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0-bis(methylsulfanyl)-2,2 0-bi-1,3dithiole-4(5H)-thione

By Kazumasa Ueda A and Kenji Yoza B


0.038; wR factor = 0.090; data-to-parameter ratio = 21.8. The molecular skeleton of the title molecule, C11H6I2S9, is nearly planar [maximum deviation 0.052 (3) A ˚ ] except for the two methyl groups. In the crystal, molecules related by translation along b axis are associated into columns through – interactions between the five-membered rings, with a centroid–centroid distance of 3.593 (5) A ˚. Interaction between adjacent columns is accomplished by short S I contacts of 3.2099 (4) A ˚. Related literature For background to tetrathiafulvalenothioquinone-1,3-dithiolemethid

Topics: For details of the synthesis, see Iwamatsu et al. (1999). For
Year: 2009
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