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Cl-35 quadrupolar constants obtained by solid-state NMR: study of chlorinated Al-O-P clusters, involving OH center dot center dot center dot Cl hydrogen bonds

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Abstract

Simulation of static and MAS NMR spectra obtained at high field (B-0 = 14.08 T) and high spinning frequency (up to v(rot) = 22 kHz) allows the determination of Cl-35 quadrupolar parameters for various cubane-shaped, cage-like and cyclic Al-O-P clusters; the role of (OHCl)-Cl-... contacts is emphasized. (C) 2002 Elsevier Science (USA). All rights reserved

Topics: QD, QC
Publisher: ACADEMIC PRESS INC ELSEVIER SCIENCE
OAI identifier: oai:wrap.warwick.ac.uk:9842
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