE system is designed and applied for in situ investigations. The growth chamber is equipped with all the standard MBE components such as effusion cells with shutters, main shutter, cooling shroud, manipulator, RHEED setup and pressure gauges. The characteristic feature of the system is the beryllium windows which are used for in situ x-ray measurements. An UHV sample transfer case allows in-vacuo transfer of samples prepared elsewhere. We describe the system design and demonstrate it's performance by investigating the annealing process of buried InGaAs self organized quantum dots

    Review on the development of truly portable and in-situ capillary electrophoresis systems

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    Capillary electrophoresis (CE) is a technique which uses an electric field to separate a mixed sample into its constituents. Portable CE systems enable this powerful analysis technique to be used in the field. Many of the challenges for portable systems are similar to those of autonomous in-situ analysis and therefore portable systems may be considered a stepping stone towards autonomous in-situ analysis. CE is widely used for biological and chemical analysis and example applications include: water quality analysis; drug development and quality control; proteomics and DNA analysis; counter-terrorism (explosive material identification) and corrosion monitoring. The technique is often limited to laboratory use, since it requires large electric fields, sensitive detection systems and fluidic control systems. All of these place restrictions in terms of: size, weight, cost, choice of operating solutions, choice of fabrication materials, electrical power and lifetime. In this review we bring together and critique the work by researchers addressing these issues. We emphasize the importance of a holistic approach for portable and in-situ CE systems and discuss all the aspects of the design. We identify gaps in the literature which require attention for the realization of both truly portable and in-situ CE systems

    Deposition of particle pollution in turbulent forced-air cooling

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    Rotating fans are the prevalent forced cooling method for heat generating equipment and buildings. As the concentration of atmospheric pollutants has increased, the accumulation of microscale and nanoscale particles on surfaces due to advection-diffusion has led to adverse mechanical, chemical and electrical effects that increase cooling demands and reduce the reliability of electronic equipment. Here, we uncover the mechanisms leading to enhanced deposition of particle matter (PM10_{10} and PM2.5_{2.5}) on surfaces due to turbulent axial fan flows operating at Reynolds numbers, Re105Re \sim 10^5. Qualitative observations of long-term particle deposition from the field were combined with \textit{in situ} particle image velocimetry on a telecommunications base station, revealing the dominant role of impingement velocity and angle. Near-wall momentum transport for 10<y+<5010 < y^+ < 50 were explored using a quadrant analysis to uncover the contributions of turbulent events that promote particle deposition through turbulent diffusion and eddy impaction. By decomposing these events, the local transport behaviour of fine particles from the bulk flow to the surface has been categorised. The transition from deposition to clean surfaces was accompanied by a decrease in shear velocity, turbulent stresses, and particle sweep motions with lower flux in the wall-normal direction. Finally, using these insights, selective filtering of coarse particles was found to promote the conditions that enhance the deposition of fine particle matter

    Global meteorological data facility for real-time field experiments support and guidance

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    A Global Meteorological Data Facility (GMDF) has been constructed to provide economical real-time meteorological support to atmospheric field experiments. After collection and analysis of meteorological data sets at a central station, tailored meteorological products are transmitted to experiment field sites using conventional ground link or satellite communication techniques. The GMDF supported the Global Tropospheric Experiment Amazon Boundary Layer Experiment (GTE-ABLE II) based in Manaus, Brazil, during July and August 1985; an arctic airborne lidar survey mission for the Polar Stratospheric Clouds (PSC) experiment during January 1986; and the Genesis of Atlantic Lows Experiment (GALE) during January, February and March 1986. GMDF structure is similar to the UNIDATA concept, including meteorological data from the Zephyr Weather Transmission Service, a mode AAA GOES downlink, and dedicated processors for image manipulation, transmission and display. The GMDF improved field experiment operations in general, with the greatest benefits arising from the ability to communicate with field personnel in real time

    High heat flux measurements and experimental calibrations/characterizations

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    Recent progress in techniques employed in the measurement of very high heat-transfer rates in reentry-type facilities at the Arnold Engineering Development Center (AEDC) is described. These advances include thermal analyses applied to transducer concepts used to make these measurements; improved heat-flux sensor fabrication methods, equipment, and procedures for determining the experimental time response of individual sensors; performance of absolute heat-flux calibrations at levels above 2,000 Btu/cu ft-sec (2.27 kW/cu cm); and innovative methods of performing in-situ run-to-run characterizations of heat-flux probes installed in the test facility. Graphical illustrations of the results of extensive thermal analyses of the null-point calorimeter and coaxial surface thermocouple concepts with application to measurements in aerothermal test environments are presented. Results of time response experiments and absolute calibrations of null-point calorimeters and coaxial thermocouples performed in the laboratory at intermediate to high heat-flux levels are shown. Typical AEDC high-enthalpy arc heater heat-flux data recently obtained with a Calspan-fabricated null-point probe model are included

    Mobile spectroscopic instrumentation in archaeometry research

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    Mobile instrumentation is of growing importance to archaeometry research. Equipment is utilized in the field or at museums, thus avoiding transportation or risk of damage to valuable artifacts. Many spectroscopic techniques are nondestructive and micro-destructive in nature, which preserves the cultural heritage objects themselves. This review includes over 160 references pertaining to the use of mobile spectroscopy for archaeometry. Following a discussion of terminology related to mobile instrumental methods, results of a literature survey on their applications for cultural heritage objects is presented. Sections devoted to specific techniques are then provided: Raman spectroscopy, X-ray fluorescence spectrometry, Fourier transform infrared spectroscopy, laser-induced breakdown spectroscopy, and less frequently used techniques. The review closes with a discussion of combined instrumental approaches

    Characterisation and optimisation of mobile Raman spectroscopy for art analysis

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