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Residual dipolar couplings by off-magic-angle spinning in solid-state nuclear magnetic resonance spectroscopy

By Giuseppe Pileio, Ying Guo, Tran N. Pham, John M. Griffin, Malcolm H. Levitt and Steven P. Brown

Abstract

A solid-state NMR analogue of the solution-state residual dipolar coupling effect is demonstrated. A small misset of the spinning axis by less than 0.5 changes the modulation frequency of spin-echoes, allowing the estimation of internuclear dipole-dipole couplings and hence internuclear distances

Year: 2007
OAI identifier: oai:eprints.soton.ac.uk:146445
Provided by: e-Prints Soton
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