2,121 research outputs found

    Oxidation-induced changes in mechanical properties of silicon nitride ceramics

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    The effect of oxidation on the room-temperature mechanical properties of four different silicon nitride ceramics is investigated. The strength and the elastic modulus of the whole material and the hardness, the fracture toughness and the elastic modulus of the internal region (without surface oxide layer) are determined for the materials oxidized at temperatures up to 1400°C. It is found that the fracture toughness decreases during oxidation at 1000°C. Reduction of the elastic modulus of the materials oxidized at 1400°C is also observed. A part of the changes in the mechanical properties is interpreted by the changes in the phase composition

    Fe-substituted mullite powders for the in situ synthesis of carbon nanotubes by catalytic chemical vapor deposition

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    Powders of iron-substituted mullite were prepared by combustion and further calcination in air at different temperatures. A detailed study involving notably Mo¨ssbauer spectroscopy showed that the Fe3+ ions are distributed between the mullite phase and a corundum phase that progressively dissolves into mullite upon the increase in calcination temperature. Carbon nanotube-Fe-mullite nanocomposites were prepared for the first time by a direct method involving a reduction of these powders in H2-CH4 and without any mechanical mixing step. The carbon nanotubes formed by the catalytic decomposition of CH4 on the smallest metal particles are mostly double-walled and multiwalled, although some carbon nanofibers are also observed

    221113 - Facility Water Distribution Piping

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    Effect of fly ash washing conditions on the properties of coupling agent modified polypropylene/fly ash composites

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    Two fly ash samples (one from UK, UKFA, and another from South Africa, SAFA) were washed with water and 1 M hydrochloric acid (followed by water) prior to incorporation (at 65% wt) into polypropylene homopolymer, containing an unsaturated carboxylic acid coupling agent (Lubrizol Solplus® C800) with dicumyl peroxide free radical initiator. Melt blending was achieved using a Haake Rheomix 600 mixing chamber, and composite test plaques were compression moulded. Flexural and impact testing was then carried out. Unwashed and water washed fly ash-based composites responded well to C800 modification, and flow microcalorimetry (FMC) and diffuse reflectance Fourier transform infrared spectroscopy studies confirmed strong interaction between C800 and fly ash. However, washing the fly ash with HCl led to a reduction in composite flexural and impact properties. Scanning electron microscopy imaging of the latter composite fracture surfaces revealed poor filler-matrix adhesion, which was thought to be due to reduced interaction between C800 and HCl washed fly ash. The latter was confirmed using FMC. Reduction of C800/fly ash interaction led to a reduction in the nucleation of polypropylene (PP) crystallization and a decrease in melt flow rate. The latter may be due to a shift in locus of PP-C800 addition reactions from the interfacial region to the bulk matrix. © 2013 Society of Plastics Engineers

    Progressive Label Distillation: Learning Input-Efficient Deep Neural Networks

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    Much of the focus in the area of knowledge distillation has been on distilling knowledge from a larger teacher network to a smaller student network. However, there has been little research on how the concept of distillation can be leveraged to distill the knowledge encapsulated in the training data itself into a reduced form. In this study, we explore the concept of progressive label distillation, where we leverage a series of teacher-student network pairs to progressively generate distilled training data for learning deep neural networks with greatly reduced input dimensions. To investigate the efficacy of the proposed progressive label distillation approach, we experimented with learning a deep limited vocabulary speech recognition network based on generated 500ms input utterances distilled progressively from 1000ms source training data, and demonstrated a significant increase in test accuracy of almost 78% compared to direct learning.Comment: 9 page

    1969 July, Memphis State University bulletin

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    Vol. 58, No. 5 of the Memphis State University bulletin containing the schedule of classes for fall semester 1969, 1969 July.https://digitalcommons.memphis.edu/speccoll-ua-pub-bulletins/1321/thumbnail.jp

    On Comon's and Strassen's conjectures

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    Comon's conjecture on the equality of the rank and the symmetric rank of a symmetric tensor, and Strassen's conjecture on the additivity of the rank of tensors are two of the most challenging and guiding problems in the area of tensor decomposition. We survey the main known results on these conjectures, and, under suitable bounds on the rank, we prove them, building on classical techniques used in the case of symmetric tensors, for mixed tensors. Finally, we improve the bound for Comon's conjecture given by flattenings by producing new equations for secant varieties of Veronese and Segre varieties.Comment: 12 page

    Water and small organic molecules as probes for geometric confinement in well- ordered mesoporous carbon material

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    Mesoporous carbon materials were synthesized employing polymers and silica gels as structure directing templates. The basic physico-chemical properties of the synthetic mesoporous materials were characterized by 1H and 13C MAS solid-state NMR, X-ray diffraction, transmission electron microscopy (TEM) and nitrogen adsorption measurements. The confinement effects on small guest molecules such as water, benzene and pyridine and their interactions with the pore surface were probed by a combination of variable temperature 1H-MAS NMR and quantum chemical calculations of the magnetic shielding effect of the surface on the solvent molecules. The interactions of the guest molecules depend strongly on the carbonization temperature and the pathway of the synthesis. All the guest-molecules, water, benzene and pyridine, exhibited high-field shifts by the interaction with the surface of carbon materials. The geometric confinement imposed by the surface causes a strong depression of the melting point of the surface phase of water and benzene. The theoretical calculation of 1H NICS maps shows that the observed proton chemical shifts towards high-field values can be explained as the result of electronic ring currents localized in aromatic groups on the surface. The dependence on the distance between the proton and the aromatic surface can be exploited to estimate the average diameter of the confinement structures
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