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By Edward R. T. Tiekink, Seik Weng Ng, R. Karvembu and N. Gunasekaran


The title molecule, C16H24N2OS, is twisted about the central N(H)—C bond with a C—N(H)—C—N torsion angle of −62.67 (15)°. The carbonyl group is twisted out of the plane of the benzene ring, forming a C—C—C=O torsion angle of −25.06 (17)°. In the crystal, molecules related by centres of symmetry are linked by pairs of intermolecular N—H...S hydrogen bonds, forming eight-membered {...HNCS}2 synthons. These are further connected by weak via C—H...O contacts, forming a two-dimensional array in the bc plane

Topics: Chemistry, QD1-999, Science, Q, DOAJ:Chemistry (General), DOAJ:Chemistry
Publisher: International Union of Crystallography
Year: 2010
DOI identifier: 10.1107/S1600536810037177
OAI identifier:
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