Magnetic transitions in Pr2NiO4 single crystal

The magnetic properties of a stoichiometric Pr2NiO4 single crystal have been examined by means of the temperature dependence of the complex ac susceptibility and the isothermal magnetization in fields up to 200 kOe at T=4.2 K. Three separate phases have been identified and their anisotropic character has been analyzed. A collinear antiferromagnetic phase appears first between TN = 325 K and Tc1 = 115 K, where the Pr ions are polarized by an internal magnetic field. At Tc1 a first modification of the magnetic structure occurs in parallel with a structural phase transition (Bmab to P42/ncm). This magnetic transition has a first‐order character and involves both the out‐of‐plane and the in‐plane spin components (magnetic modes gx and gxcyfz, respectively). A second magnetic transition having also a first‐order character is also clearly identified at Tc2 = 90 K which corresponds to a spin reorientation process (gxcyfz to cxgyaz magnetic modes). It should be noted as well that the out‐of‐phase component of χac shows a peak around 30 K which reflects the coexistence of both magnetic configurations in a wide temperature interval. Finally, two field‐induced transitions have been observed at 4.2 K when the field is directed along the c axis. We propose that the high‐field anomaly arises from a metamagnetic transition of the weak ferromagnetic component, similarly to La2CuO4

Permo-Carboniferous magmatism in the core of Pangaea (Southern Pyreness): a possible linkange between the Variscan and Cimmerian cycles?

In southern Europe and the western Mediterranean, Permo-Carboniferous magmatism is well represented in areas of Iberia, the Alps, Sardinia and the Balkan Peninsula. In Iberia, the magmatism that has been related to the Variscan orogeny is associated with syn-orogenic events at ca. 350-315 Ma and post-orogenic at ca. 310-295 Ma. In the southern Pyrenees there is Permo-Carboniferous sedimentary basins with a significant volume of rhyolitic ignimbrites and andesitic flows. The Erill Castell-Estac, Cadí and Castellar de n’Hug basins are spatially associated with the Boí, Montellá and Vielha granites and the Cardet dacitic dykes emplaced in Variscan basement rocks. U-Pb SHRIMP dating of zircons extracted from these granites, an andesitic flow, a dacitic dyke and six ignimbrites, revealed that magmatism was active from ca. 304 Ma to ca. 266 Ma. The scattering of zircon ages in each sample shows that the history of melt crystallization was prolonged and complex. The reported ages of the magmatic activity for the Southern Pyrenees in the range ca. 304-283 Ma (this study) fit in well with the time interval of magmatism related to the early North-dipping subduction of the Western Paleotethys Ocean, the subsequent development of Iberian orocline (Variscan cycle), and the large-scale bending and blocking of the Paleotethys Ocean subduction at East of Iberia.In paleogeographic reconstructions of the Permo-Carboniferous, Iberia is located in the core of Pangaea to the east of the probable Rheic Ocean suture and near the western end of the subduction zone of the Paleotethys Ocean. The emplacement in Iberia of granites with ca. 310-278 Ma age occurred after the collision of Laurussia and Gondwana, when the subduction of the Rheic Ocean was inactive. From a Variscan-cycle perspective, the Permo-Carboniferous magmatism of the Pyrenees has been considered as post-orogenic. However, global paleogeographic reconstructions put Iberia in between the Rheic Ocean suture and the still active subduction zone of the Western Paleotethys Ocean. Therefore, the Permo-Carboniferous magmatism of Iberia, from a Cimmerian-cycle perspective, may have accompanied the closing of the Paleotethys Ocean. During this stage of the evolution of Pangaea, the east of Iberia was geologically affected by the active subduction zone of the Paleotethys Ocean. The period ca. 310-285 Ma is marked by the development of an orocline that extends from Iberia to Armorica. The northwards subduction of the western corner of Paleotethys probably caused orocline formation and consequent large-scale bending and blocking of Paleotethys subduction immediately east of Iberia. The Permo-Carboniferous magmatism of Iberia, coeval with this tectonic evolution, shows a mixed imprint of subduction and delamination geochemical signatures. Although this may seem controversial, in our view the magmatic activity preserved in the Southern Pyrenees could provide the missing link between the development of the Iberian orocline and the continued subduction of easternmost segments of the Paleotethys Ocean (Cimmerian cycle) during the evolution of Pangaea

Crystal and magnetic structure of the oxypnictide superconductor LaO(1-x)FxFeAs: evidence for magnetoelastic coupling

High-resolution and high-flux neutron as well as X-ray powder-diffraction experiments were performed on the oxypnictide series LaO(1-x)FxFeAs with 0<x<0.15 in order to study the crystal and magnetic structure. The magnetic symmetry of the undoped compound corresponds to those reported for ReOFeAs (with Re a rare earth) and for AFe2As2 (A=Ba, Sr) materials. We find an ordered magnetic moment of 0.63(1)muB at 2 K in LaOFeAs, which is significantly larger than the values previously reported for this compound. A sizable ordered magnetic moment is observed up to a F-doping of 4.5% whereas there is no magnetic order for a sample with a F concentration of x=0.06. In the undoped sample, several interatomic distances and FeAs4 tetrahedra angles exhibit pronounced anomalies connected with the broad structural transition and with the onset of magnetism supporting the idea of strong magneto-elastic coupling in this material.Comment: 8 pages, 7 figures, regular articl

Millimagnitude Photometry for Transiting Extrasolar Planetary Candidates. V. Follow-up of 30 OGLE Transits. New Candidates

We used VLT/VIMOS images in the V band to obtain light curves of extrasolar planetary transits OGLE-TR-111 and OGLE-TR-113, and candidate planetary transits: OGLE-TR-82, OGLE-TR-86, OGLE-TR-91, OGLE-TR-106, OGLE-TR-109, OGLE-TR-110, OGLE-TR-159, OGLE-TR-167, OGLE-TR-170, OGLE-TR-171. Using difference imaging photometry, we were able to achieve millimagnitude errors in the individual data points. We present the analysis of the data and the light curves, by measuring transit amplitudes and ephemerides, and by calculating geometrical parameters for some of the systems. We observed 9 OGLE objects at the predicted transit moments. Two other transits were shifted in time by a few hours. For another seven objects we expected to observe transits during the VIMOS run, but they were not detected. The stars OGLE-TR-111 and OGLE-TR-113 are probably the only OGLE objects in the observed sample to host planets, with the other objects being very likely eclipsing binaries or multiple systems. In this paper we also report on four new transiting candidates which we have found in the data.Comment: 11 pages, 17 figures, accepted for publication in A&

Crystal structure and phonon softening in Ca3Ir4Sn13

We investigated the crystal structure and lattice excitations of the ternary intermetallic stannide Ca3Ir4Sn13 using neutron and x-ray scattering techniques. For T > T* ~ 38 K the x-ray diffraction data can be satisfactorily refined using the space group Pm-3n. Below T* the crystal structure is modulated with a propagation vector of q = (1/2, 1/2, 0). This may arise from a merohedral twinning in which three tetragonal domains overlap to mimic a higher symmetry, or from a doubling of the cubic unit cell. Neutron diffraction and neutron spectroscopy results show that the structural transition at T* is of a second-order, and that it is well described by mean-field theory. Inelastic neutron scattering data point towards a displacive structural transition at T* arising from the softening of a low-energy phonon mode with an energy gap of Delta(120 K) = 1.05 meV. Using density functional theory the soft phonon mode is identified as a 'breathing' mode of the Sn12 icosahedra and is consistent with the thermal ellipsoids of the Sn2 atoms found by single crystal diffraction data

Entropy calculation for a toy black hole

In this note we carry out the counting of states for a black hole in loop quantum gravity, however assuming an equidistant area spectrum. We find that this toy-model is exactly solvable, and we show that its behavior is very similar to that of the correct model. Thus this toy-model can be used as a nice and simplifying `laboratory' for questions about the full theory.Comment: 18 pages, 4 figures. v2: Corrected mistake in bibliography, added appendix with further result

Recombinant lipid transfer protein Tri a 14: a novel heat and proteolytic resistant tool for the diagnosis of baker's asthma

BACKGROUND Baker's asthma is an important occupational allergic disease. Wheat lipid transfer protein (LTP) Tri a 14 is a major allergen associated with wheat allergy. No panel of wheat recombinant allergens for component-resolved diagnosis of baker's asthma is currently available. OBJECTIVE To evaluate the potential role of recombinant Tri a 14 as a novel tool for the diagnosis of baker's asthma, and to test the heat and proteolytic resistance of the wheat LTP allergen. METHODS A cDNA encoding Tri a 14 was isolated and sequenced, the recombinant allergen produced in Pichia pastoris and purified by chromatographic methods. Physicochemical and immunological comparison of the natural and recombinant forms of Tri a 14 was carried out by N-terminal amino acid sequencing, matrix-assisted laser desorption/ionization mass spectrometry, circular dichroism (CD) analysis, IgE immunodetection, and specific IgE determination and ELISA-inhibition assays using a pool or individual sera from 26 patients with baker's asthma. Thermal denaturation and simulated gastrointestinal digestion of both Tri a 14 forms were checked by spectroscopic and electrophoretic methods, respectively, and biological activity by basophil activation test (BAT). RESULTS Natural and recombinant Tri a 14 were similarly folded, as indicated by their nearly identical CD spectra and heat denaturation profiles. A high interclass correlation coefficient (0.882) was found between specific IgE levels to both Tri a 14 proteins in individual sera from baker's asthma patients, but a slightly lower IgE-binding potency of rTri a 14 was detected by ELISA-inhibition assays. Natural and recombinant Tri a 14 elicited positive BAT in two and one out of three patients, respectively. Heat denaturation profiles and simulated gastrointestinal digestion assays indicated that Tri a 14 displayed a high heat and digestive proteolytic resistance, comparable to those of peach Pru p 3, the model food allergen of the LTP family. CONCLUSIONS Recombinant Tri a 14 is a potential tool for baker's asthma diagnosis, based on its physicochemical and immunological similarity with its natural counterpart. Wheat Tri a 14 shows a high thermal stability and resistance to gastrointestinal digestion

MAXI J1659-152: the shortest orbital period black-hole binary

Following the detection of a bright new X-ray source, MAXI J1659-152, a series of observations was triggered with almost all currently flying high-energy missions. We report here on XMM-Newton, INTEGRAL and RXTE observations during the early phase of the X-ray outburst of this transient black-hole candidate. We confirm the dipping nature in the X-ray light curves. We find that the dips recur on a period of 2.4139+/-0.0005 hrs, and interpret this as the orbital period of the system. It is thus the shortest period black-hole X-ray binary known to date. Using the various observables, we derive the properties of the source. The inclination of the accretion disk with respect to the line of sight is estimated to be 60-75 degrees. The companion star to the black hole is possibly a M5 dwarf star, with a mass and radius of about 0.15 M_sun and 0.23 R_sun, respectively. The system is rather compact (orbital separation is about 1.35 R_sun) and is located at a distance of roughly 7 kpc. In quiescence, MAXI J1659-152 is expected to be optically faint, about 28 mag in the V-band.Comment: 5 pages, 4 figures, to be published in the proceedings of the 4th International MAXI Workshop `The First Year of MAXI: Monitoring variable X-ray sources', 2010 Nov 30 - Dec 2, Tokyo, Japa