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By Adriano Bof De Oliveira, A Christian, B Inke Jessb, Ro Bresolinc and Mo K Radiation


R factor = 0.037; wR factor = 0.107; data-to-parameter ratio = 15.7. In the title compound, C10H11N3O2S, the 1,3-benzodioxole and hydrazinecarbothioamide fragments are nearly planar [(mean deviations from planarity for non-H atoms of 0.0325 (12) A ̊ and 0.0707 (10) Å, respectively] and subtend a dihedral angle of 29.06 (5). In the crystal, molecules are linked by pairs of almost linear N—H S hydrogen bonds, forming inversion dimers. These dimers are additionally connected by weaker and strongly bent N—H S interactions into chains along [101]. There is one additional weak N— H O contact which, if considered as an interaction, leads to the formation of a three-dimensional network. Related literature For the adapted synthesis of the title compound, see: de Oliveira et al. (2012). For the pharmacological activity of 30,40-(methylenedioxy)acetophenone thiosimecarbazone deriva-tives, see: Silva et al. (1998)

Year: 2013
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