Real time in situ characterisation of solids concentration would aid operational understanding and improve efficiency in many industrial systems. This is especially true in the processing of legacy nuclear wastes where hazardous material is encountered. Acoustic methods have been previously demonstrated for the measurement of concentration in solid-liquid systems at a small scale. This study explores the use of the ultrasound array research platform (UARP) for backscatter measurements of concentration at a large scale in a dynamic settling system. The theory of acoustic measurement of solids concentration is described for both backscatter based attenuation and backscatter power methods. Acoustic based backscatter power and attenuation measurements are compared to laboratory analysed samples. Ultrasonic solids concentration analysis is shown to reveal flow dynamics within the settling tank
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