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organic compounds Acta Crystallographica Section E Structure Reports Online

By Yong Wang, A Kaiqing Fan, B Chenghong Li A, Ge A and Mo K Radiation


R factor = 0.058; wR factor = 0.155; data-to-parameter ratio = 12.1. In the title compound, C19H13F2N3O3, the anilinobenzamide unit is essentially planar, with a maximum deviation of 0.036 (3) A ˚. The nitro group and the benzene ring form dihedral angles of 9.6 (5)and 62.20 (8) , respectively, with the anilinobenzamide unit. An intramolecular N—H O interaction occurs. In the crystal, molecules are linked by weak intermolecular C—H O, N—H O and C—H F hydrogen bonds, which stabilize the structure. Related literature For comparison of bond lengths, see: Allen et al. (1987). For the synthetic procedure, see: Schelz & Inst (1978). = 70.76 (3

Year: 2010
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