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Triol protection with 6-benzoyl-3,4-dihydro-(2H)-pyran.

By Caroline D. L. Baker, John Fawcett, Christopher D. Insley, Derek S. Messenger, Claire L. Newland, Helen L. Overend, Anup B. Patel, Mufakhrul Shah, Bhavna Vara, Davinder Virdee and Bernard J. Rawlings

Abstract

6-Benzoyl-3,4-dihydro-(2H)-pyran will protect 1,2,3-triols such as glycerol as their corresponding spiro-[5-phenyl-3,6,8-trioxabicyclo[3.2.1]octane-4,2′-tetrahydropyran]s and 1,2,4-triols (less efficiently) as the corresponding trioxabicyclo[3.2.2]nonanes; the hexol mannitol is converted into the corresponding bis-protected product.Peer-reviewedPublisher Versio

Publisher: The Royal Society of Chemistry
Year: 2005
DOI identifier: 10.1039/B418035F
OAI identifier: oai:lra.le.ac.uk:2381/622
Journal:

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Citations

  1. (1978). A 3,6,8-trioxabicyclo[3.2.1]octane has been reported previously:
  2. (1995). Tetrahedron: Asymmetry, doi

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